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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,1-Diethoxypropane

Cas:4744-08-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 4744-08-5 with best quality

Cas:4744-08-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

PROPIONALDEHYDE DIETHYL ACETAL CAS:4744-08-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org

PROPIONALDEHYDE DIETHYL ACETAL CAS:4744-08-5

Cas:4744-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Boiling point 122.8 °C(lit.) density 0.815 g/mL at 25 °C

Propionaldehyde Diethyl Acetal

Cas:4744-08-5

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Propionaldehyde Diethyl acetal

Cas:4744-08-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

4744-08-5

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Prpional Diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Other

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DB BIOTECH CO., LTD

best seller Application:API

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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Hangzhou Fandachem Co.,Ltd

Propionaldehyde diethyl acetal cas 4744-08-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Propionaldehyde diethyl acetal cas 4744-08-5

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

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SAGECHEM LIMITED

4744-08-5 Application:intermediate

Propane, 1,1-diethoxy-

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,1-Diethoxypropane

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Other

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

4744-08-5

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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Hebei Muhuang Technology Co., Ltd

best seller Application:API

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

1,1-diethoxypropane

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Yuanye Bio-Technology Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica

1,1-Diethoxypropane manufacturer

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Propionaldehyde diethyl acetal

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

Propionaldehyde Diethyl acetal

Cas:4744-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

Propionaldehyde Diethyl Acetal CAS NO.4744-08-5

Cas:4744-08-5

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

Triethyl orthopropionate
115-80-0

Triethyl orthopropionate

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In n-heptane at 100℃; under 67506.8 Torr; Temperature;98.6%
triethylaluminum
97-93-8

triethylaluminum

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
In dichloromethane at -20 - 20℃;98%
In hexane at 35 - 40℃;78%
ethanol
64-17-5

ethanol

1-bromopropylamine

1-bromopropylamine

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With copper(l) chloride In cyclohexane at 45 - 65℃; for 12h; Temperature;91%
propionaldehyde
123-38-6

propionaldehyde

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With ammonium nitrate In ethanol at 20 - 36℃;81.6%
Stage #1: propionaldehyde; orthoformic acid triethyl ester With ammonium nitrate; ethanol at 20 - 36℃;
Stage #2: With sodium carbonate In water at 20℃; pH=7.5;
81.6%
With sulfuric acid
3,3-diethoxypropyl lithium

3,3-diethoxypropyl lithium

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With water In tetrahydrofuran at -78 - 20℃; for 2h;80%
With water In tetrahydrofuran at -78 - 20℃; for 2h; Product distribution; also other electrophiles (D2O, (PhCH2)2S2, n-C3H7CHO, PhCHO, n-C7H15CHO, PhCH=NPh);80%
ethanol
64-17-5

ethanol

propionaldehyde
123-38-6

propionaldehyde

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With calcium chloride at 25 - 35℃; for 10h; Temperature;78.8%
With hydrogenchloride
With hydrogenchloride at 25℃; Gleichgewicht der Reaktion;
Triethyl orthopropionate
115-80-0

Triethyl orthopropionate

A

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

B

ethylpropylether
628-32-0

ethylpropylether

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In n-heptane at 150℃; under 67506.8 Torr; Temperature;A 63%
B 36.9%
diethoxymethyl acetate
14036-06-7

diethoxymethyl acetate

diethylaluminium chloride
96-10-6

diethylaluminium chloride

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
In diethyl ether at 20℃; for 4h;53%
(E)-1-ethoxyprop-1-ene
4696-26-8

(E)-1-ethoxyprop-1-ene

A

(Z)-1-ethoxyprop-1-ene
4696-25-7

(Z)-1-ethoxyprop-1-ene

B

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

C

propionaldehyde
123-38-6

propionaldehyde

Conditions
ConditionsYield
(sulphos)Rh(CO)2 In 1,2-dichloro-ethane at 100℃; for 1h;A 22%
B 31%
C 14%
ethanol
64-17-5

ethanol

ethyl 1-propenyl ether
928-55-2

ethyl 1-propenyl ether

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With Fuller's Earth
tetraethoxy orthosilicate
78-10-4

tetraethoxy orthosilicate

propionaldehyde
123-38-6

propionaldehyde

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With ethanol; phosphoric acid
ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With diethyl ether Hydrolyse mit verduennter Essigsaeure und sofortige Neutralisation;
(E)-3-Ureido-but-2-enoic acid ethyl ester
5435-44-9, 22243-66-9

