Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:4427-92-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:4427-92-3
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Sartort Biopharma Co., Ltd
Appearance:- Storage:ln stock Package:25kg/Barrel Application:Synthetic material intermediate Transportation:Express/Sea/Air Port:Any port in China
Cas:4427-92-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryShanghai Upbio Tech Co.,Ltd
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:4427-92-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryQingdao Beluga Import and Export Co., LTD
Carbonic acid 1-phenylethylene ester CAS:4427-92-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quali
Cas:4427-92-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:4427-92-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:4427-92-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryTAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD
Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:4427-92-3
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryKono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Hubei Taiho Chemical Co.,LTD
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryXian Changyue Biological Technology Co., Ltd.
best seller Application:API
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Manufacturers
inquiryAntimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBaoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
DB BIOTECH CO., LTD
best seller Application:API
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Trading Company
inquiryHangzhou Fandachem Co.,Ltd
Phenylethylene carbonate cas 4427-92-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Henan Kanbei Chemical Co.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirySAGECHEM LIMITED
laboratory Application:Synthetic building block
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryShanghai Chinqesen Biotechnology Co., Ltd.
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
Hebei Muhuang Technology Co., Ltd
best seller Application:API
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Trading Company
inquiryZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Trading Company
inquiryZouping Mingxing Chemical Co.,Ltd.
CaPurity:97% Package:100g 1kgrbonic acid 1-phenylethylene ester CAS: 4427-92-3 Appearance:colorless liquid Storage:ambient condition Package:according to quantity Application:chemical synthesis Port:Any port
Cas:4427-92-3
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryShanghai united Scientific Co.,Ltd.
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryNanjing Raymon Biotech Co., Ltd.
Carbonicacid1-phenylethyleneesterAppearance:Good Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx
Sino-Biochemical Laboratory Co.,Ltd
High quality ,special structure, regular with stock , custom synthese ,quotation with 24hrsAppearance:Good Storage:G to KG to 100KG Application:With high quality for lab research or production in pharm or special material area . With stock or custom
Cas:4427-92-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHebei Ruishun Trade Co.,Ltd
Supply top quality products with a reasonable price Application:api
Chemical Co.Ltd
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
Synthetic route
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; tetrabutylammomium bromide; zinc dibromide; silica gel; gold In decane at 80℃; under 60004.8 Torr; for 4h; | 100% |
| With [aluminum((1R,2R)-N,N′-bis(3,5-di-tert-butyl-salicylidene)cyclohexane-1,2-diamine)2O]; tetrabutylammomium bromide at 60℃; under 3750.38 Torr; for 24h; Mechanism; Reagent/catalyst; Temperature; Pressure; Autoclave; | 100% |
| With tetrabutylammomium bromide at 105℃; under 760.051 Torr; for 20h; Schlenk technique; | 100% |
