Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:5521-55-1
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inquiryhigh quality ,iso , cgmp . accept the supplier audit . in stock now ,capacity is flexible support the documents Appearance: Light yellow to off white powder Storage: protect from light seal room temperature Package:DRUM Application:key inter
Product name :5-Methylpyrazine-2-Carboxylic Acid cas:5521-55-1 we are specialize in manufacturing Glipizide/Acipimox intermediates ,we are supplying 5-Methylpyrazine-2-Carboxylic Acid CAS:5521-55-1 2,5-dimethylpyrazine CAS:123-32-0 wit
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Orange to light brown crystalline powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:pharmac
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inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/535.html Product Name 5-Methyl-2-pyrazinecarboxylic acid CAS No. 5521-55-1
Cas:5521-55-1
Min.Order:1 Gram
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryProduct name 5-Methyl-2-pyrazinecarboxylic acid CAS 5521-55-1 Boiling point 253.51°C (rough estimate) form Amorphous Powder Appe
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Cas:5521-55-1
Min.Order:100 Gram
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inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Appearance:light yellow powder Storage:storage
Cas:5521-55-1
Min.Order:1 Kilogram
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inquiry5-Methyl-2-pyrazinecarboxylic acid CAS: 5521-55-1 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure
Cas:5521-55-1
Min.Order:1 Kilogram
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Type:Other
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
5-Methyl-2-pyrazinecarboxylic acid Cas No 5521-55-1 Molecular formula C6H6N2O2 Appearance white to light yellow powder Melting point 164ºC-168ºC Water ≤0.5%
Cas:5521-55-1
Min.Order:1 Kilogram
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Min.Order:10 Kilogram
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Min.Order:1 Kilogram
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Cas:5521-55-1
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inquiryName 5-Methyl-2-pyrazinecarboxylic acid Synonyms 5-Methylpyrazine-2-carboxylic acid Molecular Structure Mole
Cas:5521-55-1
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Cas:5521-55-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
at 30℃; for 16h; Pseudomonas putida ATCC 33015; | 90% |
With potassium permanganate In water at 76 - 82℃; for 5.7h; Temperature; Industrial scale; | 81.6% |
With sodium tungstate; oxygen; cobalt(II) nitrate; manganese(ll) chloride In water | 75.6% |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen; sodium hydroxide In methanol at 60℃; under 15001.5 Torr; for 12h; Autoclave; Inert atmosphere; | 68% |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen; sodium hydroxide In methanol at 60℃; under 15001.5 Torr; for 12h; Reagent/catalyst; Autoclave; Inert atmosphere; | 71% |
2-(chloromethyl)-5-methylpyrazine hydrochloride
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With potassium carbonate In water; tert-butyl alcohol at 60℃; Ni-anode, 12 mA/cm2; | 82% |
Multi-step reaction with 2 steps 1: 74 percent / KOAc, KHCO3 / ethanol / 6 h / Heating 2: 93 percent / 1 N aq. NaOH / 40 °C / Ni-anode, 12 mA/cm2 View Scheme | |
Multi-step reaction with 2 steps 1: 65 percent / KOAc / ethanol / 6 h / Heating 2: 87 percent / 1 N aq.NaOH / 40 °C / Ni-anode, 12 mA/cm2 View Scheme |
2-Hydroxymethyl-5-methylpyrazine
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 40℃; Ni-anode, 12 mA/cm2; | 93% |
With potassium permanganate for 0.5h; Oxidation; |
2-Acetoxymethyl-5-methylpyrazine
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 40℃; Ni-anode, 12 mA/cm2; | 87% |
Multi-step reaction with 2 steps 1: 85 percent / NaOH / ethanol / 0.17 h 2: aq. KMnO4 / 0.5 h View Scheme |
Conditions | Yield |
---|---|
at 175 - 185℃; under 2 Torr; | 71% |
2,5-dimethyl-pyrazine
A
2-methylpyrazin-5-carboxylic acid
B
2,5-pyrazinedicarboxylic acid
Conditions | Yield |
---|---|
With chromium(III) nitrate In water Ambient temperature; electrochemical oxidation on activated nickel hydroxide anode; | A 40% B 20% |
