CAS No.56563-01-0,ETHYL 2-(1H-1,2,4-TRIAZOL-1-YL)ACETATE Suppliers

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Nanjing Raymon Biotech Co., Ltd.

ETHYL 2-(1H-1,2,4-TRIAZOL-1-YL)ACETATE Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Sha

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Allichem LLC

ETHYL 2-(1H-1,2,4-TRIAZOL-3-YL)ACETATE

1H-1,2,4-Triazole-1-aceticacid, ethyl ester

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Synthetic route

: 288-88-0
1,2,4-Triazole

: 105-39-5
chloroacetic acid ethyl ester

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

Conditions

Conditions	Yield
With potassium carbonate In 1,4-dioxane for 6h; Heating;	84%
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In acetone at 50 - 55℃; for 4h;	76%
With sodium hydroxide In N,N-dimethyl-formamide for 1h; Ambient temperature;	70%
With sodium ethanolate In ethanol at 70℃; for 12h; sealed tube;	69%

: 288-88-0
1,2,4-Triazole

: 105-39-5
chloroacetic acid ethyl ester

A: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

B: ethyl 4H-1,2,4-triazol-4-yl-acetate

Conditions

Conditions	Yield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0 - 20℃; Alkylation;	A 69% B n/a

...Expand

: 288-88-0
1,2,4-Triazole

: 105-36-2
ethyl bromoacetate

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h;	65%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h;	65%
With potassium carbonate In N,N-dimethyl-formamide for 16h;	56%
With sodium ethanolate

: 288-88-0
1,2,4-Triazole

: 105-36-2
ethyl bromoacetate

A: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

B: ethyl 4H-1,2,4-triazol-4-yl-acetate

Conditions

Conditions	Yield
With sodium ethanolate 1.) EtOH, RT, 2 h, 2.) EtOH, overnight; Yield given. Multistep reaction;
With sodium ethanolate 1.) EtOH, RT, 2 h, 2.) EtOH, overnight; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

...Expand

: 288-88-0
1,2,4-Triazole

: 70-11-1
α-bromoacetophenone

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

Conditions

Conditions	Yield
With ethanol; sodium Yield given. Multistep reaction;

: 41253-21-8
sodium triazole

: 105-36-2
ethyl bromoacetate

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at -10 - 20℃; for 20h;

: 28711-29-7
2-(1H-1,2,4-triazol-1-yl)acetic acid

: 64-17-5
ethanol

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

Conditions

Conditions	Yield
With hydrogenchloride at 20℃;

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 109-94-4
formic acid ethyl ester

: 82248-27-9
Sodium; (E)-2-ethoxycarbonyl-2-[1,2,4]triazol-1-yl-ethenolate

Conditions

Conditions	Yield
With sodium In ethanol; toluene at 31℃; for 2h;	98.5%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 56563-02-1
2-(1H-1,2,4-triazol-1-yl)acetohydrazide

Conditions

Conditions	Yield
With hydrazine hydrate for 5h; Reflux;	94%
With hydrazine hydrate In 1,4-dioxane for 5h; Heating;	82%
With hydrazine hydrate In ethanol for 24h; Ambient temperature;	71%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 62-53-3
aniline

: 154221-24-6
α-(1,2,4-triazole-1-yl)-N-phenylacetamide

Conditions

Conditions	Yield
In ethanol for 15h; Heating;	82%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 100-46-9
benzylamine

: 156097-78-8
N-Benzyl-2-[1,2,4]triazol-1-yl-acetamide

Conditions

Conditions	Yield
In ethanol for 15h; Heating;	81%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 79-19-6
thiosemicarbazide

: 503524-74-1
(N1-1,2,4-triazolylacetyl)-thiosemicarbazide

Conditions

Conditions	Yield
In 1,4-dioxane for 7h; Heating;	81%

: 107-10-8
propylamine

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 156097-77-7
N-Propyl-2-[1,2,4]triazol-1-yl-acetamide

Conditions

Conditions	Yield
In ethanol for 15h; Heating;	78%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 70-11-1
α-bromoacetophenone

: 133593-04-1
(1-N-carbethoxymethylene-4-N-phenacyl)-1,2,4-triazolium bromide

Conditions

Conditions	Yield
In acetone Heating;	77%
In acetone

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 38100-34-4
hydroxylamine O-picryl ether

