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inquiryProduct description: Product name 2-Isopropylimidazole CAS number 36947-68-9 Assay ≥99% Appearance White crystalline powder Capacity 200mt/year Application Organic synthesis
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inquiryHigh quality 2-Isopropylimidazole Cas 36947-68-9 with steady supply Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed a
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inquiry2-Isopropylimidazole CAS 36947-68-9 2-Isopropyl-1H-imidazole CAS no 36947-68-9 1H-Imidazole,2-(1-methylethyl)- 2-Isopropylimidazole 2-Isopropyl-1H-imidazole 1H-Imidazole,2-(1-methylethyl)- 2-Isopropylimidazole CAS 36947-68-9 2-Isopropyl-1H-im
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inquiry2-Isopropylimidazole Basic information Product Name: 2-Isopropylimidazole Synonyms: 1H-Imidazole, 2-(1-methylethyl)-;2-(1-methylethyl)-1h-imidazol;2-(1-methylethyl)-1H-Imidazole;2-is
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inquiryName: 2-Isopropylimidazole Synonyms:2-Isopropyl-1H-imidazole CAS: 36947-68-9 MF: C6H10N2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:organic synthesis Transportation:By
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Product Name: 2-Isopropylimidazole Synonyms: 1H-Imidazole, 2-(1-methylethyl)-;2-(1-methylethyl)-1h-imidazol;2-(1-methylethyl)-1H-Imidazole;2-isopropyl-1h-imidazole;2-ISOPROPYLIMDAZOLE;2-ISOPROPYLIMIDAZOLE;N-Isopropylimdazole;2-Isopropylimidazol
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryGlyoxal
isobutyraldehyde
A
1H-imidazole
B
2-isopropylimidazole
Conditions | Yield |
---|---|
Stage #1: isobutyraldehyde With ammonia In methanol; water at 25℃; for 1h; Stage #2: Glyoxal With ammonia In methanol; water at 25℃; for 2h; Product distribution / selectivity; | A 2 %Chromat. B 95% |
With ammonia In water at 25℃; for 1h; Product distribution / selectivity; | A 23 %Chromat. B 56% |
2-(1-Methylethyl)-4,5-dihydro-1H-imidazol
2-isopropylimidazole
Conditions | Yield |
---|---|
nickel In ethanol for 48h; Heating / reflux; | 41% |
2-isopropyl-1H-imidazole-4,5-dicarboxylic acid
A
2-isopropylimidazole
B
methylammonium carbonate
Conditions | Yield |
---|---|
With ethanol; ammonia | |
With ammonium hydroxide In ethanol; water at 0 - 20℃; for 96h; | |
at 0 - 25℃; for 24h; |
2-isopropylimidazole
N-(2,2-Dimethoxy-ethyl)-isobutyramidine
2-isopropylimidazole
Conditions | Yield |
---|---|
Stage #1: N-(2,2-Dimethoxy-ethyl)-isobutyramidine With thioacetamide In methanol at 0 - 45℃; Stage #2: With hydrogenchloride In methanol at 0 - 80℃; |
2-isopropylimidazole
Conditions | Yield |
---|---|
at 50℃; for 1h; | 100% |
2-isopropylimidazole
chloro(dimethylsulfide) gold(I)
A
dimethylsulfide
B
(2-isopropylimidazole)2AuCl
Conditions | Yield |
---|---|
In dichloromethane refluxed for 2 h; evapd. to dryness, stirred under Et2O for 24 h, filtered, washed with Et2O; elem. anal.; | A n/a B 100% |
Conditions | Yield |
---|---|
With sodium hydroxide; tetra-(n-butyl)ammonium iodide In toluene for 20h; Heating; | 98% |
2-isopropylimidazole
4,5-diiodo-2-isopropylimidazole
Conditions | Yield |
---|---|
With iodine; sodium carbonate In 1,4-dioxane; water at 20℃; for 24h; | 97% |
With iodine; potassium iodide; sodium hydroxide In water at 20℃; Inert atmosphere; | 44% |
With iodine; sodium carbonate In 1,4-dioxane; water at 20℃; |
Conditions | Yield |
---|---|
With 2,3,4,5,6-pentafluorophenol; briphos; bis(dibenzylideneacetone)-palladium(0) In dichloromethane at 50℃; for 24h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h; Inert atmosphere; Glovebox; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate at 20℃; for 10h; Aza-Michael addition; Neat (no solvent); | 93% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; tetrabutylammomium bromide; 1,10-phenanthroline-4,7-diol In water at 100℃; for 24h; Ullmann Condensation; Schlenk technique; Inert atmosphere; Green chemistry; | 93% |
2-isopropylimidazole
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 90% |
2-isopropylimidazole
methyl chloroformate
methyl 2-isopropyl-1-imidazolecarboxylate
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; for 16h; Inert atmosphere; | 89% |
2-chloropyrimidine
2-isopropylimidazole
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Stage #2: 2-chloropyrimidine In N,N-dimethyl-formamide; mineral oil at 130℃; | 88% |
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole With potassium tert-butylate at 20℃; for 1h; Stage #2: ethyl bromide In acetonitrile at 20℃; for 8h; | 88% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; tetrabutylammomium bromide; 1,10-phenanthroline-4,7-diol In water at 100℃; for 24h; Ullmann Condensation; Schlenk technique; Inert atmosphere; Green chemistry; | 87% |
