As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:515-84-4
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Min.Order:5 Kiloliter
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Type:Manufacturers
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Cas:515-84-4
Min.Order:1 Metric Ton
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:515-84-4
Min.Order:10 Kilogram
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Type:Trading Company
inquiryProduct Name: Ethyl Trichloroacetate CAS: 515-84-4 MW: 191.44 MF: C4H5Cl3O2 Appearance: Colorless transparent liquid Assay: 98% Min. Appearance:Colorless liquid Storage: Preserve in well-closed, light-resistant and airtight containers. Package:
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryEthyl trichloroacetate CAS:515-84-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
Cas:515-84-4
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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inquiryCompany information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big cust
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Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Conditions | Yield |
---|---|
With sulfuric acid for 7h; Reflux; | 85% |
With sodium hydrogen sulfate for 2h; Esterification; Heating; | 84.5% |
With phosphorus pentoxide; copper(II) sulfate; sodium sulfate for 2h; Heating; | 41% |
diethyl (trichloromethyl)phosphonate
trichloroacetic acid
Ethyl trichloroacetate
Conditions | Yield |
---|---|
at 120℃; for 24h; | 77% |
acetaldehyde
triethyl phosphite
A
Ethyl trichloroacetate
B
diethyl 1-(1-ethoxyethyl)ethylphosphonate
Conditions | Yield |
---|---|
A n/a B 76% |
1,1,2,2-tetrachloroethylene
ethanol
ethyl acetate
A
freon-111
B
Ethyl trichloroacetate
Conditions | Yield |
---|---|
With chlorine monofluoride 1.) Freon 113; 2.) 20 - 25 deg C, 30 min.; Yield given. Multistep reaction; | A 68% B n/a |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide at 55℃; for 9h; Product distribution; other times, other temperatures; | 98 % Chromat. |
With aluminum ethoxide | |
With N,N-dimethyl-formamide at 55℃; for 9h; | 98 % Chromat. |
trichloro-acetic acid-(1-ethoxy-4,4,4-trichloro-3-oxo-but-1-enyl ester)
ethanol
A
Ethyl trichloroacetate
B
ethyl 4,4,4-trichloroacetoacetate
ethanol
chlorocarbonic acid pentachloroethyl ester
A
Ethyl trichloroacetate
B
chloroformic acid ethyl ester
ethanol
trichloro-acetic acid pentachloroethyl ester
Ethyl trichloroacetate
Conditions | Yield |
---|---|
With diethyl ether; aluminum ethoxide | |
With diethyl ether; magnesium methanolate | |
With aluminium triisopentylate |
Conditions | Yield |
---|---|
With chlorine; phosphorus trichloride im UV-Licht; Behandeln des Reaktionsprodukts mit Aethanol; |
Conditions | Yield |
---|---|
With benzene |
aluminum ethoxide
chloral
benzene
A
Ethyl trichloroacetate
B
2,2,2-trichloroethyl trichloroacetate
orthoformic acid triethyl ester
Trichloroacetyl chloride
Ethyl trichloroacetate
Conditions | Yield |
---|---|
at 95 - 160℃; |
orthoformic acid triethyl ester
Trichloroacetyl chloride
A
chloroethane
B
Ethyl trichloroacetate
C
formic acid ethyl ester
Conditions | Yield |
---|---|
at 160℃; reagiert analog mit anderen Carbonsaeure- und Sulfonsaeurechloriden; | |
at 95 - 160℃; |
phosphorus pentachloride
oxalic acid diethyl ester
Ethyl trichloroacetate
acetaldehyde
chloral
A
Ethyl trichloroacetate
B
2,2,2-trichloroethyl trichloroacetate
C
ethyl acetate
Conditions | Yield |
---|---|
