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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Vigabatrin Manufacturer/High quality/Best price/In stock

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

VIGABATRIN CAS NO.60643-86-9

Cas:60643-86-9

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Vigabatrin

Cas:60643-86-9

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% Vigabatrin 60643-86-9 ISO Manufacturer

Cas:60643-86-9

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap

Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $5.0 / 10.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

CHemwill -- VIGABATRIN (4-Amino-5-hexenoic acid)

Cas:60643-86-9

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

High Purity Vigabatrin CAS 60643-86-9 Assay 98% with Best Price!

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

TIANFU CHEM-- VIGABATRIN

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 60643-86-9 with competitive price

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: Vigabatrin CAS:60643-86-9 MF: C6H11NO2 Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25kg Application:API Transportation:By sea or by air Port:Qingdao Port

Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Vigabatrin 60643-86-9

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

VIGABATRIN CAS:60643-86-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,

VIGABATRIN CAS:60643-86-9

Cas:60643-86-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Vigabatrin/ LIDE PHARMA- Factory supply / Best price

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

Vigabatrin CAS: 60643-86-9 Specification Test Item Standard: USP Identification IR spectrum similar to that of RS HPLC retention time similar to that of RS Related substance

Factory supply Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Vigabatrin

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

vigabatrin

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

VIGABATRIN

Cas:60643-86-9

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

CPP-109 Vigabatrin 60643-86-9

Cas:60643-86-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

vigabatrin

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Vigabatrin

Cas:60643-86-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Vigabatrin

Cas:60643-86-9

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: Vigabatrin CAS No.:60643-86-9 Molecule Formula:C6H11NO2 Molecule Weight:129.15 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality Vigabatrin(CAS:60643-86-9) in stock

Cas:60643-86-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Vigabatrin

Cas:60643-86-9

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

High Purity Vigabatrin

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

vigabatrin

Cas:60643-86-9

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

VIGABATRIN

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Vigabatrin

Cas:60643-86-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Vigabatrin

Cas:60643-86-9

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Synthetic route

5(S)-Vinyl-2-Pyrrolidinone
7529-16-0

5(S)-Vinyl-2-Pyrrolidinone

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Stage #1: 5(S)-Vinyl-2-Pyrrolidinone With potassium hydroxide In water for 2h; Reflux;
Stage #2: With acetic acid In water; isopropyl alcohol at 0 - 30℃; for 4.5h;
74%
Stage #1: 5(S)-Vinyl-2-Pyrrolidinone With water; potassium hydroxide In isopropyl alcohol at 20 - 60℃; for 16h; Inert atmosphere;
Stage #2: With acetic acid In water; isopropyl alcohol
60%
With water; potassium hydroxide at 90 - 100℃; for 3h; Reflux;
4-benzenesulphonamido 5-hexenoic acid
144085-15-4

4-benzenesulphonamido 5-hexenoic acid

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
With ammonia; sodium In tetrahydrofuran63%
vigabatrin hydrochloride

vigabatrin hydrochloride

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
With ammonium hydroxide; Dowex H(+)
4-(carbobenzyloxy)amino-5-hexenenitrile
440366-57-4

4-(carbobenzyloxy)amino-5-hexenenitrile

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
With diclazuril In water-d2 at 100℃;
5-bromo-3-(carbobenzyloxy)amino-1-pentene
440366-56-3

5-bromo-3-(carbobenzyloxy)amino-1-pentene

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 70 percent / tetrahydrofuran / 2 h / Heating
2: DCl / D2O / 100 °C
View Scheme
3-(carbobenzyloxy)amino-4-penten-1-ol
440366-55-2

3-(carbobenzyloxy)amino-4-penten-1-ol

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 89 percent / PPh3; CBr4 / CH2Cl2 / 1 h / 0 °C
2: 70 percent / tetrahydrofuran / 2 h / Heating
3: DCl / D2O / 100 °C
View Scheme
(E)-6-hydroxy-hex-4-enoic acid ethyl ester
66855-20-7

(E)-6-hydroxy-hex-4-enoic acid ethyl ester

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) ether, 0 deg C, 1 h; 2.) xylene, 48 h, reflux
2: 6N HCl / 12 h / Heating
3: Dowex H(+), 1N NH4OH
View Scheme
6-formyloxy-4-hexenoic acid ethyl ester

6-formyloxy-4-hexenoic acid ethyl ester

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: HCl gas / ethanol
2: 1.) NaH / 1.) ether, 0 deg C, 1 h; 2.) xylene, 48 h, reflux
3: 6N HCl / 12 h / Heating
4: Dowex H(+), 1N NH4OH
View Scheme
4-(2,2,2-Trichloro-acetylamino)-hex-5-enoic acid ethyl ester
149815-86-1