| Conditions | Yield |
|---|---|
| With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In 2-methyltetrahydrofuran at 30℃; for 2h; Reagent/catalyst; Solvent; | 99% |
| With iron(II) bromide In 1,4-dioxane at 150℃; for 18h; Inert atmosphere; Sealed tube; | 96% |
| Conditions | Yield |
|---|---|
| With aluminum oxide; cesium fluoride at 129.85℃; for 0.416667h; | 98% |
| aluminum oxide; cesium fluoride at 129.85℃; for 0.416667h; | 98% |
| With MgLa mixed oxide at 125℃; for 2h; | 98% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide at 80℃; under 15001.5 Torr; for 10h; Reagent/catalyst; Time; Autoclave; | 98% |
| With tert.-butylhydroperoxide; aniline In neat (no solvent) at 100℃; under 15001.5 Torr; for 5h; Catalytic behavior; Reagent/catalyst; Solvent; Time; Temperature; Pressure; | 97% |
| With N-Bromosuccinimide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene at 60℃; under 12929 Torr; for 2 - 3h; Product distribution / selectivity; | 85% |
-
-
93-56-1
phenylethane 1,2-diol
-
-
124-38-9
carbon dioxide
-
-
115-19-5
2-methyl-but-3-yn-2-ol
-
A
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
B
-
115-22-0
3-Hydroxy-3-methyl-2-butanone
| Conditions | Yield |
|---|---|
| With 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) chloride In acetonitrile at 80℃; under 15001.5 Torr; for 24h; Autoclave; Sealed tube; chemoselective reaction; | A 98% B 91 %Chromat. |
| With silver(l) oxide; N,N,N',N'-tetramethylguanidine In acetonitrile at 80℃; under 7500.75 Torr; for 12h; Autoclave; | A 95 %Spectr. B 97 %Spectr. |
| Conditions | Yield |
|---|---|
| With N-chloro-succinimide; (neocuproine)Pd(OAc)2; sodium acetate In acetonitrile at 55℃; under 760.051 Torr; for 24h; Molecular sieve; | 97% |
| With air; potassium iodide; palladium(II) iodide In ISOPROPYLAMIDE at 100℃; under 15201 Torr; for 15h; Autoclave; | 94% |
| Stage #1: phenylethane 1,2-diol; carbon monoxide With sulfur; triethylamine In N,N-dimethyl-formamide at 80℃; under 7500.75 Torr; for 5h; Inert atmosphere; Autoclave; Stage #2: With copper(ll) bromide In N,N-dimethyl-formamide at 20℃; under 760.051 Torr; for 16h; | 94% |
| Conditions | Yield |
|---|---|
| With 2-Cyanopyridine; cerium(IV) oxide at 179.84℃; under 37503.8 Torr; for 48h; Autoclave; | 95% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 70℃; under 7500.75 Torr; for 18h; Autoclave; | 79% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,1-dibromomethane at 70℃; under 7500.75 Torr; for 18h; Reagent/catalyst; Autoclave; Ionic liquid; | 79% |
| Conditions | Yield |
|---|---|
| With γ-Fe2O3-immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene nanoparticles (MNPs-TBD) at 125℃; for 10h; | 95% |
-
-
93-56-1
phenylethane 1,2-diol
-
-
1659-31-0
2,2'-dipyridyl carbonate
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| In toluene at 110℃; for 0.5h; | 94% |
-
-
124-38-9
carbon dioxide
-
-
1774-47-6
trimethylsulfoxonium iodide
-
-
100-52-7
benzaldehyde
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| Stage #1: trimethylsulfoxonium iodide With sodium hydride In dimethyl sulfoxide at 25℃; for 0.0833333h; Inert atmosphere; Stage #2: benzaldehyde In tetrahydrofuran; dimethyl sulfoxide for 1h; Inert atmosphere; Stage #3: carbon dioxide In tetrahydrofuran; dimethyl sulfoxide at 40℃; under 760.051 Torr; for 6h; Inert atmosphere; | 94% |
-
-
93-56-1
phenylethane 1,2-diol
-
-
3582-05-6
trifluoromethyl trifluoromethanesulfonate
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| With triethylamine In acetonitrile at 20℃; for 1h; Reagent/catalyst; Sealed tube; | 94% |
| Conditions | Yield |
|---|---|
| 93.6% |
| Conditions | Yield |
|---|---|
| With 4C33H15O6(3-)*6Zr(4+)*4O(2-)*4HO(1-)*4H2O; tetrabutylammomium bromide at 100℃; under 760.051 Torr; for 16h; Catalytic behavior; | 92.8% |