2-methyl-5-pyrazinylmethyl chloride
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent Chromat. / ethanol / Heating 2: 85 percent / NaOH / ethanol / 0.17 h 3: aq. KMnO4 / 0.5 h View Scheme |
3-carboxamido-2-hydroxy-6-methylpyrazine
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sulfuric acid / 12 h / 100 °C 2: thionyl chloride / 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide / 6 h / 80 °C 3: palladium 10% on activated carbon; hydrogen; sodium hydroxide / methanol / 12 h / 60 °C / 15001.5 Torr / Autoclave; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: sulfuric acid / 12 h / 100 °C 2: dibromo sulfoxide / 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide / 6 h / 80 °C 3: palladium 10% on activated carbon; hydrogen; sodium hydroxide / methanol / 12 h / 60 °C / 15001.5 Torr / Autoclave; Inert atmosphere View Scheme |
2-Hydroxy-6-methylpyrazine-3-carboxylic acid
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide / 6 h / 80 °C 2: palladium 10% on activated carbon; hydrogen; sodium hydroxide / methanol / 12 h / 60 °C / 15001.5 Torr / Autoclave; Inert atmosphere View Scheme |
2,5-dimethyl-pyrazine
A
2-methylpyrazin-5-carboxylic acid
B
diethyl pyrazine-2,5-dicarboxylate
Conditions | Yield |
---|---|
With potassium permanganate |
A
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With water In acetonitrile at 37℃; for 0.166667h; pH=2.0; Kinetics; Further Variations:; pH-values; reaction time; Acid hydrolysis; |
2,5-dimethyl-pyrazine
A
2-pyrazylcarboxylic acid
B
2-methylpyrazin-5-carboxylic acid
C
2,5-pyrazinedicarboxylic acid
Conditions | Yield |
---|---|
With cobalt(II) nitrate In water Ambient temperature; electrochemical oxidation on activated nickel hydroxide anode; | A 2% B 42% C 3% |
In water Ambient temperature; electrochemical oxidation on activated nickel hydroxide anode; | A 12% B 22% C 5% |
With chromium(III) nitrate In diethyl ether Product distribution; Ambient temperature; electrochemical oxidation; var. additives, var. reaction time vs. conversion; |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With NaOH In water ligand was added to aq. soln. of NaOH, stirred at room temp. for 10 min, CuCl2*2H2O was added slowly, stirred at room temp. for 2 h; filtered, washed with water, dried in air; elem. anal.; | 99% |
2-methylpyrazin-5-carboxylic acid
acipimox
Conditions | Yield |
---|---|
Stage #1: 2-methylpyrazin-5-carboxylic acid With hydrogenchloride In water for 0.5h; Stage #2: With peracetic acid In water at 20℃; for 3h; Reagent/catalyst; Temperature; | 98.5% |
With sodium tungstate; dihydrogen peroxide; sodium hydroxide In water at 45℃; for 12h; pH=9; Concentration; pH-value; Reagent/catalyst; Temperature; | 94.5% |
Stage #1: 2-methylpyrazin-5-carboxylic acid With sulfuric acid at 60℃; for 1h; Large scale; Stage #2: With disodium tungstate dihydrate; dihydrogen peroxide In water for 8h; Heating; Large scale; | 77.3% |
2-methylpyrazin-5-carboxylic acid
1-<sulfonyl>-3-cyclohexyl-2-iminoimidazolidine
5-Methyl-pyrazine-2-carboxylic acid {2-[4-(3-cyclohexyl-2-imino-imidazolidine-1-sulfonyl)-phenyl]-ethyl}-amide
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran; acetonitrile for 12h; Ambient temperature; | 97% |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With NaOH; H2O In water acid was added to a soln. of NaOH in water and stirred at room temp. for10 min, CuCl2 was added slowly, the mixt. was stirred at room temp. for 2 h; filtered, ppt. was washed with water and dried in air; | 97% |
2-methylpyrazin-5-carboxylic acid
tert-butyl alcohol
t-butyl 5-methylpyrazine-2-carboxylate
Conditions | Yield |
---|---|
With dmap; di-tert-butyl dicarbonate at 60℃; for 18h; | 95% |
Stage #1: 2-methylpyrazin-5-carboxylic acid; tert-butyl alcohol With di-tert-butyl dicarbonate In tert-butyl alcohol at 55℃; for 0.25h; Stage #2: With dmap at 55℃; for 17h; | 86% |
2-methylpyrazin-5-carboxylic acid
N-(4-[2-amino-ethyl]-benzenesulfonyl)-N'-cyclohexyl urea
N-[2-[4-(amino-sulfonyl)phenyl]ethyl]-5-methylpyrazinecarboxamide
Conditions | Yield |
---|---|
Stage #1: 2-methylpyrazin-5-carboxylic acid With triethylamine In acetone at 0℃; for 1h; Stage #2: With chloroformic acid ethyl ester In acetone for 1h; Stage #3: N-(4-[2-amino-ethyl]-benzenesulfonyl)-N'-cyclohexyl urea With triethylamine In acetone at 20℃; for 3h; | 93.4% |
