As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:3695-77-0
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Type:Trading Company
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Min.Order:1 Kilogram
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inquiryTRIPHENYLMETHYL MERCAPTAN CAS:3695-77-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Min.Order:0 Metric Ton
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Conditions | Yield |
---|---|
With Lawessons reagent In 1,2-dimethoxyethane for 15h; Mechanism; Ambient temperature; various alcohols, other solvents, other temperatures; | 100% |
With Lawessons reagent In toluene for 0.2h; Quantum yield; Heating; DME, room temperature; | 100% |
With Lawessons reagent In 1,2-dimethoxyethane for 15h; Ambient temperature; | 100% |
triphenylmethanethiol
Conditions | Yield |
---|---|
With DL-dithiothreitol; triethylamine In tetrahydrofuran; water at 20℃; for 0.25h; | 96% |
Conditions | Yield |
---|---|
With methanol; tetra-n-butylammonium cyanide In chloroform at 20℃; for 3h; | 92% |
Conditions | Yield |
---|---|
In ethyl acetate for 13h; Heating; | A 26% B 23% C 69% |
endo-2-chloro-exo-1-(triphenylmethyldithio)bicyclo<2.2.1>heptane
A
triphenylmethanethiol
B
trityl chloride
Conditions | Yield |
---|---|
In ethyl acetate for 40h; Heating; | A 21% B 19% C 68% |
(1,1-dimethylethyl)dimethyl[[(triphenylmethyl)thio]methoxy]silane
triphenylmethanethiol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at -78℃; for 0.25h; | 68% |
With tetrabutyl ammonium fluoride In tetrahydrofuran at -78 - -10℃; for 0.3h; | 68% |
Conditions | Yield |
---|---|
In ethyl acetate for 10h; Heating; | A 27% B 19% C 67% |
Conditions | Yield |
---|---|
In ethyl acetate for 8h; Heating; | A 24% B 20% C 65% |
Conditions | Yield |
---|---|
In ethyl acetate for 15h; Heating; | A 28% B 21% C 65% |
2,3-dimethyl-buta-1,3-diene
A
triphenylmethanethiol
B
1,2-dithia-4,5-dimethyl-4-cyclohexene
C
1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene
Conditions | Yield |
---|---|
With trans-2-chloro-1-(triphenylmethyltrithio)cyclohexane In ethyl acetate for 15h; Heating; Further byproducts given; | A 29% B 8% C 63% D 12% |
With trans-2-chloro-1-(triphenylmethyldithio)cyclohexane In ethyl acetate for 10h; Heating; Further byproducts given; | A 28% B 10% C 58% D 16% |
endo-2-chloro-exo-1-(triphenylmethyldithio)bicyclo<2.2.1>heptane
A
triphenylmethanethiol
Conditions | Yield |
---|---|
In ethyl acetate Heating; | A 12% B 60% |
2,3-dimethyl-buta-1,3-diene
A
triphenylmethanethiol
B
1,2-dithia-4,5-dimethyl-4-cyclohexene
C
1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene
Conditions | Yield |
---|---|
With trans-2-chloro-1-(triphenylmethyltrithio)cyclopentane In ethyl acetate for 24h; Heating; Further byproducts given; | A 30% B 9% C 60% D 22% |
With trans-2-chloro-1-(triphenylmethyldithio)cyclopentane In ethyl acetate for 8h; Heating; Further byproducts given; | A 26% B 8% C 50% D 24% |
Conditions | Yield |
---|---|
In ethyl acetate for 42h; Heating; | A 25% B 21% C 60% |
2,3-dimethyl-buta-1,3-diene
A
triphenylmethanethiol
B
1,2-dithia-4,5-dimethyl-4-cyclohexene
C
1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene
Conditions | Yield |
---|---|
With endo-2-chloro-exo-1-(triphenylmethyldithio)bicyclo<2.2.1>heptane In ethyl acetate for 36h; Heating; Further byproducts given; | A 25% B 6% C 24% D 59% |
2,3-dimethyl-buta-1,3-diene
A
triphenylmethanethiol
B
1,2-dithia-4,5-dimethyl-4-cyclohexene
C
1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene
Conditions | Yield |
---|---|
With endo-2-chloro-exo-1-(triphenylmethyldithio)bicyclo<2.2.2>octane In ethyl acetate for 36h; Heating; Further byproducts given; | A 23% B 5% C 19% D 51% |
2,3-dimethyl-buta-1,3-diene
A
triphenylmethanethiol
B
1,2-dithia-4,5-dimethyl-4-cyclohexene
C
trityl chloride
D
1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene
Conditions | Yield |
---|---|
With trans-2-chloro-3-(triphenylmethyldithio)-1,4-dioxane In ethyl acetate for 13h; Heating; | A 24% B 7% C 20% D 45% |
Conditions | Yield |
---|---|
With hydrogen sulfide; sodium ethanolate | |
With potassium hydrosulfide; benzene | |
With 1,4-dioxane; hydrogen sulfide | |
With sodium hydrogensulfide In water; acetone for 1.25h; Inert atmosphere; |
triphenylmethyl bromide
triphenylmethanethiol
Conditions | Yield |
---|---|
With diethyl ether; sulfur; benzene |
hydrogen sulfide
sodium ethanolate
trityl chloride
triphenylmethanethiol
α,α-diphenylbenzenemethanesulfenyl chloride
A
triphenylmethanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 88 percent / CH2Cl2 / 7 h / Ambient temperature 2: 24 percent / ethyl acetate / 8 h / Heating View Scheme |
triphenylmethanedithiosulfenyl chloride
A
triphenylmethanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / CH2Cl2 / 7 h / Ambient temperature 2: 27 percent / ethyl acetate / 10 h / Heating View Scheme |
tritylsulfenyl chloride
triphenylmethanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent 2: 12 percent / ethyl acetate / Heating View Scheme |
α,α-diphenylbenzenemethanesulfenyl chloride
triphenylmethanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent 2: 12 percent / ethyl acetate / Heating View Scheme |
triphenylmethane hydrodisulfide
triphenylphosphine
A
triphenylmethanethiol
B
triphenylphosphine sulfide
Conditions | Yield |
---|---|
In dichloromethane-d2 Inert atmosphere; Glovebox; |
tetrahydrofuran
triphenylmethane hydrodisulfide
A
borane-THF
B
triphenylmethanethiol
C
hydrosulfide anion
Conditions | Yield |
---|---|
With tetrabutylammonium borohydride In dichloromethane-d2 Inert atmosphere; Glovebox; |
tritylacetyldisulfide
triphenylmethanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / ethanol; toluene / 39 h / Inert atmosphere 2: dichloromethane-d2 / Inert atmosphere; Glovebox View Scheme |
Conditions | Yield |
---|---|
With tetra-n-butylammonium cyanide In dichloromethane-d2 at 25℃; Reagent/catalyst; Inert atmosphere; Glovebox; |
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