(E)-3-Ureido-but-2-enoic acid ethyl ester

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

acetylene
74-86-2

acetylene

A

malondialdehyde bis(diethyl acetal)
122-31-6

malondialdehyde bis(diethyl acetal)

B

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

C

1,1,4,4-tetraethoxy-2-butyne
3975-08-4

1,1,4,4-tetraethoxy-2-butyne

Conditions
ConditionsYield
under 8826.09 - 12503.6 Torr;
at 170℃; under 8826.09 - 12503.6 Torr;
carbon monoxide
201230-82-2

carbon monoxide

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With hydrogen; dicobalt octacarbonyl
n-propylmagnesium bromide
927-77-5

n-propylmagnesium bromide

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
In diethyl ether
3-chloro-1,1-diethoxy-propane
35573-93-4

3-chloro-1,1-diethoxy-propane

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With water; naphthalen-1-yl-lithium 1.) THF, -78 deg C, 6 h, 2.) 20 deg C, 2 h; Yield given. Multistep reaction;
Multi-step reaction with 2 steps
1: lithium naphthalenide / tetrahydrofuran / 6 h / -78 °C
2: 80 percent / H2O / tetrahydrofuran / 2 h / -78 - 20 °C / also other electrophiles (D2O, (PhCH2)2S2, n-C3H7CHO, PhCHO, n-C7H15CHO, PhCH=NPh)
View Scheme
sulfuric acid
7664-93-9

sulfuric acid

propionaldehyde
123-38-6

propionaldehyde

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
analoge Reaktion mit Orthoameisensaeure-tripropylester;
2-bromo-3,3-diethoxypropene
17592-40-4

2-bromo-3,3-diethoxypropene

alcoholic KOH-solution

alcoholic KOH-solution

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

sunlight

sunlight

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 66 percent / formic acid / 24 h
2: 53 percent / diethyl ether / 4 h / 20 °C
View Scheme
ethanol
64-17-5

ethanol

carbon monoxide
201230-82-2

carbon monoxide

allyl alcohol
107-18-6

allyl alcohol

A

2-ethoxytetrahydrofuran
13436-46-9

2-ethoxytetrahydrofuran

B

propan-1-ol
71-23-8

propan-1-ol

C

Butane-1,4-diol
110-63-4

Butane-1,4-diol

D

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With hydrogen; acetylacetonatodicarbonylrhodium(l) at 125℃; under 30003 Torr; for 2.5h; Product distribution; Further Variations:; reagent ratios;
acrylaldehyde diethyl acetal
3054-95-3

acrylaldehyde diethyl acetal

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Conditions
ConditionsYield
With borane-ammonia complex; cobalt(II)(2,6-bis(morpholinomethyl)pyridine)bromide In methanol at 80℃; for 14h;99 %Chromat.
ethanol
64-17-5

ethanol

A

diethyl ether
60-29-7

diethyl ether

B

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

C

ethyl vinyl ether
109-92-2

ethyl vinyl ether

Conditions
ConditionsYield
at 280℃; for 4h; Reagent/catalyst; Autoclave; Inert atmosphere;
4-iodopyridine-2-carboxylic acid methyl ester
380381-28-2

4-iodopyridine-2-carboxylic acid methyl ester

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

4-(3,3-Diethoxy-prop-1-ynyl)-pyridine-2-carboxylic acid methyl ester
663614-43-5

4-(3,3-Diethoxy-prop-1-ynyl)-pyridine-2-carboxylic acid methyl ester

Conditions
ConditionsYield
With triethylamine; palladium diacetate; copper(l) iodide; triphenylphosphine at 20℃; for 3h;100%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene
251475-02-2

3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

4-ethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-hexene

4-ethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-hexene

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at -78℃; for 3h;99%
With titanium tetrachloride In dichloromethane TiCl4, CH2Cl2, -78°C, 3 h;99%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

(4R)-4-ethyl-1,3-oxazolidin-2-one
98974-04-0

(4R)-4-ethyl-1,3-oxazolidin-2-one

(R)-3-(1-ethoxypropyl)-4-ethyl-1,3-oxazolidin-2-one
925427-50-5

(R)-3-(1-ethoxypropyl)-4-ethyl-1,3-oxazolidin-2-one

Conditions
ConditionsYield
With 10-camphorsufonic acid In dichloromethane at 55℃;97%
5-iodo-1,2,3-trimethoxybenzene
25245-29-8

