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1-<2-<(2-aminoethyl)amino>ethyl>aziridine
1,5-diamino-3-azapentane
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
With hydrogen cation In water at 50℃; Rate constant; Thermodynamic data; also at 60 and 70 deg C; Ea, ΔH; | |
With hydrogen cation In water |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
With sodium hydroxide In water at 220℃; for 3.16667h; Autoclave; Inert atmosphere; |
3,6,9,12-tetraazatetradecane-1,14-diamine
heptadecanoic acid
guanidine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 3,6,9,12-tetraazatetradecane-1,14-diamine; heptadecanoic acid With toluene-4-sulfonic acid at 160℃; for 3.33h; Stage #2: guanidine hydrochloride at 160 - 180℃; for 6h; | 97% |
3,6,9,12-tetraazatetradecane-1,14-diamine
sodium tetraphenyl borate
cadmium(II) acetate dihydrate
Conditions | Yield |
---|---|
In methanol byproducts: NaOOCCH3, H2O; dissolving Cd(OAc)2*2H2O in methanol, dropwise addn. of pentaethylenehexamine in methanol and then NaBPh4 dissolved in methanol with stirring; crystn. after 1 h; filtration, washing with methanol, drying in vac., dynamic vac. for ca. 10 h to remove MeOH, elem. anal.; | 86% |
Conditions | Yield |
---|---|
In methanol at 70℃; for 10h; | 80.1% |
Conditions | Yield |
---|---|
In methanol at 70℃; for 10h; | 75% |
3,6,9,12-tetraazatetradecane-1,14-diamine
mono-6-deoxy-6-(p-tolylsulphonyl)-β-cyclodextrin
Conditions | Yield |
---|---|
at 75℃; for 8h; Inert atmosphere; | 68.5% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
In methanol byproducts: H2O; dropwise addn. of a soln. of pentaethylenehexamine to a stirred soln. of Cd(BF4)2*6H2O in methanol; ppt. after 1 h, filtration, washing two times with small amts. of ice-cold methanol, drying in vac., elem. anal.; | 66% |
ferrocenecarboxaldehyde
3,6,9,12-tetraazatetradecane-1,14-diamine
1,18-diferrocenyl-2,5,8,11,14,17-hexaazaoctadecane
Conditions | Yield |
---|---|
With LiAlH4 In tetrahydrofuran; ethanol refluxing the aldehyde and the amine in EtOH for 3 h, evapn. to dryness,dissoln. (THF), addn. of LiAlH4, reflux under argon for 1 h, quenching with H2O; filtration, evapn. to dryness, addn. of basic H2O and CH2Cl2, drying (Na2SO4), chromy. (alumina; CH2Cl2, then CH2Cl2/MeOH); elem. anal.; | 65% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
With triethylamine In MeOH-water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; acetic acid | 60% |
Conditions | Yield |
---|---|
Stage #1: 3,6,9,12-tetraazatetradecane-1,14-diamine; (E/Z)-3,7-dimethyl-2,6-octadienal With titanium(IV) isopropylate In methanol at 20℃; for 12h; Stage #2: With sodium tetrahydroborate In methanol at 0℃; for 2h; | 58% |
3,6,9,12-tetraazatetradecane-1,14-diamine
[Hg(4-(2-aminoethyl)-triethylenetetramine)][HgCl4]
Conditions | Yield |
---|---|
In methanol soln. of ligand added dropwise to MeOH soln. of HgCl2 (1:2 molar ratio) at room temp.; filtered, crystd. on storage, septd., washed (hexane), dried (vac.), elem. anal.; | 55% |
3,6,9,12-tetraazatetradecane-1,14-diamine
(E)-isopropyl cinnamate
Conditions | Yield |
---|---|
at 65℃; for 48h; aza-Michael addition; | 53% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
In methanol soln. of ligand added dropwise to MeOH soln. of CdCl2 (2:5 molar ratio) at room temp.; filtered, crystd. on storage, septd., washed (hexane), dried (vac.), elem. anal.; | 51% |
Conditions | Yield |
---|---|
In water at 140℃; for 120h; Autoclave; High pressure; | 51% |
germanium
selenium
3,6,9,12-tetraazatetradecane-1,14-diamine
water
Conditions | Yield |
---|---|
at 170℃; for 168h; Sealed tube; High pressure; | 51% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
In methanol soln. of ligand reacted with of MeOH soln. of Cd compd., NaN3 added (2:3:4 molar ratio); filtered, crystd. on storage, septd., washed (hexane), dried (vac.), elem. anal.; | 50% |
germanium
selenium
3,6,9,12-tetraazatetradecane-1,14-diamine
water
Conditions | Yield |
---|---|
at 170℃; for 168h; Sealed tube; High pressure; | 47% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
Stage #1: 3,6,9,12-tetraazatetradecane-1,14-diamine; (6Z)-3,7,11-trimethyldodeca-2,6,10-trienal With titanium(IV) isopropylate In methanol at 20℃; for 12h; Stage #2: With sodium tetrahydroborate In methanol at 0℃; for 2h; | 47% |
germanium
selenium
3,6,9,12-tetraazatetradecane-1,14-diamine
water
Conditions | Yield |
---|---|
at 170℃; for 168h; Sealed tube; High pressure; | 46% |
germanium
selenium
3,6,9,12-tetraazatetradecane-1,14-diamine
water
Conditions | Yield |
---|---|
at 170℃; for 168h; Sealed tube; High pressure; | 43% |
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
With O2; HClO4 In water bubbling air through a soln. for 36 h at 25°C; filtered; concentrated; ethanol added; pptd.; filtered; washed with ethanol and ether; chromy. (HClO4); elem. anal.; | 40% |
Conditions | Yield |
---|---|
In methanol at 170℃; for 6h; Autoclave; High pressure; | 38% |
Conditions | Yield |
---|---|
With hydrogen; C29H33BNOP2Ru In tetrahydrofuran; water at 145℃; under 60006 Torr; for 12h; | 38% |
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane for 5.5h; Heating; | 35% |
germanium
selenium
cerium(IV) chloride
3,6,9,12-tetraazatetradecane-1,14-diamine
Conditions | Yield |
---|---|
at 170℃; for 168h; Sealed tube; High pressure; | 33% |
2,6-Dibromopyridine
3,6,9,12-tetraazatetradecane-1,14-diamine
sodium t-butanolate
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane Heating; | A 27% B 12% |
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane Heating; | A 10% B 21% |
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; [Pd(dibenzylideneacetone)2] In 1,4-dioxane Heating; | A 10 % Spectr. B 1.5% |
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane for 8h; Heating; | A n/a B 25% C n/a |
3,6,9,12-tetraazatetradecane-1,14-diamine
1,8-dichloroanthracene
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In 1,4-dioxane for 72h; Heating; | 22% |
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane Heating; | A 10% B 21% |
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In 1,4-dioxane Inert atmosphere; Reflux; | A 10% B 21% |
Conditions | Yield |
---|---|
With sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane for 8h; Heating; | 4% |
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