2-methylpyrazin-5-carboxylic acid
benzyl alcohol
benzyl-5-methylpyrazin-2-yl carbamate
Conditions | Yield |
---|---|
With diphenyl phosphoryl azide; triethylamine In acetonitrile at 120℃; | 87% |
Stage #1: 2-methylpyrazin-5-carboxylic acid With N-ethyl-N,N-diisopropylamine In toluene at 50℃; Inert atmosphere; Stage #2: With diphenyl phosphoryl azide In toluene at 15℃; Stage #3: benzyl alcohol In toluene at 85 - 90℃; for 3h; | 85% |
2-methylpyrazin-5-carboxylic acid
di(n-butyl)tin oxide
[((n-Bu)2Sn(2-methylpyrazine-5-acid(-1H)))2O]2
Conditions | Yield |
---|---|
In methanol; benzene (N2); acid was added to soln. of Sn compd. in C6H6/MeOH (5/1) in Schlenkflask; refluxed for 10 h; solvent evapd. (vac. ); recrystd. (MeOH); elem. anal.; | 86% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In tetrahydrofuran; N,N-dimethyl-formamide | 86% |
2-methylpyrazin-5-carboxylic acid
2-(2,4-dimethylphenylsulphanyl)benzeneamine
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide for 1h; | 85% |
Conditions | Yield |
---|---|
Stage #1: 2-methylpyrazin-5-carboxylic acid; tert-butyl N-(1-amino-3-bicyclo[1.1.1]pentanyl)carbamate With pyridine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: trifluoroacetic acid In acetonitrile at 20℃; for 1h; | 83% |
2-methylpyrazin-5-carboxylic acid
diphenyltin(IV) oxide
[(Ph2Sn(2-methylpyrazine-5-acid(-1H)))3O2(Ph2Sn(OCH3))]
Conditions | Yield |
---|---|
In methanol; benzene (N2); acid was added to soln. of Sn compd. in C6H6/MeOH (5/1) in Schlenkflask; refluxed for 10 h; solvent evapd. (vac. ); recrystd. (MeOH); elem. anal.; | 82% |
2-methylpyrazin-5-carboxylic acid
7-(5-aminopyridin-2-yloxy)-4-methyl-2H-chromen-2-one
5-methyl-N-(6-((4-methyl-2-oxo-2H-chromen-7-yl)oxy)pyridin-3-yl)pyrazine-2-carboxamide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 81.9% |
Conditions | Yield |
---|---|
Stage #1: 2-methylpyrazin-5-carboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h; Stage #2: 3-aminolup-20(29)-en-28-oic acid With dmap In dichloromethane at 20℃; for 8h; | 81% |
Stage #1: 2-methylpyrazin-5-carboxylic acid With dmap; 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 2h; Inert atmosphere; Stage #2: 3-aminolup-20(29)-en-28-oic acid In dichloromethane at 20℃; for 8h; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With C2H5ONa In benzene byproducts: NaCl; (N2); acid was added to soln. of Sn compd. in C6H6 in Schlenk flask; stirred for 0.5 h; EtONa was added; stirred at 50°C for 12 h; filtered; solvent evapd. (vac. ); recrystd. (MeOH); elem. anal.; | 80% |
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 30℃; for 6h; Inert atmosphere; | 80% |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: 4-[5-(naphtho[2,1-b]furan-2-yl)-1,3,4-oxadiazol-2-yl]aniline With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; Inert atmosphere; Stage #2: 2-methylpyrazin-5-carboxylic acid In dichloromethane at 20℃; Inert atmosphere; | 80% |
2-methylpyrazin-5-carboxylic acid
(2,4-Cl2C6H3CH2)3SnCl
[(2,4-Cl2C6H3CH2)2Sn(2-methylpyrazine-5-acid(-1H))2ClSn(CH2C6H3Cl2-2,4)3]2
Conditions | Yield |
---|---|
With C2H5ONa In benzene byproducts: NaCl; (N2); acid was added to soln. of Sn compd. in C6H6 in Schlenk flask; stirred for 0.5 h; EtONa was added; stirred at 50°C for 12 h; filtered; solvent evapd. (vac. ); recrystd. (MeOH); elem. anal.; | 79% |
2-methylpyrazin-5-carboxylic acid
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 10h; | 79% |
2-methylpyrazin-5-carboxylic acid
di[bis[9-(2-(2-methoxyethoxy)ethyl)-3-(4-phenylquinolin-2-yl)-9H-carbazolato-N,C2']iridium(III) chloride]
bis[9-(2-(2-methoxyethoxy)ethyl)-3-(4-phenylquinolin-2-yl)-9H-carbazolato-N,C2']iridium(III)(5-methyl-2-pyridinecarboxylate)
Conditions | Yield |
---|---|
With Na2CO3 In 2-ethoxy-ethanol Ir complex and 5-methyl-2-pyridinecarboxylic acid (5 equiv.) mixed with Na2CO3 (10 equiv.) in 2-ethoxyethanol, refluxed for 12 h (N2); cooled ro room temp., poured into H2O, extd.(EtOAc), dried (MgSO3), evapd.(vac.), chromy.(silica gel - hexane/EtOAc 1:4), recrystd twice (CH2Cl2/hexane), elem. anal.; | 78% |
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