5-iodo-1,2,3-trimethoxybenzene

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

1,1-diethoxy-3-(3,4,5-trimethoxyphenyl)-2-propyne

1,1-diethoxy-3-(3,4,5-trimethoxyphenyl)-2-propyne

Conditions
ConditionsYield
With copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride In triethylamine at 20℃; for 3h;97%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene
252062-23-0

3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

(E)-1-cyclohexyl-4-ethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-hexene

(E)-1-cyclohexyl-4-ethoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-hexene

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at -78℃; for 3h;95%
With titanium tetrachloride In dichloromethane TiCl4, CH2Cl2, -78°C, 3 h;95%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene
252062-22-9

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene

(E)-6-ethoxy-1-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxacarborolan-2-yl)-3-octene

(E)-6-ethoxy-1-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxacarborolan-2-yl)-3-octene

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at -78℃; for 3h;94%
With titanium tetrachloride In dichloromethane TiCl4, -78°C, CH2Cl2, 3 h;94%
With aluminium trichloride In dichloromethane AlCl3, CH2Cl2, -78°C, 0.5 h; -20°C for 2.5 h;82%
With trimethylsilyl trifluoromethanesulfonate In dichloromethane TMSOTf, CH2Cl2, -78°C, 0.5 h; -20°C for 2.5 h;30%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

acetophenone
98-86-2

acetophenone

3-ethoxy-1-phenyl-pentan-1-one

3-ethoxy-1-phenyl-pentan-1-one

Conditions
ConditionsYield
Stage #1: acetophenone With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine In dichloromethane at -78℃; for 0.5h;
Stage #2: 1,1-diethoxypropane In dichloromethane at -78℃; for 0.5h;
90%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

7-chloro-4,6-dimethoxy-2,3-dihydrobenzofuran-3-one
3261-06-1

7-chloro-4,6-dimethoxy-2,3-dihydrobenzofuran-3-one

(Z)-7-chloro-4,6-dimethoxy-2-(1-propylidene)-3(2H)-benzofuranone
129529-56-2

(Z)-7-chloro-4,6-dimethoxy-2-(1-propylidene)-3(2H)-benzofuranone

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane for 24h; Ambient temperature;89%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

1,3-diphenylpropanedione
120-46-7

1,3-diphenylpropanedione

2-(1-Ethoxy-propyl)-1,3-diphenyl-propane-1,3-dione
116863-89-9

2-(1-Ethoxy-propyl)-1,3-diphenyl-propane-1,3-dione

Conditions
ConditionsYield
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃;89%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

(Z)-1-Phenyl-6-trimethylsilanyl-hex-4-en-1-ol
164076-17-9

(Z)-1-Phenyl-6-trimethylsilanyl-hex-4-en-1-ol

(2S,3S,6S)-2-Ethyl-6-phenyl-3-vinyl-tetrahydro-pyran

(2S,3S,6S)-2-Ethyl-6-phenyl-3-vinyl-tetrahydro-pyran

Conditions
ConditionsYield
With toluene-4-sulfonic acid for 24h; Product distribution; Ambient temperature; reactions of derivatives with var. acetals;84%
With toluene-4-sulfonic acid for 24h; Ambient temperature;84%
acetamide
60-35-5

acetamide

1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

N,N'-(propane-1,1-diyl)diacetamide
7073-48-5

N,N'-(propane-1,1-diyl)diacetamide

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In dichloromethane for 0.25h; Heating;83%
With sulfuric acid
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

3,3-diethoxy-2-methyl-propionaldehyde
22634-86-2

3,3-diethoxy-2-methyl-propionaldehyde

Conditions
ConditionsYield
With trichlorophosphate at 70℃; for 2h; Vilsmeier reaction;83%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

ethyl vinyl ether
109-92-2

ethyl vinyl ether

1,1,3-triethoxypentane
39595-61-4

1,1,3-triethoxypentane

Conditions
ConditionsYield
Montmorillonite clay K-10 at 10 - 15℃;80%
NdNaY at 0 - 25℃; for 0.5h;61%
With iron(III) chloride
With iron(III) chloride
With boron trifluoride diethyl etherate at 65℃;
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

ethyl 1-propenyl ether
928-55-2

ethyl 1-propenyl ether

Conditions
ConditionsYield
2-ethyl-N-(2-ethylhexyl)-1-hexanamine; toluene-4-sulfonic acid77.5%
With quinoline; phosphorus pentoxide distillation at a bath temp. 150 deg C;75%
With quinoline; phosphorus pentoxide vermutlich entsteht als Gemisch von cis- und trans-Form;
With sodium hydrogen sulfate vermutlich entsteht als Gemisch von cis- und trans-Form;
With silver-asbestos at 280℃; vermutlich entsteht als Gemisch von cis- und trans-Form;
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