| With carbon dioxide; pyrrolidine hydrochloride at 195℃; under 44130.5 Torr; | |
| Multi-step reaction with 2 steps 1: COCl2; pyridine / Behandeln des Reaktionsgemisches mit NH3 in Benzol 2: water View Scheme | |
| With potassium iodide; L-Tryptophan at 120℃; under 15001.5 Torr; for 2h; | 22 %Chromat. |
| With ZnBr2 complex with hybrid polymer based on 5,5'-dibromo-2,2'-bipyridine and octavinylsilsesquioxane at 100℃; under 750.075 Torr; for 72h; Reagent/catalyst; Temperature; Schlenk technique; | 89 %Spectr. |
-
-
2425-28-7
2-Bromo-1-phenylethanol
-
-
58345-96-3
Tetramethylammonium hydrogen carbonate
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| In acetonitrile at 20℃; for 0.25h; | 92% |
| Conditions | Yield |
|---|---|
| With iron(II) bromide In 1,4-dioxane at 150℃; for 18h; Reagent/catalyst; Solvent; Inert atmosphere; Sealed tube; | 90% |
| With zinc(II) chloride at 160℃; under 112.511 Torr; for 3h; Ionic liquid; | 81.2% |
| With 1-hexadecyl-3-methylimidazolium chloride; zinc(II) chloride In neat (no solvent) at 160℃; under 112.511 Torr; for 3h; Green chemistry; | 81.2% |
-
-
292638-84-7
styrene
-
-
144-55-8
sodium hydrogencarbonate
-
A
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
B
-
2425-28-7
2-Bromo-1-phenylethanol
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 30℃; for 1h; Microwave irradiation; | A 6% B 89% |
| With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 100℃; for 1h; Microwave irradiation; | A 70% B 20% |
-
-
93-56-1
phenylethane 1,2-diol
-
-
622-46-8
carbamic acid phenyl ester
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| With iron(II) bromide In 1,4-dioxane at 150℃; for 18h; Inert atmosphere; Sealed tube; | 89% |
| Conditions | Yield |
|---|---|
| at 25℃; under 750.075 Torr; for 24h; Inert atmosphere; Schlenk technique; | 89% |
| With 1-carboxypropyl-imidazolium bromide at 120℃; under 11251.1 Torr; for 2h; | 86.85% |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In water; acetone at 24 - 60℃; for 18h; Solvent; Microwave irradiation; | 86% |
-
-
96-09-3
styrene oxide
-
-
124-38-9
carbon dioxide
-
A
-
93-56-1
phenylethane 1,2-diol
-
B
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| With cobalt 1,4-benzenedicarboxylate; 1-butyl-4-aza-1-azoniabicyclo[2.2.2]octane bromide In neat (no solvent) at 70℃; under 760.051 Torr; for 27h; | A 9% B 85% |
| With Zn(2,5-bis{N-(2,6-diisopropylphenyl)iminomethyl}pyrrole)2; tetrabutylammomium bromide at 105℃; under 760.051 Torr; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Schlenk technique; Inert atmosphere; | A n/a B 80% |
| With C16H18Cl2CrN4(1+)*Cl(1-); tetra-(n-butyl)ammonium iodide In dichloromethane at 100℃; under 15001.5 Torr; for 18h; Catalytic behavior; Reagent/catalyst; Autoclave; | A 12 %Chromat. B 79 %Chromat. |
-
-
292638-84-7
styrene
-
-
144-55-8
sodium hydrogencarbonate
-
A
-
96-09-3
styrene oxide
-
B
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In water; acetone at 60℃; for 7.5h; Time; Microwave irradiation; | A 11% B 78% |
| With N-Bromosuccinimide In water; acetone at 60℃; for 7.5h; Sealed tube; | A 45% B 37% |
-
-
124-38-9
carbon dioxide
-
-
40434-87-5, 40435-14-1, 127911-68-6, 40348-74-1
toluene-4-sulfonic acid 2-hydroxy-2-phenylethyl ester
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| With caesium carbonate In N,N-dimethyl-formamide at 40℃; under 760.051 Torr; for 15h; Inert atmosphere; Glovebox; Green chemistry; | 77% |
-
-
96-09-3
styrene oxide
-
-
124-38-9
carbon dioxide
-
A
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
B
-
98-86-2
acetophenone
| Conditions | Yield |
|---|---|
| With (2-hydroxyphenyl)diphenyl(propyl)phosphonium iodide In neat (no solvent) at 23℃; under 7500.75 Torr; for 24h; Autoclave; | A 74% B n/a |
