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1-pentylindoleAppearance:ask Storage:Keep in dry and cool condition Package:foil aluminium bag/vacuum packing Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or b
The factory supplies Application:manufacturing supplies
Conditions | Yield |
---|---|
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; | 100% |
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 5 - 20℃; Inert atmosphere; Stage #2: 1-Bromopentane In N,N-dimethyl-formamide; mineral oil at 5 - 20℃; for 16h; Inert atmosphere; | 95% |
With potassium hydroxide; tetrabutylammomium bromide; potassium carbonate for 0.0075h; microwave irradiation (300 W); | 86% |
1-pentyl-1H-indole
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In toluene for 5.5h; Heating; | 92% |
Conditions | Yield |
---|---|
With chloro-(pentamethylcyclopentadienyl)-{5-methoxy-2-{1-[(4-methoxyphenyl)imino-N]ethyl}phenyl-C}-iridium(lll); potassium carbonate In 2,2,2-trifluoroethanol at 100℃; for 12h; | 77% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 80℃; for 16h; | 75% |
n-butyl magnesium bromide
1-(1H-benzotriazol-1-yl-methyl)-1H-indole
1-pentyl-1H-indole
Conditions | Yield |
---|---|
In benzene for 25h; Heating; | 37% |
1-(5-Iodopentyl)-2-(phenylsulfanyl)-1H-indole
A
1-pentyl-1H-indole
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In toluene for 4h; Yield given. Yields of byproduct given; |
1-pentyl-1H-indole
2-aminoacetonitrile hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2-aminoacetonitrile hydrochloride With sodium nitrite In water at 55℃; Stage #2: 1-pentyl-1H-indole With meso-tetraphenylporphyrin iron(III) chloride In dichloromethane; water at 20℃; for 2.16h; Inert atmosphere; | 96% |
1-pentyl-1H-indole
phenyltrifluorodiazoethane
Conditions | Yield |
---|---|
With o-phenylenebis(diphenylphosphine); palladium diacetate; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In dichloromethane at 20℃; | 94% |
1-pentyl-1H-indole
ethyl 3,3,3-trifluoro-2-((4-methoxyphenyl)imino)propanoate
Conditions | Yield |
---|---|
With copper(II) trifluoroacetate In dichloromethane at 25℃; for 12h; Friedel-Crafts Alkylation; | 93% |
1-pentyl-1H-indole
Conditions | Yield |
---|---|
With silica-gel-supported sulfuric acid In acetonitrile at 80℃; for 2h; | 89% |
1-pentyl-1H-indole
o-phenylbenzoyl chloride
[1,1'-biphenyl]-2-yl(1-pentyl-1H-indol-3-yl)methanone
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With diethyl aluminiumcholoride In hexane; dichloromethane at -10℃; for 0.75h; Inert atmosphere; Stage #2: o-phenylbenzoyl chloride In hexane; dichloromethane at -10 - 0℃; Friedel Crafts acylation; Inert atmosphere; | 88% |
1-pentyl-1H-indole
3-phenylbenzoyl chloride
[1,1'-biphenyl]-3-yl(1-pentyl-1H-indol-3-yl)methanone
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With diethyl aluminiumcholoride In hexane; dichloromethane at -10℃; for 0.75h; Inert atmosphere; Stage #2: 3-phenylbenzoyl chloride In hexane; dichloromethane at -10 - 0℃; Friedel Crafts acylation; Inert atmosphere; | 87% |
1-pentyl-1H-indole
1-Adamantanecarbonyl chloride
1-pentyl-N-tricyclo[3.3.1.1]dec-1-yl-1H-indole-3-carboxamide
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With dimethylaluminum chloride In hexane; dichloromethane at 0℃; Inert atmosphere; Stage #2: 1-Adamantanecarbonyl chloride In hexane; dichloromethane for 2h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
Stage #1: 6-methoxy-1-naphthoic acid With oxalyl dichloride In dichloromethane for 1h; Heating; Stage #2: 1-pentyl-1H-indole With ethylaluminum dichloride In toluene for 18h; Friedel-Crafts reaction; | 81% |
1-pentyl-1H-indole
bromodifluoroacetic acid
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 100℃; Friedel-Crafts Acylation; | 80% |
1-pentyl-1H-indole
benzoic acid hydrazide