4-(2,2,2-Trichloro-acetylamino)-hex-5-enoic acid ethyl ester

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 6N HCl / 12 h / Heating
2: Dowex H(+), 1N NH4OH
View Scheme
ethyl hex-5-enoate
54653-25-7

ethyl hex-5-enoate

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 75 percent / diethyl ether / 40 h / Ambient temperature
2: 1.) hexamethyldisilazane, 2.) 0.2 N NaOH / 1.) dichloromethane, reflux, 24 h, 2.) 48 h
3: 72 percent / potassium hydroxide / H2O / 2 h / 100 °C
4: 63 percent / sodium, liquid ammonia / tetrahydrofuran
View Scheme
diethyl 2-(3-butenyl)malonate
31696-00-1

diethyl 2-(3-butenyl)malonate

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 85 percent / LiCl / dimethylsulfoxide
2: 75 percent / diethyl ether / 40 h / Ambient temperature
3: 1.) hexamethyldisilazane, 2.) 0.2 N NaOH / 1.) dichloromethane, reflux, 24 h, 2.) 48 h
4: 72 percent / potassium hydroxide / H2O / 2 h / 100 °C
5: 63 percent / sodium, liquid ammonia / tetrahydrofuran
View Scheme
4-Benzenesulfonylamino-hex-5-enoic acid ethyl ester
119703-95-6

4-Benzenesulfonylamino-hex-5-enoic acid ethyl ester

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 72 percent / potassium hydroxide / H2O / 2 h / 100 °C
2: 63 percent / sodium, liquid ammonia / tetrahydrofuran
View Scheme
C14H19NO5S2

C14H19NO5S2

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) hexamethyldisilazane, 2.) 0.2 N NaOH / 1.) dichloromethane, reflux, 24 h, 2.) 48 h
2: 72 percent / potassium hydroxide / H2O / 2 h / 100 °C
3: 63 percent / sodium, liquid ammonia / tetrahydrofuran
View Scheme
2-oxo-5-vinylpyrrolidine-3-amide

2-oxo-5-vinylpyrrolidine-3-amide

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
With hydrogenchloride; acetic acid In water for 8h; Reflux;
triisopropylsilyl 4-aminohex-5-enoate

triisopropylsilyl 4-aminohex-5-enoate

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

Conditions
ConditionsYield
With water; sodium methylate In methanol at 45℃; for 2h; Reagent/catalyst;176 g
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

5(S)-Vinyl-2-Pyrrolidinone
7529-16-0

5(S)-Vinyl-2-Pyrrolidinone

Conditions
ConditionsYield
at 180℃;95%
ethanol
64-17-5

ethanol

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-benzenesulphonamido 5-hexenoic acid
144085-15-4

4-benzenesulphonamido 5-hexenoic acid

Conditions
ConditionsYield
Stage #1: ethanol; 4-amino-5-hexenoic acid With thionyl chloride at 20℃; for 0.333333h; Esterification;
Stage #2: With ammonia In diethyl ether; water at 20℃; for 0.0333333h; Elimination;
93%
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
58632-95-4

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-tert-butoxycarbonylamino-hex-5-enoic acid
124099-19-0

4-tert-butoxycarbonylamino-hex-5-enoic acid

Conditions
ConditionsYield
With sodium hydrogencarbonate In 1,4-dioxane Acylation;92%
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-ethyl aminobutyric acid
5415-99-6

4-ethyl aminobutyric acid

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol; water at 20 - 30℃; under 3750.38 Torr; for 16h; Autoclave;90%
shikimic acid
138-59-0

shikimic acid

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

C13H19NO6

C13H19NO6

Conditions
ConditionsYield
Stage #1: shikimic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere;
Stage #2: 4-amino-5-hexenoic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 20℃; for 24h; Temperature; Inert atmosphere;
87.76%
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
58632-95-4

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-tert-butoxycarbonylamino-hex-5-enoic acid
124099-19-0

4-tert-butoxycarbonylamino-hex-5-enoic acid

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane at 20℃; for 3h;82.6%
ethanol
64-17-5

ethanol

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride
39637-99-5, 20445-33-4

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

ethyl N-<(2R)-2-methoxy-2-phenyl-3,3,3-trifluoropropionoyl>-(4S,4R)-4-amino-5-hexenoate

ethyl N-<(2R)-2-methoxy-2-phenyl-3,3,3-trifluoropropionoyl>-(4S,4R)-4-amino-5-hexenoate

Conditions
ConditionsYield
With hydrogenchloride; triethylamine 1.) 1 h, 25 degC; 2.) methylene chloride, 4 h, 25 degC; Yield given. Multistep reaction;
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

5-amino-6-hydroxy-3,4,5,6-tetrahydropyran-2-one

5-amino-6-hydroxy-3,4,5,6-tetrahydropyran-2-one

Conditions
ConditionsYield
With ozone In water-d2
formaldehyd
50-00-0

formaldehyd

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

acetylacetone
123-54-6

acetylacetone

4-(3,5-diacetyl-2,6-dimethyl-4H-pyridin-1-yl)-hex-5-enoic acid

4-(3,5-diacetyl-2,6-dimethyl-4H-pyridin-1-yl)-hex-5-enoic acid

Conditions
ConditionsYield
With sodium acetate In water at 100℃; for 0.3h; Hantzsch reaction;
ethanol
64-17-5

ethanol

(R)-methoxytrifluoromethylphenylacetyl chloride
20445-33-4, 39637-99-5

(R)-methoxytrifluoromethylphenylacetyl chloride

4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

A

(S)-4-((S)-2-methoxy-2-phenyl-3,3,3-trifluoropropionylamino)hex-5-enoic acid ethyl ester

