CAS No.4875-10-9,2-NITROTHIOPHENOL Suppliers

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Synthetic route

: 1155-00-6
bis(2-nitrophenyl)disulfide

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With sodium tetrahydroborate In tetrahydrofuran	100%
With triisopropoxyborohydride In tetrahydrofuran at 0℃; for 0.25h;	92%
With triphenylphosphine; 2-hydroxyethanethiol In tetrahydrofuran; water at 50℃; for 21h; Inert atmosphere;	90%

: 1155-00-6
bis(2-nitrophenyl)disulfide

A: 4875-10-9
2-nitrothiophenol

B: 137-07-5
2-amino-benzenethiol

Conditions

Conditions	Yield
With sodium tetrahydroborate; zirconium(IV) chloride In tetrahydrofuran at 35℃; for 0.5h; Reduction;	A 10% B 90%
With sodium tetrahydroborate; zirconium(IV) chloride In tetrahydrofuran at 35℃; for 0.166667h; Reduction;	A 80% B 20%

: 88-73-3
2-Chloronitrobenzene

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With sodium sulfide In N,N-dimethyl-formamide for 62h; Ambient temperature;	87%
With thiourea In ethanol Heating;	60%
With ethanol; sodium disulfide

: 108732-56-5
4-o-nitrophenylthio-1,2-naphthoquinone

A: 83-72-7
2-Hydroxy-1,4-naphthoquinone

B: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With sodium hydroxide In ethanol; water for 0.0333333h;	A 80% B n/a

sodium sulfide (Na2 S.9H2 O): sodium sulfide (Na2 S.9H2 O)

: 88-73-3
2-Chloronitrobenzene

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
In hydrogenchloride	61%

: 88-73-3
2-Chloronitrobenzene

A: 1155-00-6
bis(2-nitrophenyl)disulfide

B: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With sodium sulfide In N,N-dimethyl-formamide for 62h; Ambient temperature;	A 60% B 25%
With sodium sulfide In dimethyl sulfoxide at 50℃; for 0.5h; Product distribution; further reagents, further solvent, further substituted o-chloronitrobenzenes, further times and temp.;	A 10% B 50%

: 1155-00-6
bis(2-nitrophenyl)disulfide

: 64-17-5
ethanol

: 50-99-7, 59-23-4, 921-60-8, 1949-88-8, 1990-29-0, 2152-76-3, 2595-97-3, 2595-98-4, 3458-28-4, 4205-23-6, 5934-56-5, 5978-95-0, 5987-68-8, 6027-89-0, 6038-51-3, 7635-11-2, 10030-80-5, 15572-79-9, 19163-87-2, 23567-25-1, 26566-61-0, 30077-17-9, 31103-86-3, 39665-52-6, 40866-07-7, 58367-01-4, 58407-05-9, 58407-06-0, 83198-69-0, 83198-70-3, 83198-71-4, 93780-23-5, 145920-48-5
glucose

: furan-2,3,5(4H)-trione pyridine (1:1)

: 4875-10-9
2-nitrothiophenol

...Expand

: 67-56-1
methanol

: 3406-02-8
bis(phenylsulfonyl)methane

: 124-41-4
sodium methylate

A: 4875-10-9
2-nitrothiophenol

B: 73622-50-1
Bis(phenylsulfonyl)(phenylthio)methane

Conditions

Conditions	Yield
anschliessendes Behandeln mit <2-Nitro-phenyl>-phenyl-disulfid;

...Expand

: 64-17-5
ethanol

: 28215-02-3
(2-nitro-phenyl)-phenyl disulfide

: 3111-52-2
potassium thiophenolate

A: 1155-00-6
bis(2-nitrophenyl)disulfide

B: 4875-10-9
2-nitrothiophenol

C: 882-33-7
diphenyldisulfane

...Expand

: 22024-99-3
2-nitrobenzenesulfenyl bromide

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With phosphorus tribromide Verduennen mit Aether und anschliessendes Versetzen mit Wasser;

