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Cas:4602-84-0
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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
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Product Name: FARNESOL Synonyms: 10-dodecatrien-1-ol,3,7,11-trimethyl-6;2,6,10-trimethyl-2,6,10-dodecatrien-12-ol[qr];3,7,11-trimethyl-2,6,10-dodecatrien-1-ol[qr];3,7,11-Trimethyl-2,6,10-dodec
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Cas:4602-84-0
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inquiryProduct name: Farnesol(CAS:4602-84-0) CAS No.:4602-84-0 Molecule Formula:C15H26O Molecule Weight:222.37 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTI
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Cas:4602-84-0
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Conditions | Yield |
---|---|
With N-chloro-succinimide In dichloromethane at 0 - 20℃; for 1.25h; | 98% |
methyl 3,7,11-trimethyldodeca-2,6,10-trienoate
farnesol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | 85% |
ethyl 3,7,11-trimethyldodeca-2,6,10-trienoate
farnesol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | 85% |
Conditions | Yield |
---|---|
With perchloric acid; acetone at 15 - 20℃; for 24.25h; Product distribution / selectivity; | A 15.3% B 21.3% C 57.3% |
With perchloric acid; trifluorormethanesulfonic acid; acetone In water at 15 - 20℃; for 8.16667h; Product distribution / selectivity; | A 1.8% B 52.7% C 16.2% |
With perchloric acid; methanesulfonic acid; acetone In water at 15 - 20℃; for 24.1667h; Product distribution / selectivity; | A 1.9% B 51.7% C 16.2% |
farnesal
farnesol
Conditions | Yield |
---|---|
With sodium amalgam; ethanol; acetic acid at 0℃; | |
With potassium phosphate; recombinant rat brain aldo-keto reductase R1B10; NADP In methanol Kinetics; Enzymatic reaction; | |
With rabbit 3-hydroxyhexobarbital dehydrogenase (AKR1C29); NADPH In aq. phosphate buffer; ethyl acetate at 37℃; for 0.5h; pH=7.4; Catalytic behavior; Kinetics; Enzymatic reaction; |
(+/-)-nerolidol
acetic anhydride
methylammonium carbonate
A
cis-α-farnesene
B
farnesol
Conditions | Yield |
---|---|
at 120 - 140℃; nachfolgendes Kochen des Reaktionsprodukts mit alkoh.Kalilauge im Wasserstoffstrom; dextrorotatory form of 2.6.10-trimethyl-dodecatrien-(2.6.11)-ol-(10); |
(+/-)-nerolidol
acetic anhydride
A
cis-α-farnesene
B
farnesol
Conditions | Yield |
---|---|
nachfolgendes Kochen des Reaktionsprodukts mit alkoh.Kalilauge im Wasserstoffstrom; inactive form of 2.6.10-trimethyl-dodecatrien-(2.6.11)-ol-(10); |
Conditions | Yield |
---|---|
at 120 - 140℃; nachfolgenden Kochen des Reaktionprodukts mit alkoh.Kalilauge im Wasserstoffstrom; |
Conditions | Yield |
---|---|
With sulfuric acid; copper (I) acetate; hydroquinone at 24℃; und folgendes Verseifen der erhaltenen Ester mit methylalkoh.KOH; |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) CH2Cl2, -78 deg C, 0.5 h, 2.) 190-195 deg C, 2 h; Yield given. Multistep reaction; |
farnesol
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid | |
With formic acid |
Conditions | Yield |
---|---|
at 120 - 140℃; nachfolgenden Kochen des Reaktionprodukts mit alkoh.Kalilauge im Wasserstoffstrom; |
farnesol
Conditions | Yield |
---|---|
With pyridine; phosphorus tribromide at -15℃; Schuetteln des erhaltenen Farnesylbromids mit Kaliumacetat in wasserfreiem Aceton und Verseifen des Farnesylacetats mit siedender methylalkoh.KOH; |
Conditions | Yield |
---|---|
at 0℃; |
(+/-)-nerolidol
sulfuric acid
acetic acid
A
cis-α-farnesene
B
farnesol
Conditions | Yield |
---|---|
inactive form of 2.6.10-trimethyl-dodecatrien-(2.6.11)-ol-(10); |
Conditions | Yield |
---|---|
inactive form of 2.6.10-trimethyl-dodecatrien-(2.6.11)-ol-(10); |
(E)-2-Methanesulfinyl-3,7,11-trimethyl-dodeca-6,10-dienoic acid ethyl ester
farnesol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 86 percent / calcium carbonate / toluene / 7 h / Heating 2: 85 percent / LiAl-hydride View Scheme |
