DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryItems Standard Result Appearance Colorless transpant liquid Colorless transpant liquid Content
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Cas:587-04-2
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inquiryChemical Name 3-Chlorobenzaldehyde CAS No. 587-04-2 Molecular Formula C7H5ClO Molecular Weight 140.56700 PSA 17.07000 LogP
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Cas:587-04-2
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Cas:587-04-2
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inquiryHigh Purity 3-ChlorobenzaldehydeAppearance:Colorless clear liquid Storage:Dissolved in water, dissolved in hot water. Package:according to customers' requirements Application:Synthetic material intermediates Transportation:By air(EMS or EUB or FedEx
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3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With Oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide In ethyl acetate at 20℃; for 24h; Reagent/catalyst; Solvent; | 99% |
With tert.-butylnitrite; oxygen; acetic acid In toluene at 50℃; for 1h; | 99% |
With tert.-butylhydroperoxide In toluene at 120℃; for 4h; | 98% |
Conditions | Yield |
---|---|
With samarium diiodide; phosphoric acid In tetrahydrofuran for 0.000833333h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With water; Sulfate; titanium(IV) oxide In benzene for 0.166667h; Deacetylation; Heating; | 98% |
With water; silica sulfate In benzene for 0.0166667h; Heating; | 98% |
With iron(II) sulfate In benzene for 0.5h; Heating; | 96% |
Conditions | Yield |
---|---|
Stage #1: formic acid; 3-iodochlorobenzene With palladium diacetate; acetic anhydride; tricyclohexylphosphine In N,N-dimethyl-formamide at 30℃; for 1h; Inert atmosphere; Green chemistry; Stage #2: With triethylamine In N,N-dimethyl-formamide at 80℃; for 6h; Inert atmosphere; Green chemistry; | 98% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 2h; Sealed tube; | 94% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; Inert atmosphere; Sealed tube; | 93% |
With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tricyclohexylphosphine In N,N-dimethyl-formamide at 60℃; for 10h; Inert atmosphere; Sealed tube; | 56% |
Conditions | Yield |
---|---|
With laccase at 20℃; Reagent/catalyst; Green chemistry; Enzymatic reaction; | 97% |
With dipotassium peroxodisulfate; iron(II) acetylacetonate In water; acetonitrile at 80℃; for 3h; Catalytic behavior; | 95% |
With laccase of Pleurotus ostreatus MTCC-1801; 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt In 1,4-dioxane at 20℃; pH=4.5; Enzymatic reaction; | 92% |
Conditions | Yield |
---|---|
With 1H-imidazole; sodium periodate; MnCl-TPP-(PEO750)4 In water; acetonitrile at 80℃; for 24h; | 96% |
With dihydrogen peroxide In water at 100℃; for 4h; | 90% |
With dihydrogen peroxide In water; acetonitrile at 20℃; for 8h; UV-irradiation; Sealed tube; Green chemistry; | 85% |
Conditions | Yield |
---|---|
With water; oxygen at 140℃; under 3800.26 Torr; for 10h; | A 92% B n/a |
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With copper(II) nitrate monohydrate at 90℃; for 0.0833333h; | 92% |
With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 1.5h; | 87% |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate In dichloromethane at 20℃; | 91% |
With sulfuric acid; quinolinium dichromate(VI) In acetic acid at 29.9℃; Rate constant; Thermodynamic data; ΔHact, ΔSact, ΔGact; var. concentration of reagents; |
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With clayfen (montmorillonite K-10, Fe(NO3)3*9H2O) for 0.0333333h; microwave irradiation; | 90% |
aluminum oxide; ammonium cerium(IV) nitrate for 0.0111111h; microwave irradiation; | 82% |
With bis(trimethylsilyl)chromate; Montmorillonite K10 for 0.0166667h; Solid phase reaction; Cleavage; microwave irradiation; | 80% |