Prod.5,6,7:2.2.2-Trichlor-aethylalkohol, 3-Hydroxy-1-acetoxy-butan, 4.4.4-Trichlor-3-hydroxy-1-acetoxy-butan; |
trichloromethyl trichloroacetate
A
Ethyl trichloroacetate
B
chloroformic acid ethyl ester
Conditions | Yield |
---|---|
in Waerme; |
triethyl phosphite
A
Ethyl trichloroacetate
B
diethyl 1-ethoxyethylphosphonate
Conditions | Yield |
---|---|
at 50 - 80℃; for 4.5h; Title compound not separated from byproducts; |
chloral
zinc
A
ethyl 2,2,4,4,4-pentachloro-3-hydroxybutyrate
B
Ethyl trichloroacetate
Ethyl trichloroacetate
Conditions | Yield |
---|---|
With sodium methylate | 99% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran 1.) r.t., 10 min, 2.) r.t., 10 min; | 98% |
Conditions | Yield |
---|---|
With silicon carbide In chlorobenzene at 200℃; for 1h; Microwave irradiation; regioselective reaction; | 98% |
Ethyl trichloroacetate
(Z)-1-methoxy-1,2-diphenylethene
1,1-Dichloro-r-2-methoxy-2,3-c-diphenylcyclopropane
Conditions | Yield |
---|---|
With sodium methylate In diethyl ether 1.) -15 deg C, 90 min, 2.) 4 deg C, overnight; | 95% |
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate at 90 - 150℃; for 2h; | 95% |
Ethyl trichloroacetate
cyclohexanecarbaldehyde
ethyl (Z)-2-chloro-3-cyclohexylacrylate
Conditions | Yield |
---|---|
With manganese for 5h; Inert atmosphere; Heating; stereoselective reaction; | 95% |
With Rieke-manganese In tetrahydrofuran for 5h; Inert atmosphere; Reflux; optical yield given as %de; stereoselective reaction; | 95% |
With manganese In tetrahydrofuran for 5h; Reflux; Inert atmosphere; stereoselective reaction; | 95% |
Conditions | Yield |
---|---|
ruthenium(II) bis(triphenylphosphine) dichloride In 1,4-dioxane at 75℃; for 24h; Kharasch reaction; | 94% |
Ethyl trichloroacetate
endo-10'-<(triisopropylsilyl)oxy>-anti-spiro2,5>undec-3'-ene>
4',exo-5'-dichloro-endo-11'-<(triisopropylsilyl)oxy>-anti-spiro2,6>dodec-3'-ene>
Conditions | Yield |
---|---|
With sodium methylate In hexane 1) 0 deg C to room temperature, 2) room temperature, 8 h; | 93% |
Conditions | Yield |
---|---|
With heptamethyl Coβ-perchlorato-cob(II)yrinate; tetrabutylammonium perchlorate In acetonitrile at 20℃; for 3h; Electrolysis; | 93% |
Ethyl trichloroacetate
isovaleraldehyde
ethyl (Z)-2-chloro-5-methylhex-2-enoate
Conditions | Yield |
---|---|
With manganese In tetrahydrofuran for 5h; Inert atmosphere; Heating; stereoselective reaction; | 92% |
With Rieke-manganese In tetrahydrofuran for 5h; Inert atmosphere; Reflux; optical yield given as %de; stereoselective reaction; | 92% |
With manganese In tetrahydrofuran for 5h; Reflux; Inert atmosphere; stereoselective reaction; | 92% |
Ethyl trichloroacetate
(E)-(1aS,7aR,1'aR,7'aS)-3,6,3',6'-Tetramethoxy-1a,2,7,7a,1'a,2',7',7'a-octahydro-[1,1']bi[cyclopropa[b]naphthalenylidene]
Conditions | Yield |
---|---|
With sodium methylate In benzene at 0 - 18℃; for 16h; | 91% |
Conditions | Yield |
---|---|
With sodium methylate In pentane 0 deg C to 18 deg C, 16 h; | 90% |
Conditions | Yield |
---|---|
In potassium carbonate; ethylene glycol | 90% |
With dmap In ethylene glycol |
dimethylenecyclourethane
Ethyl trichloroacetate
3-Carboethoxy-2-Oxazolidinone
Conditions | Yield |
---|---|
With dmap | 89% |
1-ethenyl-4-methylbenzene
Ethyl trichloroacetate
2,2,4-trichloro-4-phenyl-butyric acid ethyl ester
Conditions | Yield |
---|---|
With PS-PEG-PPh2-CP*RuCl2 In water at 60℃; for 9h; Kharasch reaction; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With Rieke-manganese In tetrahydrofuran for 5h; Inert atmosphere; Reflux; optical yield given as %de; stereoselective reaction; | 89% |