: 20940-09-4
2-(2-nitro-phenylsulfanyl)-1-phenyl-ethanone

: 124-41-4
sodium methylate

A: 1629-75-0
2-benzoylbenzothiazole

B: 4875-10-9
2-nitrothiophenol

C: 65-85-0
benzoic acid

...Expand

: 28215-02-3
(2-nitro-phenyl)-phenyl disulfide

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With ethanol; potassium thiophenolate

: 7669-54-7
2-nitrobenzenesulfenyl chloride

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With DL-thiomalic acid; acetic acid Erwaermen des Reaktionsprodukts mit Natriumcyanid und wss. Alkalilauge;
Multi-step reaction with 2 steps 1: diethyl ether 2: potassium thiophenolate; alcohol View Scheme

: 528-29-0
1,2-Dinitrobenzene

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With methanol; sodium hydrogensulfide

: 20940-09-4
2-(2-nitro-phenylsulfanyl)-1-phenyl-ethanone

: 865-47-4
potassium tert-butylate

: 75-65-0
tert-butyl alcohol

A: 1629-75-0
2-benzoylbenzothiazole

B: 4875-10-9
2-nitrothiophenol

C: 65-85-0
benzoic acid

...Expand

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With sulfuric acid; zinc at 10℃;

: [Dimethylamino-(2-nitro-phenylsulfanyl)-methylene]-dimethyl-ammonium; iodide

A: 4875-10-9
2-nitrothiophenol

B: 632-22-4
tetramethylurea

Conditions

Conditions	Yield
at 20℃; Rate constant; pH=11;

: 6375-65-1
(2-nitro-phenylsulfanyl)-acetic acid

A: 4875-10-9
2-nitrothiophenol

B: 298-12-4
Glyoxilic acid

Conditions

Conditions	Yield
With perchloric acid; sodium perborate; acetic acid at 24.9℃; Rate constant; Thermodynamic data; Mechanism; var. temp., ΔH(excit.), ΔS(excit.);

: 6375-65-1
(2-nitro-phenylsulfanyl)-acetic acid

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With perchloric acid; pyridinium chlorochromate In water; acetic acid at 24.85 - 44.85℃; Kinetics; Oxidation;

: 528-29-0
1,2-Dinitrobenzene

Na2S: Na2S

: 4875-10-9
2-nitrothiophenol

: 64-17-5
ethanol

: 88-73-3
2-Chloronitrobenzene

sodium disulfide: sodium disulfide

A: 1155-00-6
bis(2-nitrophenyl)disulfide

B: 4875-10-9
2-nitrothiophenol

...Expand

: 67-56-1
methanol

: 528-29-0
1,2-Dinitrobenzene

NaHS: NaHS

A: 1155-00-6
bis(2-nitrophenyl)disulfide

B: 22100-66-9
bis-(2-nitro-phenyl)-sulfide

C: 4875-10-9
2-nitrothiophenol

...Expand

: 7732-18-5
water

: 88-73-3
2-Chloronitrobenzene

sodium sulfide: sodium sulfide

A: 22100-66-9
bis-(2-nitro-phenyl)-sulfide

B: 4875-10-9
2-nitrothiophenol

C: 137-07-5
2-amino-benzenethiol

D: 95-51-2
2-Chloroaniline

...Expand

: 88-73-3
2-Chloronitrobenzene

: furan-2,3,5(4H)-trione pyridine (1:1)

sodium sulfide: sodium sulfide

A: 22100-66-9
bis-(2-nitro-phenyl)-sulfide

B: 4875-10-9
2-nitrothiophenol

C: 137-07-5
2-amino-benzenethiol

D: 95-51-2
2-Chloroaniline

...Expand

: 22024-99-3
2-nitrobenzenesulfenyl bromide

: 7789-60-8
phosphorus tribromide

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
anschliessendes Verduennen mit Aether und Versetzen mit Wasser;

sodium-salt of thiosulfuric acid S-<2-nitro-phenyl ester>: sodium-salt of thiosulfuric acid S-<2-nitro-phenyl ester>