m-Chlorobenzaldehyde 2,4-Dinitrophenylhydrazone
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With potassium ferrate for 0.133333h; microwave irradiation; | 90% |
With 1,4-dichloro-1,4-diazoniabicyclo[2,2,2]octane bischloride In water at 50℃; for 0.416667h; pH=7; | 86% |
3-chlorobenzyl acetate
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With methanol; potassium permanganate In ethyl acetate at 25℃; for 12h; | 90% |
Conditions | Yield |
---|---|
With bismuth(III) nitrate; tetrabutyl ammonium fluoride at 100℃; for 4.5h; | 89% |
With dihydrogen peroxide In ethanol for 10h; Heating; | 80% |
With hexamethylenetetramine In chloroform for 1h; Heating; | |
With potassium carbonate; dimethyl sulfoxide at 90℃; for 2h; Kornblum Aldehyd Synthesis; |
Conditions | Yield |
---|---|
With solid-phase supported silica chloride In methanol at 20℃; for 0.666667h; | 89% |
Conditions | Yield |
---|---|
With copper(l) iodide; oxygen In dimethyl sulfoxide at 120℃; for 13h; chemoselective reaction; | 89% |
2-(3-chlorophenyl)-1,3-dithiane
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With eosin y In water; acetonitrile at 20℃; for 3h; Irradiation; | 89% |
With water In 1,4-dioxane at 100℃; for 48h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With hydrogen bromide; dimethyl sulfoxide at 110℃; for 14h; | 88% |
With nitric acid In dichloromethane at 20℃; for 1h; | 78% |
With Cu(NO3)2-SiO2 In 2,2,4-trimethylpentane for 1h; Heating; Yield given; | |
With titanium(IV) oxide; silver sulfate In acetonitrile at 20℃; for 2h; UV-irradiation; |
Conditions | Yield |
---|---|
With oxygen; 1-butyl-3-methylimidazolium Tetrafluoroborate; copper(l) chloride; palladium dichloride In water at 60℃; for 24h; Wacker oxidation; | A n/a B 88% |
With [PdCl2(tBu-BINC)]; oxygen In N,N-dimethyl acetamide; water at 70℃; under 760.051 Torr; for 96h; Wacker oxidation; |
2-(3-chlorophenyl)-1,3-dithiolane
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With iodosylbenzene In dichloromethane at 20℃; for 0.5h; | 88% |
With sodium nitrate; sulfuric acid; silica gel In dichloromethane at 20℃; for 0.25h; | 85% |
m-chlorobenzyl alcohol
nitrobenzene
A
N-(3-chlorobenzylidene)aniline
B
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
With α,α,α-trifluorotoluene; titanium(IV) oxide In dodecane under 750.075 Torr; for 3h; Darkness; Inert atmosphere; Irradiation; | A 87.87% B n/a |
Conditions | Yield |
---|---|
Stage #1: m-aminobenzaldehyde With potassium nitrite at 6 - 10℃; for 1h; Stage #2: With iron phosphite; sodium carbonate; sodium bromide; sodium nitrite at 60 - 80℃; for 26h; Temperature; | 86% |
3-Chlorobenzaldehyde
1,2-bis(3-chlorophenyl)-1,2-ethanediol
Conditions | Yield |
---|---|
With aluminium; potassium hydroxide In methanol at 0℃; for 1h; Inert atmosphere; | 100% |
With sodium hydroxide; aluminium In methanol; water for 0.0833333h; pinacol coupling; microwave irradiation; | 94% |
With niobium pentachloride; zinc In 1,4-dioxane; toluene at 0℃; for 1.5h; | 87% |
Conditions | Yield |
---|---|
With cobalt(II) 2,9,16,23-phthalocyanine tetrasulfonic acid In water; acetonitrile at 20℃; under 760.051 Torr; for 150h; UV-irradiation; | 100% |
With sodium perborate In acetic acid for 1.5h; steam bath; | 95% |
With dihydrogen peroxide; 7-(trifluoromethyl)-1,10-ethyleneisoalloxazinium chloride In water; acetonitrile at 85℃; for 18h; | 94% |
2-benzoyl-1-cyano-1,2-dihydroisoquinoline
3-Chlorobenzaldehyde
benzoyloxy-(3-chloro-phenyl)-isoquinolin-1-yl-methane
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile for 0.0833333h; ultrasound sonication; | 100% |
ethyl acetoacetate
3-Chlorobenzaldehyde
2-acetyl-3-(3-chloro-phenyl)-acrylic acid ethyl ester
Conditions | Yield |
---|---|
With piperidine; acetic acid In toluene at 20 - 120℃; | 100% |
With piperidine; acetic acid In isopropyl alcohol at 20℃; for 24h; | 97% |
