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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Cyclododeca-1,5,9-triene cas 4904-61-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryOMNISTAB® CDDT 1、Chemical Component: Cyclododeca-1,5,9-triene; 2、CAS:4904-61-4 3、Molecular Formula:Colorless clear liquid 4、Molecular Weight:162.27 5、Structure: 6、Specifications: Purity(%) : ≥99.50
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inquiryUnited Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Molecular Formula C12H18 Molecular Weight 162.27 CAS Registry Number 4904-61-4 EINECS 225-533-8 Cyclododeca-1,5,9-triene S…
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inquirystyrene
buta-1,3-diene
A
1,5-cis,cis-cyclooctadiene
B
cyclododeca-1,5,9-triene
C
1-phenyl-1,4,8(9)-decatriene
Conditions | Yield |
---|---|
With Ni acetylacetonate; triethylaluminum; triphenylphosphine In toluene at 90℃; for 1.41667h; Kinetics; Mechanism; Product distribution; other temperature; various ratio of components. Other object of study: the rate constants; | A 11.2 % Turnov. B 10.2 % Turnov. C 78.6 % Turnov. |
buta-1,3-diene
A
1,5-cis,cis-cyclooctadiene
B
vinylcyclohexane
C
cyclododeca-1,5,9-triene
Conditions | Yield |
---|---|
at 80℃; for 5h; Product distribution; also in presence aprotic solvents, var, times, temp.; |
buta-1,3-diene
A
1,5-cis,cis-cyclooctadiene
B
octa-1,3,7-triene
C
5-methyl-hepta-1,3,6-triene
D
4-ethenylcyclohexene
E
cyclododeca-1,5,9-triene
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; C17H34O2P2; triethylaluminum In benzene at 50℃; for 4h; Product distribution; Pressure (range begins): 730 ; |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; PC-P(OBu-t)2; triethylaluminum In benzene at 50℃; for 1h; Product distribution; Pressure (range begins): 730 ; |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide at 165℃; for 24h; Product distribution; Further Variations:; Reagents; Temperatures; copolymerization; |
Conditions | Yield |
---|---|
ethylaluminum sesquichloride; water; titanium tetrachloride In benzene at 60℃; under 1500.15 Torr; Product distribution / selectivity; | |
ethylaluminum sesquichloride; ammonia; water; titanium tetrachloride In benzene at 46 - 60℃; under 1500.15 Torr; Product distribution / selectivity; | |
ethylaluminum sesquichloride; ammonia; water; titanium tetrachloride In benzene at 60℃; under 1500.15 Torr; Product distribution / selectivity; | |
ethylaluminum sesquichloride; ammonia; water; titanium tetrachloride In 1-vinylcyclohexene; 1,3-cyclooctadiene at 60℃; under 1500.15 Torr; Product distribution / selectivity; | |
ethylaluminum sesquichloride; ammonia; titanium tetrachloride In benzene at 60℃; under 1500.15 Torr; Product distribution / selectivity; |
cyclododeca-1,5,9-triene
A
cyclododecane
B
cyclododecene
C
cyclododeca-1,5-diene
Conditions | Yield |
---|---|
With hydrogen at 80 - 160℃; under 760.051 Torr; Reagent/catalyst; Flow reactor; | A 100% B n/a C n/a |
With hydrogen; Ru4Sn6/Davison 923 mesoporous silica at 119.84℃; under 22502.3 Torr; for 12h; Product distribution; Further Variations:; reaction times; |
styrene
4-ethenylcyclohexene
cyclododeca-1,5,9-triene
polymer, average characteristics Mn 2570 Da, Mw 5080 Da, Mz 8020 Da; monomer(s): styrene; 4-vinylcyclohexene; 1,5,9-cyclododecatriene; n-dodeca-2,4,6,10-tetraene
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In octane; toluene at 160℃; for 18h; | 99.2% |
cyclododeca-1,5,9-triene
cyclododeca-1,5-diene
Conditions | Yield |