(E)-3,7,11-Trimethyl-dodeca-6,10-dienoic acid methyl ester
farnesol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: 1. sodium methaperiodate 2. reflux, toluene, 20 h, CaCO3 3: 85 percent / LiAlH4 View Scheme |
farnesol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1. sodium methaperiodate 2. reflux, toluene, 20 h, CaCO3 2: 85 percent / LiAlH4 View Scheme |
3,7,11-trimethyl-6,10-dodecadien-1-yn-3-ol
farnesol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium; diethyl ether / 0 °C 2: 120 - 140 °C / nachfolgenden Kochen des Reaktionprodukts mit alkoh.Kalilauge im Wasserstoffstrom View Scheme |
Conditions | Yield |
---|---|
With perchloric acid; methanesulfonic acid In water; acetone at 10 - 15℃; for 24.5h; Product distribution / selectivity; | |
With phosphotungstic acid In acetone at 30℃; for 3h; Catalytic behavior; Solvent; Green chemistry; Overall yield = 55 %Chromat.; |
Conditions | Yield |
---|---|
With perchloric acid; methanesulfonic acid In water; acetone at 15 - 20℃; for 24.67h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With methanol; sodium hydroxide; water at 20 - 40℃; for 2.25h; Product distribution / selectivity; |
farnesyl benzoate
farnesol
Conditions | Yield |
---|---|
With methanol; potassium hydroxide at 20℃; Reflux; |
farnesyl pyrophosphate
farnesol
Conditions | Yield |
---|---|
With Mycobacterium tuberculosis N-terminal His-tagged Rv3376 enzyme; water Enzymatic reaction; |
farnesol
farnesal
Conditions | Yield |
---|---|
With dipyridinium dichromate In dichloromethane at 0 - 25℃; for 24h; | 100% |
With pyridinium chlorochromate In hexane at 25℃; for 2h; Oxidation; | 87% |
With 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; toluene-4-sulfonic acid In dichloromethane 1) 0 deg C, 1 h, 2) r.t., 1 h; | 86% |
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In tetrahydrofuran | 100% |
With toluene-4-sulfonic acid at 25℃; |
farnesol
Conditions | Yield |
---|---|
With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate In dichloromethane at -50℃; Molecular sieve; Inert atmosphere; enantioselective reaction; | 100% |
With bis(acetylacetonate)dioxotungsten(VI); C96H142N2O4; sodium chloride In dichloromethane at 20℃; for 3h; | 88% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
With potassium methanolate at 110 - 120℃; for 18.4333h; Inert atmosphere; | 99.3% |
Conditions | Yield |
---|---|
With platinum/carbon xerogel catalyst; hydrogen In ethanol at 20℃; for 12h; Inert atmosphere; | 99% |
With palladium on activated charcoal; hydrogen In ethyl acetate at 20℃; | 97% |
With hydrogen; palladium 10% on activated carbon In ethanol for 36h; | 93% |
Conditions | Yield |
---|---|
With N-chloro-succinimide; dimethylsulfide In dichloromethane at 0 - 20℃; for 2.5h; | 98% |
With N-chloro-succinimide; dimethylsulfide In dichloromethane at 0 - 20℃; for 2.83h; | 98% |
With N,N-dimethyl-formamide; phosphorus trichloride In tetrahydrofuran at 20℃; for 0.5h; |
farnesol
tert-butylchlorodiphenylsilane
(2E,6E)-1-((tert-butyldiphenylsilyl)oxy)-3,7,11-trimethyl-2,6,10-dodecatriene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; | 97% |
Conditions | Yield |
---|---|
Stage #1: farnesol With lithium hexamethyldisilazane at 0 - 20℃; Inert atmosphere; Stage #2: With methanol Inert atmosphere; | 97% |
With dodecacarbonyl-triangulo-triruthenium; 4,5-bis((diisopropylphosphanyl)methyl)acridine; ammonia In tert-Amyl alcohol at 170℃; for 21h; Temperature; Inert atmosphere; Schlenk technique; Autoclave; |
Conditions | Yield |
---|---|
With oxygen; copper In acetonitrile for 4h; Reagent/catalyst; Temperature; Reflux; | 95% |
With tert.-butylhydroperoxide; oxygen In decane; toluene at 80℃; under 750.075 Torr; | 87% |
Conditions | Yield |
---|---|
Stage #1: farnesol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Stage #2: p-methoxybenzyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃; | 92% |
farnesol
farnesyl bromide
Conditions | Yield |
---|---|
With phosphorus tribromide; triethylamine In toluene at -5℃; for 2h; Product distribution / selectivity; | 91% |
With methanesulfonyl chloride; triethylamine; lithium bromide In tetrahydrofuran at -45 - 0℃; for 1.91667h; Inert atmosphere; | 86% |
With pyridine; phosphorus tribromide at -5℃; |
Conditions | Yield |
---|---|
With benzotriazole*CrO3 In acetone for 5h; Heating; | 91% |
Multi-step reaction with 2 steps 1: Cr2O3-H2SO4 / das Edukt ist natuerlich vorkommendes Farnesol 2: AgNO3; aqueous alcoholic NaOH View Scheme | |
Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / -78 - 20 °C / Inert atmosphere 2: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / water; tert-butyl alcohol / 2 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 °C / Inert atmosphere 1.2: 1 h / 20 °C 2.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / water; tert-butyl alcohol / 2 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With {(η4-1,5-cyclooctadiene)Pd(η3-allyl)}BF4; N,N'-diethylurea; (2S)-methyl 2-(4,8-di-tert-butyl-2,10-dimethoxydibenzo[d,f][1,3,2]dioxaphosphepin-6-ylamino)benzylethanoate In toluene at 80℃; for 20h; regioselective reaction; | 90% |
With {(η4-1,5-cyclooctadiene)Pd(η3-allyl)}BF4; N,N'-diethylurea; (2S)-methyl 2-(4,8-di-tert-butyl-2,10-dimethoxydibenzo[d,f][1,3,2]dioxaphosphepin-6-ylamino)benzylethanoate In toluene at 80℃; for 20h; regioselective reaction; | 57% |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 3h; | 90% |
Stage #1: farnesol With manganese(II) iodide; naphthalene; lithium In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Stage #2: benzoyl chloride In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With triphenylphosphine; trifluoroacetic acid; palladium dichloride In toluene at 120℃; under 30003 Torr; for 24h; Inert atmosphere; Autoclave; | 88% |
farnesol
10-(2,3-Dimethoxy-5-methyl-1,4-benzoquinon-6-yl)decanoic acid
farnesyl idebenone carboxylate
Conditions | Yield |
---|---|
novozyme 435 at 50℃; Product distribution / selectivity; Enzymatic reaction; Inert atmosphere; | 87% |
farnesol
Conditions | Yield |
---|---|
In toluene at 50℃; for 1.5h; | 87% |
Conditions | Yield |
---|---|
With pyridine; trichloroacetonitrile at 80℃; for 0.25h; Microwave irradiation; | 86% |
farnesol
Conditions | Yield |
---|---|
Stage #1: farnesol; triethylammonium (2S,3R,4S,5S,6S)-3,4,5-tris-(acetyloxy)-6-(methoxycarbonyl)oxan-2-yl phosphonate With pyridine; pivaloyl chloride at -15℃; for 1.5h; Stage #2: With iodine at 20℃; for 1h; | 83% |
farnesol
ethylene glycol
2-methyl-2-((4R,8R)-4,8,12-trimethyltridecyl)-1,3-dioxolane
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In benzene at 90℃; for 8h; Inert atmosphere; Dean-Stark; | 82.6% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 95℃; under 450.045 - 525.053 Torr; for 6h; | 81% |
With potassium carbonate In N,N-dimethyl-formamide at 95℃; for 4h; | 81% |
Conditions | Yield |
---|---|
With perchloric acid | 80% |
farnesol
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate
C29H44O10
Conditions | Yield |
---|---|
With gold(I) chloride In dichloromethane at 20℃; for 2h; Inert atmosphere; stereoselective reaction; | 80% |
farnesol
Conditions | Yield |
---|---|
Stage #1: farnesol With dihydrogen peroxide; bis(2,4-pentanedionato)dioxomolybdenum(VI) In acetonitrile at 20 - 50℃; Stage #2: With diphenyl sulfide regioselective reaction; | 79% |
farnesol
(2Z,6E)-10-Chloro-3,7,11-trimethyl-dodeca-2,6,11-trien-1-ol
Conditions | Yield |
---|---|
With hypochloric acid In dichloromethane | 78% |
Conditions | Yield |
---|---|
Stage #1: farnesol With manganese(II) iodide; naphthalene; lithium In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Stage #2: acetic anhydride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 77% |
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