Conditions | Yield |
---|---|
In ethanol an ethanolic soln. of ligands was added to a stirred ethanol suspn. of Hg(SCN)2, the mixt. was kept overnight in refrigerator;; water was added; ppt. was filtered; elem. anal.; | 86% |
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole With potassium carbonate In acetonitrile at 50℃; for 0.666667h; Stage #2: C11H13NO4S In acetonitrile at 75℃; | 85.3% |
2-isopropylimidazole
(triphenylphosphine)gold(I) chloride
Conditions | Yield |
---|---|
With sodium hydroxide In methanol byproducts: H2O, Cl(1-); NaOH in MeOH and the org. compd. added to a suspn. of the Au-complex inMeOH, stirred for 4 h; evapd. to dryness under reduced pressure, extd. with benzene, concd., pptd. by addn. of petroleum ether, purified twice in the same way, elem. anal.; | 84% |
With tetra(n-butyl)ammonium hydrogensulfate In sodium hydroxide; dichloromethane byproducts: H2O, Cl(1-); soln. of the Au-complex and imidazole in CH2Cl2 mixed under stirring with an ice-cold soln. of tetrabutylammonium hydrogen sulphate in aq. NaOH, stirred for 2 h at room temp.; org. layer sepd., washed with water till neutral washing, dried over Na2SO4, evapd. to dryness under reduced pressure, extd. with benzene, concd., pptd. by addn. of petroleum ether, purified twice in the same way, elem. anal.; | 20% |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In dimethyl sulfoxide at 100℃; for 16h; optical yield given as %de; diastereoselective reaction; | A 84% B n/a |
2-isopropylimidazole
1-(2,2-dibromovinyl)-4-methylbenzene
C15H16N2
Conditions | Yield |
---|---|
With (1,10-phenanthroline)(triphenylphosphine)CuBr; caesium carbonate In dimethyl sulfoxide at 80℃; for 3h; | 84% |
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole; C18H17FO3 In ethanol at 160℃; for 0.25h; Microwave irradiation; Stage #2: With hydrogenchloride In methanol | 84% |
2-isopropylimidazole
1-(2-(oxiran-2-ylmethoxy)phenyl)-3-phenylpropan-1-one
C24H28N2O3*ClH
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole; 1-(2-(oxiran-2-ylmethoxy)phenyl)-3-phenylpropan-1-one In ethanol at 160℃; for 0.25h; Microwave irradiation; Stage #2: With hydrogenchloride In methanol | 84% |
tetrahydrofuran
2-isopropylimidazole
1-(tetrahydrofuran-2-yl)-2-isopropyl-1H-imidazole
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; iron(III) chloride hexahydrate In decane at 80℃; for 3h; Inert atmosphere; Molecular sieve; | 83% |
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole; C18H17FO3 In ethanol at 160℃; for 0.25h; Microwave irradiation; Stage #2: With hydrogenchloride In methanol | 82% |
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole; C18H16F2O3 In ethanol at 160℃; for 0.25h; Microwave irradiation; Stage #2: With hydrogenchloride In methanol | 82% |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In dimethyl sulfoxide at 100℃; for 16h; optical yield given as %de; diastereoselective reaction; | A 81% B n/a |
2-isopropylimidazole
5-bromo-pyridin-3-ylmethyl chloride
3-bromo-5-(2-isopropylimidazol-1-ylmethyl)pyridine
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.333333h; Inert atmosphere; Stage #2: 5-bromo-pyridin-3-ylmethyl chloride In N,N-dimethyl-formamide; mineral oil at 60℃; Inert atmosphere; | 81% |
2-isopropylimidazole
1-[tricyclohexylphosphine-gold]-2isopropylimidazole*benzene
Conditions | Yield |
---|---|
With tetra-n-butylammonium hydrogen sulphate In dichloromethane addn. of CH2Cl2 soln. of complex and imidazole to an ice-cold suspn. of(C4H9)4NHSO4 in aq. NaOH, stirred at room temp. for 2 h; organic layer sepd., washed with water till neutral washings, dried over Na2SO4, evapd. to dryness, extd. with benzene, concd., addn. of pentane, pptn., twice crystd.; elem. anal.; | 80% |
2-isopropylimidazole
carbonic acid dimethyl ester
2-isopropyl-1-methyl-1(H)-imidazole
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate at 100℃; for 10h; | 79% |
2-isopropylimidazole
(2S,4R)-1-allyloxycarbonyl-4-tert-butyldimethylsilyloxy-2-(methanesulfonyloxymethyl)pyrrolidine
(2S,4R)-1-allyloxycarbonyl-4-tert-butyldimethylsilyloxy-2-(2-isopropylimidazol-1-ylmethyl)pyrrolidine
Conditions | Yield |
---|---|
Stage #1: 2-isopropylimidazole With sodium hydride In N,N-dimethyl-formamide at 0℃; Stage #2: (2S,4R)-1-allyloxycarbonyl-4-tert-butyldimethylsilyloxy-2-(methanesulfonyloxymethyl)pyrrolidine In N,N-dimethyl-formamide at 60 - 70℃; | 79% |
2-isopropylimidazole
1-Bromo-2-phenylacetylene
2-isopropyl-1-(phenylethynyl)-1H-imidazole
Conditions | Yield |
---|---|
With copper(II) oxide; potassium hydroxide In 1,4-dioxane at 80℃; for 13h; | 79% |