: 4-amino-1-ethoxycarbonylmethyl-1,2,4-triazolium picrate

Conditions

Conditions	Yield
In dichloromethane at 20℃;	76%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 99-81-0
4-Nitrophenacyl bromide

: 133593-05-2
(1-N-carbethoxymethylene-4-N-p-nitrophenacyl)-1,2,4-triazolium bromide

Conditions

Conditions	Yield
In acetone Heating;	67%
In acetone

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 28711-29-7
2-(1H-1,2,4-triazol-1-yl)acetic acid

Conditions

Conditions	Yield
With sodium hydroxide In methanol for 0.25h; Ambient temperature;	63%
With hydrogenchloride In water at 95℃; for 16h;	62%
With hydrogenchloride at 95℃; for 16h;	62%
With hydrogenchloride; water

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 589-15-1
1-bromomethyl-4-bromobenzene

: 501031-47-6
ethyl 3-(4-bromophenyl)-2-(1H-1,2,4-triazol-1-yl)propanoate

Conditions

Conditions	Yield
Stage #1: ethyl 2-(1H-1,2,4-triazol-1-yl)acetate With lithium diisopropyl amide In diethyl ether; hexane at -20℃; Inert atmosphere; Stage #2: 1-bromomethyl-4-bromobenzene In diethyl ether; hexane at -20 - 20℃; Inert atmosphere;	21%

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 3273-14-1
1-(2-hydroxyethyl)-1H-1,2,4-triazole

Conditions

Conditions	Yield
With lithium aluminium tetrahydride; diethyl ether

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 63190-93-2
2-[1,2,4]triazol-1-yl-acetamide

Conditions

Conditions	Yield
With methanol; ammonia

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C6H7(2)H2N3O2

Conditions

Conditions	Yield
With [(2)H6]acetone; water-d2; triethylamine for 53h; Ambient temperature;

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 100-39-0
benzyl bromide

: 4-benzyl-1-ethoxycarbonylmethyl-1H-[1,2,4]triazol-4-ium; bromide

Conditions

Conditions	Yield
In acetone at 20℃; for 168000h; Alkylation;

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 103-72-0
phenyl isothiocyanate

: 4-phenyl-3-(1,2,4-triazol-1-ylmethyl)-1,2,4-triazoline-5-thione

Conditions

Conditions	Yield
With sodium hydroxide; hydrazine In water

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C18H17N5O2S

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: acetone / 168000 h / 20 °C 2: K2CO3 / CHCl3; ethanol / 168000 h / 20 °C View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C18H16N4O3S

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: acetone / 168000 h / 20 °C 2: 28 percent / K2CO3 / CHCl3; ethanol / 168000 h / 20 °C View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C19H19N3O5

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: acetone / 168000 h / 20 °C 2: K2CO3 / CHCl3; ethanol / 168000 h / 20 °C 3: 30 percent / xylene / 24 h / Heating View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C18H17N5O2S

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: acetone / 168000 h / 20 °C 2: K2CO3 / CHCl3; ethanol / 168000 h / 20 °C 3: 35 percent / xylene / 24 h / Heating View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C21H25N3O6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: acetone / 168000 h / 20 °C 2: K2CO3 / CHCl3; ethanol / 168000 h / 20 °C View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C14H15N3O3

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 77 percent / acetone / Heating 2: aq. K2CO3 / CH2Cl2 / 0.33 h View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: C14H14N4O5

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 67 percent / acetone / Heating 2: aq. K2CO3 / CH2Cl2 / 0.33 h View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 1-carbethoxymethylene, benzoyl 2,4,6-trinitrophenyl 4-triazolium-methylide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 77 percent / acetone / Heating 2: Et3N / CH2Cl2 / Ambient temperature View Scheme

: 56563-01-0
ethyl 2-(1H-1,2,4-triazol-1-yl)acetate

: 1-carbethoxymethylene, p-nitrobenzoyl 2,4,6-trinitrophenyl 4-triazolium-methylide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 67 percent / acetone / Heating 2: Et3N / CH2Cl2 / Ambient temperature View Scheme

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Antimex Chemical Limied

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