With manganese In tetrahydrofuran for 5h; Reflux; Inert atmosphere; stereoselective reaction; | 89% |
Ethyl trichloroacetate
Conditions | Yield |
---|---|
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; copper(II) bis(trifluoromethanesulfonate); sodium hydrogencarbonate In 1,2-dichloro-ethane at 80℃; for 18h; Inert atmosphere; Sealed tube; regioselective reaction; | 89% |
Ethyl trichloroacetate
(3,4-dihydronaphthalen-1-yl)(phenyl)sulfane
1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene
Conditions | Yield |
---|---|
88% |
Ethyl trichloroacetate
2,6,6-trimethyl-1-((trimethylsilyl)oxy)cycloheptene
8,8-dichloro-3,3,7-trimethyl-1-((trimethylsilyl)oxy)bicyclo<5.1.0>octane
Conditions | Yield |
---|---|
With sodium methylate In pentane 1) 0 deg C, 6h, 2) RT, 15h; | 88% |
Ethyl trichloroacetate
N-(indolyl-3-imidoyl)guanidine
2-amino-4-(indolyl-3)-6-trichloromethyl-sym-triazine
Conditions | Yield |
---|---|
In ethanol Heating; | 88% |
Conditions | Yield |
---|---|
With silicon carbide In chlorobenzene at 200℃; for 1h; Microwave irradiation; regioselective reaction; | 88% |
Ethyl trichloroacetate
6β-methoxy-3α,5-cyclo-5α-androstan-17-one
ethyl 6β-methoxy-20ξ-chloro-17(20)-i-pregnen-21-oate
Conditions | Yield |
---|---|
With diethylaluminium chloride; zinc In tetrahydrofuran; hexane at 0℃; for 2h; | 87% |
10-Undecenal
Ethyl trichloroacetate
ethyl (Z)-2-chlorotrideca-2,12-dienoate
Conditions | Yield |
---|---|
With Rieke-manganese In tetrahydrofuran for 5h; Inert atmosphere; Reflux; optical yield given as %de; stereoselective reaction; | 87% |
With manganese In tetrahydrofuran for 5h; Reflux; Inert atmosphere; stereoselective reaction; | 87% |
styrene
Ethyl trichloroacetate
2,2,4-trichloro-4-phenyl-butyric acid ethyl ester
Conditions | Yield |
---|---|
With (η5-1-t-Bu-2-PhC≡C-(1,2-azaboronyl))RuCl(PPh3)2 In toluene at 85℃; for 5h; Schlenk technique; Inert atmosphere; Glovebox; | 85% |
With 2,2'-azobis(isobutyronitrile); Cp*Ru(PPh3)2Cl In (2)H8-toluene at 60℃; for 1.5h; Inert atmosphere; | 61% |
ruthenium(II) bis(triphenylphosphine) dichloride In benzene at 75℃; for 24h; Kharasch reaction; | 60% |
Ethyl trichloroacetate
phenylacetylene
1,1,1-trichloro-4-phenyl-3-butyn-2-one
Conditions | Yield |
---|---|
Stage #1: phenylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: Ethyl trichloroacetate With boron trifluoride diethyl etherate In tetrahydrofuran; hexane at 20℃; for 2h; Further stages.; | 85% |
Stage #1: phenylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 3h; Inert atmosphere; Stage #2: Ethyl trichloroacetate With boron trifluoride diethyl etherate In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere; | 83% |
(i) nBuLi, (ii) /BRN= 1761567/; Multistep reaction; |
Conditions | Yield |
---|---|
With sodium methylate | 85% |
Ethyl trichloroacetate
3-tetrahydropyran-2-yloxy-androst-5-en-17-one
ethyl 20ξ-chloro-3β-(tetrahydropyranyloxy)-5,17(20)-pregnadien-21-oate
Conditions | Yield |
---|---|
With diethylaluminium chloride; zinc In tetrahydrofuran; hexane at 0℃; for 2h; | 85% |
Conditions | Yield |
---|---|
Stage #1: acetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: Ethyl trichloroacetate With boron trifluoride diethyl etherate In tetrahydrofuran; hexane at 20℃; for 2h; Further stages.; | 85% |
1.3-propanedithiol
Ethyl trichloroacetate
ethyl 1,3-dithiane-2-carboxylate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.25h; | 85% |
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