(Z)-1-ethoxyprop-1-ene
4696-25-7

(Z)-1-ethoxyprop-1-ene

Conditions
ConditionsYield
With 2-ethyl-N-(2-ethylhexyl)-1-hexanamine; toluene-4-sulfonic acid at 160℃; Distillation;77.5%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

propionaldehyde
123-38-6

propionaldehyde

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene
252062-22-9

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene

(2R*,4S*,4aR*,10bS*)-2,4-diethyl-1,4,4a,5,6,10b-hexahydro-10b-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-naphtho[2,1-c]pyran

(2R*,4S*,4aR*,10bS*)-2,4-diethyl-1,4,4a,5,6,10b-hexahydro-10b-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-naphtho[2,1-c]pyran

Conditions
ConditionsYield
Stage #1: propionaldehyde; 3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene With titanium tetrachloride In dichloromethane at -78℃; for 2h;
Stage #2: 1,1-diethoxypropane In dichloromethane at 0℃; for 3h;
75%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

propionaldehyde
123-38-6

propionaldehyde

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene
252062-22-9

3-(dimethylphenylsilyl)-5-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-pentene

C6H4(CH2)2CHCH(C2H5)OCH(C2H5)CH2CBO2C2(CH3)4
347868-66-0

C6H4(CH2)2CHCH(C2H5)OCH(C2H5)CH2CBO2C2(CH3)4

Conditions
ConditionsYield
With titanium tetrachloride; sodium hydrogencarbonate In dichloromethane B salt mixed with TiCl4 at -78°C, stirred at -78°C for 2 h, treated with aldehydes at -78°C, stirred at 0°C for 3 h,treated with aq.NaHCO3; extd.(AcOC2H5), chromy.(silica gel);75%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

1,1'-oxybisethene
109-93-3

1,1'-oxybisethene

1,1,3,5-tetraethoxyheptane

1,1,3,5-tetraethoxyheptane

Conditions
ConditionsYield
at 0 - 50℃; for 2.5h; Time;75%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

P,P-diphenylphosphinothioic amide
17366-80-2

P,P-diphenylphosphinothioic amide

C18H20NPS
1138700-42-1

C18H20NPS

Conditions
ConditionsYield
at 120 - 160℃;73%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

di-tert-butyl 1-(6-methoxypyridin-3-yl)hydrazine-1,2-dicarboxylate
1338466-39-9

di-tert-butyl 1-(6-methoxypyridin-3-yl)hydrazine-1,2-dicarboxylate

3-methylpyrrolo<3,2-b>pyridinee
138469-76-8

3-methylpyrrolo<3,2-b>pyridinee

Conditions
ConditionsYield
Stage #1: 1,1-diethoxypropane; di-tert-butyl 1-(6-methoxypyridin-3-yl)hydrazine-1,2-dicarboxylate With sulfuric acid In water for 1h; Reflux; Inert atmosphere;
Stage #2: With sodium carbonate In water Saturated solution; Inert atmosphere;
72%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

diethyl ether-acetonitrile
87271-68-9

diethyl ether-acetonitrile

Conditions
ConditionsYield
zinc(II) iodide at 25℃; for 3h;71%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

Phenoxymagnesium bromide
35770-74-2

Phenoxymagnesium bromide

1,1-bis(2-hydroxyphenyl)propane
34240-91-0

1,1-bis(2-hydroxyphenyl)propane

Conditions
ConditionsYield
In benzene for 24h; Heating;70%
1,1-diethoxypropane
4744-08-5

1,1-diethoxypropane

benzamide
55-21-0

benzamide

N-(n-propyl)benzamide
10546-70-0

N-(n-propyl)benzamide

Conditions
ConditionsYield
With triethylsilane; trifluoroacetic acid In acetonitrile at 22℃; for 18h;65%

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