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Product Name: 2-Isopropoxyphenol Synonyms: 2-ISOPROPOXYPHENOL;2-(1-methylethoxy)phenol;2-(1-methylethoxy)-pheno;Phenol, 2-(1-methylethoxy)-;Phenol, 2-isopropoxy;propoxurphenol;o-Isopropoxyphenol;1-Hydroxy-2-isopropoxybenzene
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2,2-dimethyl-1,3-benzodioxole
2-Isopropoxyphenol
Conditions | Yield |
---|---|
With aluminium trichloride; sulfuric acid | 88% |
With sulfuric acid; diisobutylaluminium hydride In methanol; water; toluene | 72% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 24h; Williamson synthesis; Reflux; | 88% |
With potassium hydroxide In dimethyl sulfoxide for 0.5h; | 53% |
With potassium hydroxide In dimethyl sulfoxide at 18℃; for 2h; |
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 21h; Ambient temperature; | 78.5% |
Conditions | Yield |
---|---|
With sodium In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 2h; | 78% |
With sodium In N,N,N,N,N,N-hexamethylphosphoric triamide at 100℃; for 2h; Mechanism; | 78% |
With ammonia; sodium |
benzene-1,2-diol
isopropyl bromide
A
2-Isopropoxyphenol
B
Brenzcatechindi-isopropylether
Conditions | Yield |
---|---|
With sodium In methanol for 3h; Condensation; Heating; | A 63% B 16% |
2-Isopropoxyphenol
Conditions | Yield |
---|---|
With sodium persulfate; oxygen In acetonitrile at 55℃; for 9h; | 56% |
Conditions | Yield |
---|---|
With sodium di(ethyl)amine In N,N,N,N,N,N-hexamethylphosphoric triamide; benzene for 12h; Product distribution; Heating; other metal amide, other reagent-substrate ratio; | A 48% B 30% |
With sodium di(ethyl)amine In N,N,N,N,N,N-hexamethylphosphoric triamide; benzene for 12h; Heating; | A 48% B 30% |
Conditions | Yield |
---|---|
With borate buffer; cetyltrimethylammonim bromide In water at 100℃; for 0.00833333h; pH=9.0; Product distribution; Further Variations:; Temperatures; Decomposition; |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; for 0.0833333h; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / K2CO3 / dimethylformamide / 48 h / Ambient temperature 2: 6.30 g / selenium dioxide, H2O2 / CH2Cl2 / 72 h / Ambient temperature 3: 78.5 percent / KOH / methanol / 21 h / Ambient temperature View Scheme |
2-isopropoxybenzaldehyde
2-Isopropoxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 6.30 g / selenium dioxide, H2O2 / CH2Cl2 / 72 h / Ambient temperature 2: 78.5 percent / KOH / methanol / 21 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / Na / hexamethylphosphoric acid triamide / 100 °C 2: 78 percent / Na / hexamethylphosphoric acid triamide / 2 h / 100 °C View Scheme |
Conditions | Yield |
---|---|
With trifluoroacetic acid |
2,2-dimethyl-1,3-benzodioxole
2-Isopropoxyphenol
Conditions | Yield |
---|---|
With aluminium trichloride In toluene |
2,2-dimethyl-1,3-benzodioxole
2-Isopropoxyphenol
Conditions | Yield |
---|---|
With aluminium trichloride; sulfuric acid In methanol; water; toluene |
2-Isopropoxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium; iodine / tetrahydrofuran / 0.25 h / Inert atmosphere 2: sodium persulfate; oxygen / acetonitrile / 9 h / 55 °C View Scheme |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 12h; | 100% |
Conditions | Yield |
---|---|
With N,N'-dimethylbenzylamine at 60 - 90℃; for 3h; Reagent/catalyst; Temperature; | 99% |
In Dimethyldisulphide at 20℃; for 1h; |
Conditions | Yield |
---|---|
With palladium diacetate; triphenylphosphine; benzoic acid In tetrahydrofuran at -40 - 80℃; under 15001.5 Torr; Autoclave; Inert atmosphere; | 99% |
2-Isopropoxyphenol
propargyl bromide
1-Isopropoxy-2-prop-2-ynyloxy-benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 2.5h; | 97% |
2-Isopropoxyphenol
5-iodo-2-isopropoxyphenol
Conditions | Yield |
---|---|
Stage #1: 2-Isopropoxyphenol With potassium iodide; sodium hydroxide In methanol at 20℃; Stage #2: With sodium hypochlorite In methanol | 96% |