Conditions | Yield |
---|---|
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; oxygen; tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 24h; Irradiation; regioselective reaction; | 80% |
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With dimethylaluminum chloride In hexane; dichloromethane at 0℃; for 0.5h; Friedel-Crafts reaction; Inert atmosphere; Stage #2: 8-bromo-1-naphthoyl chloride In hexane; dichloromethane at 0 - 20℃; Friedel-Crafts reaction; Inert atmosphere; | 78% |
1-pentyl-1H-indole
1,1'-dipentyl-1H,1'H-2,3'-biindole-3-carbonitrile
Conditions | Yield |
---|---|
With copper diacetate; palladium diacetate In dimethyl sulfoxide at 80℃; for 24h; Inert atmosphere; Sealed vial; regioselective reaction; | 77% |
Conditions | Yield |
---|---|
Stage #1: formaldehyd; dimethyl amine With acetic acid In water for 0.5h; Stage #2: 1-pentyl-1H-indole In dichloromethane; water for 16h; | 76% |
1-pentyl-1H-indole
3-Chlorobenzaldehyde
(3-chlorophenyl)(1-pentyl-1H-indol-3-yl)methanone
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; palladium diacetate In chlorobenzene at 140℃; for 24h; Inert atmosphere; Sealed tube; | 73% |
1-pentyl-1H-indole
4-biphenyl-carboxylic acid chloride
[1,1'-biphenyl]-4-yl(1-pentyl-1H-indol-3-yl)methanone
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With diethyl aluminiumcholoride In hexane; dichloromethane at -15℃; for 0.5h; Inert atmosphere; Stage #2: 4-biphenyl-carboxylic acid chloride In hexane; dichloromethane at -15 - 0℃; Friedel Crafts acylation; Inert atmosphere; | 72% |
1-pentyl-1H-indole
naphthalene-1-carbonic acid chloride
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With diethylaluminium chloride In hexane; dichloromethane at 0℃; for 1h; Stage #2: naphthalene-1-carbonic acid chloride In hexane; dichloromethane at 0℃; for 16h; | 72% |
1-pentyl-1H-indole
C20H18BrNO6S
1-pentyl-7-(phenylsulfonyl)-indolo[3,2-b]carbazole
Conditions | Yield |
---|---|
With zinc dibromide In 1,2-dichloro-ethane at 20℃; for 4h; Inert atmosphere; | 70% |
1-pentyl-1H-indole
Conditions | Yield |
---|---|
With 1-methyl-3-(4-sulfobutyl)-1H-imidazol-3-ium 4-methylbenzene-1-sulfonate In neat (no solvent) at 80℃; for 4h; | 67% |
Conditions | Yield |
---|---|
Stage #1: 7-methoxynaphthalene-1-carboxylic acid With oxalyl dichloride In dichloromethane for 1h; Heating; Stage #2: 1-pentyl-1H-indole With ethylaluminum dichloride In toluene for 18h; Friedel-Crafts reaction; | 66% |
1-pentyl-1H-indole
1-acetoxy-1,2-benziodoxol-3-one
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In dichloromethane at 20℃; | 60% |
Conditions | Yield |
---|---|
With zinc dibromide In 1,2-dichloro-ethane at 20℃; Inert atmosphere; Reflux; | 58% |
Conditions | Yield |
---|---|
With zinc dibromide In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere; | 55% |
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With dimethylaluminum chloride In hexane; dichloromethane at 0℃; for 0.5h; Friedel-Crafts reaction; Inert atmosphere; Stage #2: 4-bromo-1-naphthoic acid chloride In hexane; dichloromethane at 0 - 20℃; Friedel-Crafts reaction; Inert atmosphere; | 53% |
1-pentyl-1H-indole
1-adamantylacetyl chloride
2-(adamantan-1-yl)-1-(1-pentyl-1H-indol-3-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With dimethylaluminum chloride In hexane; dichloromethane at 0℃; Inert atmosphere; Stage #2: 1-adamantylacetyl chloride In hexane; dichloromethane for 2h; Inert atmosphere; | 35% |
Conditions | Yield |
---|---|
Stage #1: 1-pentyl-1H-indole With dimethylaluminum chloride In hexane; dichloromethane at 0℃; for 1h; Friedel-Crafts reaction; Inert atmosphere; Stage #2: C11H6Cl2O In hexane; dichloromethane at 0 - 20℃; for 6h; Friedel-Crafts reaction; Inert atmosphere; | 33% |
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