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(1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol cas 46032-98-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry46032-98-8 C9H13NO2 (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediolAppearance:white powder Storage:Normal temperature Package:Woven bag Application:Amino Alcohols (Chiral);Asymmetric Synthesis;Chiral Building Blocks;Synthetic Organ
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inquirysyn-(2R,3R)-[2-azido-3-hydroxy-3-phenyl-1-propanol]
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760 Torr; for 12h; | 99% |
(2S,3R)-2-Azido-3-nitrosooxy-3-phenyl-propionic acid methyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760 Torr; for 12h; | 97% |
(+/-)-threo-2-amino-1-phenyl-1,3-propanediol
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With L-Tartaric acid | |
With L-(-)-O,O'-dibenzoyltartaric acid | |
With (1S)-(+)-3-bromocamphor-10-sulfonic acid | |
With D-Glutamic acid |
(2S,3R)-2-amino-3-hydroxy-3-phenyl-propionic acid cyclohexyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
1-Phenyl-2-acetamido-1,3-propandiol
A
(1S,2S)-2-amino-1-phenyl-1,3-diol
B
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
C
(1R,2S)-(+)-2-amino-1-phenyl-1,3-propanediol
D
(1S,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
hydrolysis; |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 4h; Heating; |
(1R,2R)-2-amino-(N-benzyloxycarbonyl)-1-phenylpropane-1,3-diol
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With hydrogen |
A
(1S,2S)-2-amino-1-phenyl-1,3-diol
B
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With (1S)-(+)-3-bromocamphor-10-sulfonic acid; ethyl acetate |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With (1S)-(+)-3-bromocamphor-10-sulfonic acid; ethyl acetate |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With 1,4-dioxane; sodium tetrahydroborate und Erwaermen des Reaktionsprodukts mit wss.HCl; |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With diethyl ether; nitric acid; acetic acid |
anti-(4S,2'S,3'S)-3-(3'-Hydroxy-3'-phenyl-2'-bromo-1'-oxopropyl)-4-(1-methylethyl)-2-oxazolidinone
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 89 percent / NaN3 / dimethylformamide / 6 h / 25 °C 2: 90 percent / LiBH4 / tetrahydrofuran; methanol / 1 h / 0 °C 3: 99 percent / H2 / Pd/C / methanol / 12 h / 20 °C / 760 Torr View Scheme |
(4S)-4-isopropyl-3-[(2E)-3-phenylprop-2-enoyl]-1,3-oxazolidin-2-one
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Ag2O; Br2 / acetone / -10 °C 2: 89 percent / NaN3 / dimethylformamide / 6 h / 25 °C 3: 90 percent / LiBH4 / tetrahydrofuran; methanol / 1 h / 0 °C 4: 99 percent / H2 / Pd/C / methanol / 12 h / 20 °C / 760 Torr View Scheme |
syn-(4S,2'S,3'R)-3-(2'-azido-3'-hydroxy-3'-phenyl-propionyl)-4-(1-methylethyl)-2-oxazolidinone
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / LiBH4 / tetrahydrofuran; methanol / 1 h / 0 °C 2: 99 percent / H2 / Pd/C / methanol / 12 h / 20 °C / 760 Torr View Scheme |
methyl (2R,3S)-3-phenylglycidate
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 89 percent / NaNO2; AcOH / H2O / 2 h / 0 - 20 °C 2: 82 percent / diphenyl phosphoryl azide; DEAD; PPh3 / tetrahydrofuran / 12 h / 0 - 20 °C 3: 97 percent / H2 / Pd/C / methanol / 12 h / 20 °C / 760 Torr View Scheme |
(2R,3R)-2-Hydroxy-3-nitrosooxy-3-phenyl-propionic acid methyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 82 percent / diphenyl phosphoryl azide; DEAD; PPh3 / tetrahydrofuran / 12 h / 0 - 20 °C 2: 97 percent / H2 / Pd/C / methanol / 12 h / 20 °C / 760 Torr View Scheme |
methyl (4S,5R)-5-phenyl-4,5-dihydro-1,3-oxazole-4-carboxylate
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: conc. HCl / methanol / 3 h / 50 °C 2: LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: chiral ferrocenylphosphine-gold(I) complex / CH2Cl2 / 20 h / 25 °C 2: conc. HCl / methanol / 3 h / 50 °C 3: LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: HCl 2: (S)-5-oxo-pyrrolidine-2-carboxylic acid 3: LiAlH4; diethyl ether View Scheme |
(2RS,3SR)-2-amino-3-hydroxy-3-phenyl-propionic acid cyclohexyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (S)-5-oxo-pyrrolidine-2-carboxylic acid 2: LiAlH4; diethyl ether View Scheme |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
acetic anhydride
(1R,2R)-2-acetamido-1-phenylpropane-1,3-diyl diacetate
Conditions | Yield |
---|---|
With pyridine; dmap | 100% |
With pyridine |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
benzyl chloroformate
(1R,2R)-2-amino-(N-benzyloxycarbonyl)-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 30℃; for 2h; | 99% |
di-tert-butyl dicarbonate
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
acetone
tert-butyl (4R,5R)-4-(hydroxymethyl)-2,2-dimethyl-5-phenyl-1,3-oxazolidine-3-carboxylate
Conditions | Yield |
---|---|
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; acetone In toluene for 5h; Reflux; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; for 5h; | 98% |
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; acetone In toluene Reflux; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; | 91% |
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; acetone In toluene for 22h; Dean-Stark; Reflux; Stage #2: di-tert-butyl dicarbonate In toluene at 20℃; | 78.5% |