---|---|
With hydrogen at 240℃; under 760.051 Torr; for 0.000916667h; | 96% |
With hydrogen In methanol at 20℃; under 750.075 Torr; Catalytic behavior; Green chemistry; |
Conditions | Yield |
---|---|
With bromine In dichloromethane; 2-methyl-propan-1-ol; chloroform at 14 - 15℃; pH=7; Large scale; | 96% |
With bromine; sodium bromide In 2-methyl-propan-1-ol; chloroform; water at 10 - 15℃; for 4.5h; Solvent; Reagent/catalyst; Cooling with ice; | 94.9% |
With hydrogen bromide; bromine In 2-ethoxy-ethanol at 50 - 90℃; for 17h; Temperature; | 92% |
With 1-(-sulfonato)propyl-3-propanesulfonic acid imidazolium; hydrogen bromide; bromine In 2-ethoxy-ethanol at 50 - 90℃; for 8h; Temperature; | 90% |
With bromine In 2-methyl-propan-1-ol; 1,2-dichloro-ethane at 30 - 50℃; for 5.25h; |
Conditions | Yield |
---|---|
at 507℃; under 740 Torr; for 1h; Pressure; Temperature; Time; Inert atmosphere; | 76.7% |
cyclododeca-1,5,9-triene
Cyclododecadien-(5,9)-diol-(1,2)
Conditions | Yield |
---|---|
With osmium(VIII) oxide; 4-methylmorpholine N-oxide In dichloromethane; water at 20℃; for 24h; | 76% |
Stage #1: cyclododeca-1,5,9-triene With pyridine; osmium(VIII) oxide In ethanol at 0℃; for 2h; Stage #2: With sodium hydrogensulfite In ethanol at 20℃; for 12h; | |
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid / dichloromethane 2: water View Scheme |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; hydrogen; nickel dichloride In isopropyl alcohol at 50℃; under 760.051 Torr; for 6h; | 68% |
With hydrogen; oxohalogenophosphinerhenium complexes In toluene at 165℃; under 38000 Torr; Product distribution; different catalysts; other molar ratio PPh3 : catalyst; |
cyclododeca-1,5,9-triene
A
cyclododecene
B
cyclododeca-1,5-diene
Conditions | Yield |
---|---|
With hydrogen at 240℃; under 760.051 Torr; for 0.000638889h; | A 65% B 25% |
Stage #1: cyclododeca-1,5,9-triene With hydrogen; 0.5% palladium on alumina at 120℃; under 825.083 Torr; Industry scale; Gas phase; Stage #2: 0.5% palladium on alumina Product distribution / selectivity; | A n/a B 0.2% |
Stage #1: cyclododeca-1,5,9-triene With carbon monoxide; hydrogen; 0.5% palladium on alumina at 120℃; under 825.083 Torr; Industry scale; Gas phase; Stage #2: 0.5% palladium on alumina Product distribution / selectivity; | A n/a B 0.2% |
With hydrogen; Ru4Sn6/Davison 923 mesoporous silica at 99.84℃; under 22502.3 Torr; for 8h; Product distribution; Further Variations:; Catalysts; Temperatures; |
Conditions | Yield |
---|---|
With oxygen; isobutyraldehyde In acetonitrile at 60℃; for 4h; | 53% |
Stage #1: cyclododeca-1,5,9-triene With Aliquat 336 Under N2; Stirring; Heating up to 75 °ree;C; Stage #2: With phosphoric acid; dihydrogen peroxide; sodium tungstate In water at 75℃; for 1.5h; 60 % aq. H2O2 was added at 75 °ree;C; Na2WO4 and H3PO4 were added over a time of 25 min; | 163.1 g |
Stage #1: cyclododeca-1,5,9-triene Under N2; Stirring; Heating up to 75 °ree;C; Stage #2: With phosphoric acid; dihydrogen peroxide; sodium tungstate In water at 75℃; for 1.5h; 60 % aq. H2O2 was added at 75 °ree;C; Na2WO4 and H3PO4 were added over a time of 25 min; | 160.6 g |
cyclododeca-1,5,9-triene
1,2-dihydroacenaphthylene-1,2-diol
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium; 1,2-bis-(diphenylphosphino)ethane at 130℃; for 40h; Sealed tube; Inert atmosphere; diastereoselective reaction; | 43% |
tetrachloromethane
cyclododeca-1,5,9-triene
A
1-hydroxy-2-(trichloromethyl)cyclododecadiene-5,9
B
1-chloro-2-(trichloromethyl)cyclododecadiene-5,9