| Conditions | Yield |
|---|---|
| With pyridine In tetrahydrofuran for 2h; Heating; | 73% |
| Conditions | Yield |
|---|---|
| With cobalt(II) nitrate hexahydrate; 2,5-dihydroxyterephthalohydrazide In dimethyl sulfoxide at 100℃; under 4500.45 Torr; for 5h; | 73% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In water; acetone at 85℃; under 6723.1 Torr; for 0.166667h; Flow reactor; |
-
-
292638-84-7
styrene
-
-
144-55-8
sodium hydrogencarbonate
-
A
-
96-09-3
styrene oxide
-
B
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
C
-
2425-28-7
2-Bromo-1-phenylethanol
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In water; acetone at 60℃; for 0.166667h; Time; Microwave irradiation; | A 15% B 9% C 73% |
| With N-Bromosuccinimide In water; N,N-dimethyl-formamide at 80℃; for 1h; Microwave irradiation; | A 10% B 65% C 10% |
| With N-Bromosuccinimide In water; acetone at 60℃; for 1h; Solvent; Microwave irradiation; | A 40% B 48% C 10% |
| With N-Bromosuccinimide In water; acetone at 60℃; for 3h; Sealed tube; | A 47% B 36% C 8% |
| With N-Bromosuccinimide In water; acetone at 60℃; for 1h; Sealed tube; | A 41% B 24% C 33% |
-
-
124-38-9
carbon dioxide
-
-
1774-47-6
trimethylsulfoxonium iodide
-
-
100-52-7
benzaldehyde
-
A
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
B
-
57308-70-0, 85611-59-2, 100349-67-5, 54766-50-6
2-iodo-1-phenylethan-1-ol
| Conditions | Yield |
|---|---|
| Stage #1: trimethylsulfoxonium iodide With sodium hydride In dimethyl sulfoxide at 25℃; for 0.0833333h; Inert atmosphere; Stage #2: benzaldehyde In dimethyl sulfoxide for 1h; Inert atmosphere; Stage #3: carbon dioxide In dimethyl sulfoxide at 80℃; under 760.051 Torr; for 12h; Inert atmosphere; | A 71% B 23% |
| Stage #1: trimethylsulfoxonium iodide With sodium hydride In dimethyl sulfoxide at 25℃; for 0.0833333h; Inert atmosphere; Stage #2: benzaldehyde In dimethyl sulfoxide for 1h; Inert atmosphere; Stage #3: carbon dioxide In dimethyl sulfoxide at 40℃; under 760.051 Torr; for 12h; Temperature; Inert atmosphere; | A 30% B 65% |
-
-
292638-84-7
styrene
-
-
124-38-9
carbon dioxide
-
A
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
B
-
102921-26-6, 93-52-7
(1,2-dibromoethyl)benzene
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene In water under 15514.9 Torr; for 3h; | A 65% B 20% |
-
-
93-56-1
phenylethane 1,2-diol
-
-
530-62-1
1,1'-carbonyldiimidazole
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
| Conditions | Yield |
|---|---|
| In benzene for 3h; Heating; | 64% |
| Conditions | Yield |
|---|---|
| With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; hydrogen In tetrahydrofuran at 140℃; for 4h; Autoclave; | A > 99 %Chromat. B 99% |
| With C23H21MnN2O3P(1+)*Br(1-); potassium tert-butylate; hydrogen In 1,4-dioxane at 140℃; under 37503.8 Torr; for 16h; Autoclave; | A 95 %Chromat. B 99% |
| With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)-amino]ruthenium(II); potassium carbonate In isopropyl alcohol at 140℃; Glovebox; | A 93 %Chromat. B 95% |
-
-
4427-92-3
4-Phenyl-1,3-dioxolan-2-one
-
-
99342-73-1, 31121-09-2
1-phenyl-2-phenylaminoethanol
-
-
7426-72-4
3,5-diphenyl-1,3-oxazolidin-2-one
| Conditions | Yield |
|---|---|
| With potassium phosphate In N,N-dimethyl-formamide at 130℃; for 19h; | 99% |
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; hydrogen; C16H18BrCoINO2 In dibutyl ether at 160℃; under 45004.5 Torr; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Pressure; Temperature; Sealed tube; Autoclave; | 95% |
| With water; N,N'-dimethylimidazolium-2-carboxylate at 140℃; under 3000.3 Torr; for 24h; Autoclave; Sealed tube; | 90 %Chromat. |
| Conditions | Yield |
|---|---|
| In ethyl acetate at 40℃; for 4h; | 94.1% |
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