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; acetone In dichloromethane at 50℃; Stage #2: di-tert-butyl dicarbonate at 50℃; |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
benzyl bromide
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile Heating; | 96% |
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile Heating; | 96% |
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile Heating; | |
With potassium carbonate In acetonitrile for 8h; Heating; |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
benzoyl chloride
benzoic acid (2R,3R)-2-benzoylamino-3-hydroxy-3-phenylpropyl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 24h; | 96% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
cholic acid N-succinimidyl ester
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25℃; for 1.5h; | 92% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
3α,12α-dihydroxy-5β-cholan-24-oic acid 2,5-dioxopyrrolidin-1-yl ester
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25℃; for 1.5h; | 88% |
N-Boc-L-methionine sulfone
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(1R,2R)-1-phenyl-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 24h; | 81% |
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 79% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 79% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
acetylacetone
Conditions | Yield |
---|---|
With niobium oxide phosphate In neat (no solvent) at 50℃; for 0.5h; | 78% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
ethylene dibromide
Conditions | Yield |
---|---|
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; ethylene dibromide at 100℃; for 10h; Stage #2: With sodium hydroxide In water | 75% |
but-3-enoic acid
carbon monoxide
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
A
(2R,3R,8aS)-3-(hydroxymethyl)-2-phenylhexahydrooxazolo[3,2-a]pyridin-5-one
Conditions | Yield |
---|---|
With acetylacetonatodicarbonylrhodium(l); hydrogen; pyridinium p-toluenesulfonate; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin) In tetrahydrofuran at 75℃; under 5168.02 Torr; for 1.5h; Inert atmosphere; Microwave irradiation; optical yield given as %de; regioselective reaction; | A 70% B n/a |
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 70% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 70% |
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 65% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 65% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h; | 62% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h; | 62% |
Ethyl 2-hydroxybenzimidate
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
In chlorobenzene at 80 - 110℃; for 25h; | 61% |
2-Iodobenzoyl chloride
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(R,R)-[2-(2-iodophenyl)-4,5-dihydrooxazol-4-yl]phenylmethanol
Conditions | Yield |
---|---|
Stage #1: 2-Iodobenzoyl chloride; (1R,2R)-2-amino-1-phenylpropane-1,3-diol With triethylamine In dichloromethane at 0℃; for 0.5h; Stage #2: With dmap; p-toluenesulfonyl chloride In dichloromethane for 16h; Heating; | 59% |
2-(2-chlorophenyl)-2-(6,7-dihydrothieno[3,2-c]pyridine-5(4H)-yl)acetic acid
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(S)-(+)-α-(2-chlorophenyl)-6,7-dihydro-4H-thieno[3,2-c]pyridine-5-acetic acid, (1R,2R)-(-)-2-amino-1-phenyl-1,3-propanediol salt
Conditions | Yield |
---|---|
In isopropyl alcohol at 5℃; for 2h; Heating / reflux; | 57% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol; 3,3'-bis(3-bromopropoxy)-2,2'-dimethyl-1,1'-biphenyl With N-ethyl-N,N-diisopropylamine In methanol at 65℃; for 24h; Inert atmosphere; Stage #2: (S)-3-amino-1,2-dihydroxypropane hydrochloride With N-ethyl-N,N-diisopropylamine In methanol at 65℃; Inert atmosphere; | A 54% B 17% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions | Yield |
---|---|
In chlorobenzene at 80 - 110℃; for 25h; | 52% |
2-iodobenzonitrile
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
[(R,R)-2-(2-iodophenyl)-5-phenyl-4,5-dihydrooxazol-4-yl]methanol
Conditions | Yield |
---|---|
With cadmium(II) acetate In chlorobenzene for 16h; Heating; | 40% |
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
methyl iodide
(1R,2R)-2-amino-3-methoxy-1-phenylpropan-1-ol
Conditions | Yield |
---|---|
Stage #1: (1R,2R)-2-amino-1-phenylpropane-1,3-diol With potassium hydride In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 11% |
formaldehyd
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(7aR)-1c-phenyl-(7ar)-dihydro-oxazolo[3,4-c]oxazole
Conditions | Yield |
---|---|
With benzene |
heptanal
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(7aR)-3ξ,5ξ-dihexyl-1c-phenyl-(7ar)-dihydro-oxazolo[3,4-c]oxazole
Conditions | Yield |
---|---|
With benzene |
dichloroacetic acid methyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(1R,2R)-2-(2,2-dichloro-acetylamino)-1-phenyl-propane-1,3-diol
Conditions | Yield |
---|---|
With methanol |
dichloroacetyl-phosphorous acid diethyl ester
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
(1R,2R)-2-(2,2-dichloro-acetylamino)-1-phenyl-propane-1,3-diol
Conditions | Yield |
---|---|
With ethanol; triisoamylamine |
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