(S)-4-((S)-2-methoxy-2-phenyl-3,3,3-trifluoropropionylamino)hex-5-enoic acid ethyl ester

B

(R)-4-((S)-2-methoxy-2-phenyl-3,3,3-trifluoropropionylamino)hex-5-enoic acid ethyl ester

(R)-4-((S)-2-methoxy-2-phenyl-3,3,3-trifluoropropionylamino)hex-5-enoic acid ethyl ester

Conditions
ConditionsYield
Stage #1: ethanol; 4-amino-5-hexenoic acid
Stage #2: (R)-methoxytrifluoromethylphenylacetyl chloride Title compound not separated from byproducts;
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-tert-butoxycarbonylamino-hex-5-enoic acid methyl ester
748816-92-4

4-tert-butoxycarbonylamino-hex-5-enoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2: 95 percent / NaHCO3 / dimethylformamide / 16 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(5-amino-hept-6-enoylamino)-butyric acid

4-(5-amino-hept-6-enoylamino)-butyric acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 50.1 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
3.1: 94 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C
4.1: 100 percent / aq. KOH / methanol / 48 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(4-amino-hex-5-enoylamino)-hex-5-enoic acid

4-(4-amino-hex-5-enoylamino)-hex-5-enoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 50.1 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
3.1: 100 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C
4.1: 100 percent / aq. KOH / methanol / 48 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(5-tert-butoxycarbonylamino-hept-6-enoylamino)-butyric acid methyl ester
748816-94-6

4-(5-tert-butoxycarbonylamino-hept-6-enoylamino)-butyric acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 50.1 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(4-tert-butoxycarbonylamino-hex-5-enoylamino)-hex-5-enoic acid methyl ester

4-(4-tert-butoxycarbonylamino-hex-5-enoylamino)-hex-5-enoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 59 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-amino-hex-5-enoic acid methyl ester trifluoroacetate

4-amino-hex-5-enoic acid methyl ester trifluoroacetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2: 95 percent / NaHCO3 / dimethylformamide / 16 h / 20 °C
3: 100 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(4-amino-hex-5-enoylamino)-butyric acid methyl ester; compound with trifluoro-acetic acid

4-(4-amino-hex-5-enoylamino)-butyric acid methyl ester; compound with trifluoro-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 50.1 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
3.1: 94 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

4-(4-amino-hex-5-enoylamino)-hex-5-enoic acid methyl ester; compound with trifluoro-acetic acid

4-(4-amino-hex-5-enoylamino)-hex-5-enoic acid methyl ester; compound with trifluoro-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 82.6 percent / aq. Et3N / dioxane / 3 h / 20 °C
2.1: HOBT; EDC / dimethylformamide / 0.67 h / 0 °C
2.2: 50.1 percent / diisopropylethylamine / dimethylformamide / 24 h / 20 °C
3.1: 100 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

1-(4-amino-hex-5-enoyl)-pyrrolidin-2-one

1-(4-amino-hex-5-enoyl)-pyrrolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 92 percent / aq. NaHCO3 / dioxane
2.1: TEA / tetrahydrofuran
3.1: nBuLi / tetrahydrofuran
3.2: 50 percent / TEA / tetrahydrofuran
4.1: 95 percent / TFA; DMS / CH2Cl2
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

1-(4-amino-hex-5-enoyl)-piperidine-4-carboxylic acid methyl ester

1-(4-amino-hex-5-enoyl)-piperidine-4-carboxylic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 92 percent / aq. NaHCO3 / dioxane
2: 68 percent / HOBt; EDCI
3: 96 percent / TFA; DMS / CH2Cl2
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

1-(4-amino-hex-5-enoyl)-piperidine-3-carboxylic acid methyl ester

1-(4-amino-hex-5-enoyl)-piperidine-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 92 percent / aq. NaHCO3 / dioxane
2: 73 percent / HOBt; EDCI
3: 94 percent / TFA; DMS / CH2Cl2
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

C16H27NO6

C16H27NO6

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 92 percent / aq. NaHCO3 / dioxane
2: TEA / tetrahydrofuran
View Scheme
4-amino-5-hexenoic acid
60643-86-9

4-amino-5-hexenoic acid

{1-[3-oxo-3-(2-oxo-pyrrolidin-1-yl)-propyl]-allyl}-carbamic acid tert-butyl ester
270905-52-7

{1-[3-oxo-3-(2-oxo-pyrrolidin-1-yl)-propyl]-allyl}-carbamic acid tert-butyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 92 percent / aq. NaHCO3 / dioxane
2.1: TEA / tetrahydrofuran
3.1: nBuLi / tetrahydrofuran
3.2: 50 percent / TEA / tetrahydrofuran
View Scheme

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