With piperidine; acetic acid In benzene for 1h; Heating; |
diethoxyphosphoryl-acetic acid ethyl ester
3-Chlorobenzaldehyde
ethyl (E)-3-(3-chlorophenyl)prop-2-enoate
Conditions | Yield |
---|---|
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran at 23℃; for 1h; Stage #2: m-Chlorobenzaldehyde In tetrahydrofuran for 1h; | 100% |
With sodium hydride In N,N-dimethyl-formamide at -60℃; Horner-Wadsworth-Emmons Olefination; | 95% |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 30℃; for 4h; Glovebox; | 84% |
3-Chlorobenzaldehyde
phenylazomalonamamidine hydrochloride
2,8-Bis-(3-chloro-phenyl)-1,7-dihydro-purin-6-one
Conditions | Yield |
---|---|
at 170℃; for 1h; | 100% |
cis, trans-1,3-dimethylaminocyclohexane
3-Chlorobenzaldehyde
C22H24Cl2N2
Conditions | Yield |
---|---|
In methanol at 20℃; Molecular sieve; | 100% |
In methanol at 20℃; Molecular sieve; |
2,6-dichloropyridine
3-Chlorobenzaldehyde
(3-chloro-phenyl)-(2,6-dichloro-pyridin-3-yl)-methanol
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloropyridine With n-butyllithium; diethylamine In tetrahydrofuran; hexane at -80℃; for 1.5h; Inert atmosphere; Stage #2: m-Chlorobenzaldehyde In tetrahydrofuran; hexane at -78 - 20℃; for 16h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: N-prenyl-N-propargyltosylamide With ethylmagnesium bromide In tetrahydrofuran at 50℃; for 1h; Stage #2: m-Chlorobenzaldehyde In tetrahydrofuran at 20℃; for 3h; | 100% |
Stage #1: N-prenyl-N-propargyltosylamide With ethylmagnesium bromide In tetrahydrofuran at 50℃; for 1h; Stage #2: m-Chlorobenzaldehyde In tetrahydrofuran at 20℃; for 3h; |
3-Chlorobenzaldehyde
C32H27ClN6O3
Conditions | Yield |
---|---|
With potassium hydroxide In N,N-dimethyl-formamide | 100% |
1,3-diaminoguanidine hydrochloride
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
In ethanol for 16h; Reflux; | 100% |
In ethanol for 16h; Reflux; |
3-Chlorobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: (E)-1-{4-[(4-acetyl-2-hydroxyphenyl)diazenyl]phenyl}ethanone; m-Chlorobenzaldehyde With sodium hydroxide In ethanol; water at 20℃; for 0.0833333h; Claisen-Schmidt Condensation; Stage #2: In ethanol; water for 0.166667h; Claisen-Schmidt Condensation; Microwave irradiation; | 100% |
Conditions | Yield |
---|---|
With 15T-22.4TO-S15-1123 at 59.84℃; for 6h; Mannich reaction; | 99.8% |
Conditions | Yield |
---|---|
Stage #1: m-Chlorobenzaldehyde; inden-1-one In ethanol for 0.0833333h; Inert atmosphere; Stage #2: With sodium hydroxide In ethanol; water for 0.5h; Inert atmosphere; | 99.7% |
Conditions | Yield |
---|---|
With piperidine In ethanol; water at 20℃; for 0.333333h; | 99.65% |
With silica gel; aniline; ytterbium(III) triflate at 20℃; for 0.0333333h; neat (no solvent, solid phase); | 87% |
3-Chlorobenzaldehyde
1,2-diamino-benzene
2-(3-chloro-phenyl)-1H-benzoimidazole
Conditions | Yield |
---|---|
With alumina-supported iron(III) chloride In N,N-dimethyl-formamide at 38 - 41℃; for 1.4h; Sonication; | 99.5% |
With manganese doped CdS nanoparticles In water at 90℃; for 1.5h; chemoselective reaction; | 97% |
With N-ethyl-pyridinium tetrafluoroborate at 50℃; for 0.333333h; Microwave irradiation; Green chemistry; | 97.2% |
Conditions | Yield |
---|---|
With sodium acetate In ethanol; water at 20℃; | 99.2% |
With sodium acetate In ethanol; water for 0.0194444h; Microwave irradiation; | 89.1% |
With acetic acid In ethanol Reflux; | 77% |
Conditions | Yield |
---|---|
With polystyrene-supported DABCO In methanol at 25℃; for 0.416667h; Knoevenagel Condensation; Green chemistry; | 99% |
With 1-hexyl-3-methylimidazolium 2-hydroxybenzoate In water at 20℃; for 0.0166667h; Knoevenagel Condensation; Sonication; | 99.17% |
With poly-N-methyl-4-vinylpyridinium hydroxide-SiO2-Al2O3 composite at 20℃; for 0.25h; Knoevenagel condensation; Neat (no solvent); | 98% |
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