2-Isopropoxyphenol
4-bromo-2-isopropoxy-phenol
Conditions | Yield |
---|---|
With pyridinium hydrobromide perbromide In dichloromethane at 20℃; for 6h; | 94% |
With bromine In dichloromethane at -70 - -10℃; for 1h; | 94% |
With bromine In dichloromethane; water at -70 - -10℃; for 4h; |
Conditions | Yield |
---|---|
With aluminium(III) iodide; diisopropyl-carbodiimide In acetonitrile at 80℃; for 18h; | 94% |
With aluminium(III) iodide; diisopropyl-carbodiimide In acetonitrile at 80℃; for 18h; | 94% |
With aluminium(III) iodide; calcium oxide In acetonitrile at 80℃; for 18h; | 94% |
2-Isopropoxyphenol
4-(4-chlorophenyl)-5-(3-hydroxypropyl)-2-(2-methylimidazol-1-yl)oxazole
Conditions | Yield |
---|---|
With tributylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 20℃; Mitsunobu reaction; | 93% |
2-Isopropoxyphenol
5-chloro-6-(thiophen-2-yl)pyrazine-2,3-dicarbonitrile
5-(2-isopropyloxyphenoxy)-6-(thiophen-2-yl)pyrazine-2,3-dicarbonitrile
Conditions | Yield |
---|---|
With triethylamine In acetone at 20℃; for 2h; | 89% |
Conditions | Yield |
---|---|
88% |
2-(3-bromopropyl)isoindole-1,3-dione
2-Isopropoxyphenol
2-[3-(2-isopropoxy-phenoxy)-propyl]-isoindole-1,3-dione
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 25 - 80℃; for 18.25h; | 87% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 18h; | 87% |
2-Isopropoxyphenol
5-chloropyrazine-2,3-dicarbonitrile
5-(2-isopropyloxyphenoxy)pyrazine-2,3-dicarbonitrile
Conditions | Yield |
---|---|
With triethylamine In acetone at 20℃; for 2h; | 86% |
2-Isopropoxyphenol
2-hydroxy-3-isopropoxyphenyl bromide
Conditions | Yield |
---|---|
With bromine; tert-butylamine In dichloromethane; toluene at -78 - 20℃; for 5h; | 85% |
With bromine; tert-butylamine In dichloromethane; toluene at -60 - 20℃; for 0.5h; | 39% |
With bromine; tert-butylamine In toluene at -78 - 18℃; for 14h; |
diethyl ether
ethyl-magnesium tetrahydroborate
2-Isopropoxyphenol
2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2)
Conditions | Yield |
---|---|
In diethyl ether byproducts: C2H6; all manipulations under anhydrous conditions and under N2 atm.; soln. oforg. compd. added dropwise to stirred soln. of Mg compd.; filtered, washed with Et2O, dried in vac.; elem. anal.; | 83.5% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone | 79% |
2-Isopropoxyphenol
(S)-3-chloropropan-1,2-diol
Conditions | Yield |
---|---|
79% |
2-Isopropoxyphenol
2-(N-tert-butoxycarbonylamino)ethanol
[2-(2-isopropoxy-phenoxy)-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triphenylphosphine polystyrene; di-tert-butyl-diazodicarboxylate In tetrahydrofuran at 0 - 25℃; for 18h; | 78% |
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 25℃; for 18h; | 78% |
2-Isopropoxyphenol
ethylene dibromide
1-(2-bromoethoxy)-2-isopropoxybenzene
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone at 60℃; | 67% |
With potassium hydroxide In ethanol for 75h; Reflux; | 45% |
With potassium carbonate; potassium iodide In acetone Reflux; |
2-Isopropoxyphenol
1,3-chlorobromopropane
1-(3-chloropropoxy)-2-(1-methylethoxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 24h; Heating; | 62% |
With potassium hydroxide; potassium carbonate In acetone; benzene | 232 g (62%) |
2-Isopropoxyphenol
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; copper(l) chloride In dichloromethane at 20℃; for 5h; Irradiation; Inert atmosphere; | 61% |
Conditions | Yield |
---|---|
Stage #1: 2-Isopropoxyphenol With triethylamine; magnesium chloride In acetonitrile at 20℃; for 1h; Stage #2: formaldehyd In acetonitrile for 4h; Reflux; | 57% |
Stage #1: 2-Isopropoxyphenol With triethylamine; magnesium chloride In acetonitrile at 20℃; for 1h; Stage #2: formaldehyd In acetonitrile at 82℃; for 4h; | 57% |
Propyl isocyanate
2-Isopropoxyphenol
Propyl-carbamic acid 2-isopropoxy-phenyl ester
Conditions | Yield |
---|---|
With triethylamine |
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