: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With hydrogenchloride

2-nitro-benzene-sulfonic acid-(1)-bromide: 2-nitro-benzene-sulfonic acid-(1)-bromide

A: 1155-00-6
bis(2-nitrophenyl)disulfide

B: 4875-10-9
2-nitrothiophenol

Conditions

Conditions	Yield
With phosphorus tribromide Behandeln des in Aether geloesten Reaktionsgemisches mit Wasser;

: 20940-09-4
2-(2-nitro-phenylsulfanyl)-1-phenyl-ethanone

methanol.KOH: methanol.KOH

A: 1629-75-0
2-benzoylbenzothiazole

B: 4875-10-9
2-nitrothiophenol

C: 65-85-0
benzoic acid

...Expand

: 20940-09-4
2-(2-nitro-phenylsulfanyl)-1-phenyl-ethanone

methanol.Na2CO3: methanol.Na2CO3

A: 1629-75-0
2-benzoylbenzothiazole

B: 4875-10-9
2-nitrothiophenol

C: 65-85-0
benzoic acid

...Expand

: 110-53-2
1-Bromopentane

: 4875-10-9
2-nitrothiophenol

: 76697-40-0
(2-nitrophenyl) (pentyl) sulfane

Conditions

Conditions	Yield
With sodium hydroxide In ethanol 1.) 15 min 2.) reflux, 14 h;	99.1%

: 4875-10-9
2-nitrothiophenol

: 56709-74-1
methyl 3-bromo-2,6-dinitro-5-methoxybenzoate

: 75355-04-3
methyl 2-nitro-3,6-di(2-nitrophenylthio)-5-methoxybenzoate

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide at 10℃; for 0.25h;	99%

: 4875-10-9
2-nitrothiophenol

: 67973-31-3
methyl 3-bromo-2,6-dinitro-5-methoxy-4-methylbenzoate

: 75355-07-6
methyl 2-nitro-3,6-di(2-nitrophenylthio)-5-methoxy-4-methylbenzoate

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide at 10℃; for 0.25h;	99%

: 4875-10-9
2-nitrothiophenol

: 1202041-29-9
C13H17BrO2

: 1202041-20-0
benzyl 5-(2-nitrophenylthio)hexanoate

Conditions

Conditions	Yield
With potassium carbonate; sodium iodide In acetone at 56℃;	99%

: 1-(4-nitrophenylthio)-6-bromo-hexane

: 4875-10-9
2-nitrothiophenol

: 1202041-25-5
1-(6-(4-nitrophenylthio)hexylthio)-2-nitrobenzene

Conditions

Conditions	Yield
With potassium carbonate; sodium iodide In acetone at 56℃;	98%

: 4875-10-9
2-nitrothiophenol

: 103-69-5
N-ethyl-N-phenylamine

: 81-10-7
2-Amino-N-ethyl-N-phenyl-benzenesulfonamide

Conditions

Conditions	Yield
In 1,4-dioxane at 87℃; Rate constant;	97.8%
In 1,4-dioxane at 87℃;	97.8%

: 4875-10-9
2-nitrothiophenol

: 831235-46-2
(S)-2-[(1R,3S,4aR,5R,8aS)-3-(tert-Butyl-diphenyl-silanyloxy)-5-((R)-1-methanesulfonyloxymethyl-2-methyl-propyl)-7-methyl-1,2,3,4,4a,5,6,8a-octahydro-naphthalen-1-yl]-propionic acid