Conditions | Yield |
---|---|
With chromium(III) acetylacetonate; water In acetonitrile at 130℃; for 6h; Autoclave; | A 6% B 24% |
cyclododeca-1,5,9-triene
sodium chlorodifluoroacetate
A
(4Z,8Z)-13,13-difluoro-bicyclo[10.1.0]trideca-4,8-diene
B
(9E)-5,5,14,14-tetrafluoro-tricyclo[11.1.0.04,6]tetradec-9-ene
Conditions | Yield |
---|---|
at 190℃; Pyrolysis; | A 4.2% B 13.8% |
methanol
formic acid
cyclododeca-1,5,9-triene
Octahydro-cyclopenta[d]indene-3a-carboxylic acid methyl ester
Conditions | Yield |
---|---|
(i) H2SO4, CCl4, (ii) /BRN= 1098229/; Multistep reaction; |
Conditions | Yield |
---|---|
With dibenzoyl peroxide In n-heptane |
Conditions | Yield |
---|---|
With hydrogenchloride; nitrosylchloride In diethyl ether |
cyclododeca-1,5,9-triene
dimethyl amine
1-Dimethylamino-cyclododecadien-(5,9)-on-2-oxim
Conditions | Yield |
---|---|
(i) NOCl, (ii) /BRN= 605257/, aq. MeOH; Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogen; nickel(II) In methanol at 150℃; under 36752.9 Torr; var. solvents, var. catalysts Co and Ni complexes; other object of study- activity of catalysts; | |
With ruthenium trichloride; formaldehyd; hydrogen; acetic acid; triphenylphosphine In ethanol; water at 25 - 160℃; under 7500.75 - 15001.5 Torr; for 6.66667h; | |
With ruthenium trichloride; formaldehyd; hydrogen; acetic acid; triphenylphosphine In ethanol; water at 25 - 160℃; under 7500.75 - 15001.5 Torr; for 6.66667h; | |
With ruthenium trichloride; formaldehyd; hydrogen; acetic acid; triphenylphosphine In ethanol at 160℃; under 15001.5 Torr; Temperature; Pressure; |
cyclododeca-1,5,9-triene
12-oxododecanenitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) NOCl, (ii) /BRN= 605257/, aq. MeOH 2: H2 / Pd-C / ethanol 3: SO3 / liquid sulphur dioxide / -30 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NOCl, HCl / diethyl ether 2: H2 / Pd-C / methanol View Scheme | |
Multi-step reaction with 4 steps 1: dihydrogen peroxide / phosphotungstic acid; Aliquat 336 / water 2: hydrogen / platinum on activated charcoal 3: lithium iodide / 230 °C 4: hydroxyammonium sulfate; ammonia; sulfuric acid; ammonium sulfate / toluene; water / 85 °C / pH 4 - 5.8 / Industry scale View Scheme | |
Multi-step reaction with 3 steps 1.1: ruthenium trichloride; triphenylphosphine; acetic acid; formaldehyd; hydrogen / water; ethanol / 6.67 h / 25 - 160 °C / 7500.75 - 15001.5 Torr 2.1: dinitrogen monoxide / cyclohexane / 6 h / 300 - 350 °C / 75007.5 Torr / Flow reactor 3.1: ammonium acetate / ethanol / 80 °C 3.2: 0.5 h / 1350.14 Torr View Scheme | |
Multi-step reaction with 3 steps 1.1: triphenylphosphine; ruthenium trichloride; acetic acid; formaldehyd; hydrogen / water; ethanol / 6.67 h / 25 - 160 °C / 7500.75 - 15001.5 Torr 2.1: dinitrogen monoxide / 1 h / Flow reactor 3.1: ammonium acetate; ammonia / ethanol / 0.5 h / 80 °C / 1350.14 Torr / Flow reactor 3.2: Flow reactor View Scheme |
cyclododeca-1,5,9-triene
9-Aminocyclododecadien-(1,5)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NOCl, HCl / diethyl ether 2: LiAlH4 / diethyl ether View Scheme |
cyclododeca-1,5,9-triene
1-Dimethylamino-cyclododecanon-2-oxim
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) NOCl, (ii) /BRN= 605257/, aq. MeOH 2: H2 / Pd-C / ethanol View Scheme |
Conditions | Yield |
---|---|
With hydrogen; Ru4Sn6/Davison 923 mesoporous silica at 139.84℃; under 22502.3 Torr; for 8h; Product distribution; Further Variations:; Catalysts; Temperatures; |
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