: 831235-51-9
(S)-2-{(1R,3S,4aR,5R,8aS)-3-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-5-[(R)-2-methyl-1-(2-nitro-phenylsulfanylmethyl)-propyl]-1,2,3,4,4a,5,6,8a-octahydro-naphthalen-1-yl}-propionic acid

Conditions

Conditions	Yield
With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 55℃; for 8h;	97%

: 4875-10-9
2-nitrothiophenol

: 1155-00-6
bis(2-nitrophenyl)disulfide

Conditions

Conditions	Yield
With water; dihydrogen peroxide In various solvent(s) at 20℃; for 0.166667h; Oxidation; Dimerization;	96%
With sodium hydroxide; iodine for 6h; Heating;	90%
With bipyridinium hydrobromide perbromide In acetonitrile at 20℃; for 0.25h;	90%

: 4875-10-9
2-nitrothiophenol

: 100-44-7
benzyl chloride

: 22057-44-9
1-(benzylsulfanyl)-2-nitrobenzene

Conditions

Conditions	Yield
With sodium hydroxide In ethanol 1.) 15 min 2.) reflux, 14 h;	95.2%
With C40H30Cl2N2NiO2S2; sodium hydroxide In N,N-dimethyl-formamide at 70℃; for 1h;	95%
With alkali

: 4875-10-9
2-nitrothiophenol

: 70-11-1
α-bromoacetophenone

: 20940-09-4
2-(2-nitro-phenylsulfanyl)-1-phenyl-ethanone

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h;	95%
With sodium methylate In methanol	73%
With sodium carbonate

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 4875-10-9
2-nitrothiophenol

: 366470-09-9
8-[(2-nitrophenylthio)]-3,6-dioxaoctanol

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide for 6h; Heating;	95%

: 4875-10-9
2-nitrothiophenol

: 15159-67-8
(2S)-2-benzyloxycarbonylamino-4-bromo-butyric acid methyl ester

: 1187361-39-2
benzyl (S)-1-(methoxycarbonyl)-3-(2-nitrophenylthio)propylcarbamate

Conditions

Conditions	Yield
With potassium carbonate; sodium iodide In acetone at 90℃; Sealed tube;	94.9%

: 4875-10-9
2-nitrothiophenol

: 127-00-4
1-Chloro-2-propanol

A bis[β-(2-nitrophenylthio)-α-methyl-ethyl]-terephthalate: bis[β-(2-nitrophenylthio)-α-methyl-ethyl]-terephthalate

B: 28097-57-6
1-(2-nitro-phenylsulfanyl)-propan-2-ol

Conditions

Conditions	Yield
With sodium hydroxide In water	A n/a B 94.8%

...Expand

: 4875-10-9
2-nitrothiophenol

: 100-52-7
benzaldehyde

: 883-93-2
2-Phenylbenzothiazole

Conditions

Conditions	Yield
Stage #1: o-nitrothiophenol; benzaldehyde In 1,4-dioxane; water at 90℃; for 0.0833333h; Stage #2: With formic acid In 1,4-dioxane; water at 90℃; for 8h; Temperature; Sealed tube;	94%

: 111-25-1
1-bromo-hexane

: 4875-10-9
2-nitrothiophenol

: 76697-41-1
Hexyl-(2-nitrophenyl)-sulfid

Conditions

Conditions	Yield
With sodium hydroxide In ethanol 1.) 15 min 2.) reflux, 14 h;	93.5%

: 4875-10-9
2-nitrothiophenol

: 67973-25-5
benzyl 3-bromo-2,6-dinitro-5-benzyloxybenzoate

: 75355-08-7
benzyl 2-nitro-3,6-di(2-nitrophenylthio)-5-benzyloxybenzoate

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide at 10℃; for 0.25h;	93%

: 4875-10-9
2-nitrothiophenol

: 148773-54-0
1-bromo-11-(phenylthio)undecane

: 1202041-22-2
1-(11-(2-nitrophenylthio)undecylthio)benzene

Conditions

Conditions	Yield
With potassium carbonate; sodium iodide In acetone at 56℃;	93%

: 137-43-9
Cyclopentyl bromide

: 4875-10-9
2-nitrothiophenol

: 77053-23-7
Cyclopentyl-(2-nitrophenyl)-sulfid

Conditions

Conditions	Yield
With sodium hydroxide In ethanol 1.) 15 min 2.) reflux, 14 h;	92.7%

: 4875-10-9
2-nitrothiophenol

: 225937-33-7
methyl (3,4,5-tri-O-acetyl-β-D-arabino-hex-2-ulopyranosyl)onate bromide

: 225794-00-3
methyl 2-S-(2-nitrophenyl)-3,4,5-tri-O-acetyl-α-D-arabino-2-hexulopyranosonate

Conditions

Conditions	Yield
With potassium carbonate In acetone for 2h; Heating;	92%

: 4875-10-9
2-nitrothiophenol

: 628-89-7
2-(2-Chloroethoxy)ethanol

: 240131-55-9
2-<2-<2-nitrophenyl(thio)>ethoxy>ethanol

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide for 6h; Heating;	92%

: 4875-10-9
2-nitrothiophenol

: 53784-83-1
heptakis(6-bromo-6-deoxy)-β-cyclodextrin

: Heptakis-[6-thio(2'-nitrophenyl)-6-deoxy]-β-cyclodextrin

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide Ambient temperature;	90%

: 4875-10-9
2-nitrothiophenol

: 107-07-3
2-chloro-ethanol

A bis(2-aminophenylthioethyl)terephthalate: bis(2-aminophenylthioethyl)terephthalate

B: 13287-78-0
2-((2-nitrophenyl)thio)ethan-1-ol

Conditions

Conditions	Yield
With sodium hydroxide In water	A n/a B 89.8%

...Expand

: 4214-28-2
1-iodo-2,4-dimethylbenzene

: 4875-10-9
2-nitrothiophenol

: 2,4-dimethyl-1-[(2-nitro-phenyl)-sulfanyl]-benzene

Conditions

Conditions	Yield
With sodium hydride In tetrahydrofuran at 20℃; for 2h; Reagent/catalyst; Solvent;	89.6%

: 4875-10-9
2-nitrothiophenol

: 1423-60-5
methyl ethynyl ketone

: E/Z-4-(2-nitrophenylthio)-3-buten-2-one

Conditions

Conditions	Yield
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 0.5h; Substitution;	89%

: 4875-10-9
2-nitrothiophenol

: 106-95-6
allyl bromide

: 54848-79-2
allyl(2-(nitrophenyl))sulfane

Conditions

Conditions	Yield
Stage #1: o-nitrothiophenol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.666667h; Inert atmosphere; Stage #2: allyl bromide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere;	89%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 20h; Inert atmosphere; Cooling with ice;	3.1 g

: 4875-10-9
2-nitrothiophenol

: 78277-30-2
benzyl 11‐bromoundecanoate

: 1202041-14-2
benzyl 11-(2-nitrophenylthio)undecanoate

Conditions

Conditions	Yield
With potassium carbonate; sodium iodide In acetone at 56℃;	88%
With potassium carbonate; sodium iodide In acetone at 56℃; Reflux;	88%

: 4875-10-9
2-nitrothiophenol

: 870-63-3
prenyl bromide

: 1187627-61-7
1-(3-methyl-but-2-enylsulfanyl)-2-nitro-benzene

Conditions

Conditions	Yield
Stage #1: o-nitrothiophenol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.666667h; Inert atmosphere; Stage #2: prenyl bromide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere;	88%
Stage #1: o-nitrothiophenol With sodium hydride In tetrahydrofuran at 0℃; for 0.666667h; Inert atmosphere; Stage #2: prenyl bromide In tetrahydrofuran at 0 - 20℃; for 5h; Inert atmosphere;	79%

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