DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryProduct Name: 1,2-Bis(cyanomethyl)benzene Synonyms: 1,2-Bis(cyanomethyl)benzene, o-Xylylene dicyanide;Phthalic diacetonitrile;2,2'-(2,1-Phenylene)bisacetonitrile;2,2'-o-Phenylenebis(acetonitrile);o-Phenylenediacetonitrile;o-Phe
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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inquiry1,2-Bis(cyanomethyl)benzene CAS:613-73-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:1 Gram
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inquiry613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene Application:613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene
We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Pharm intermediate
1,2-Bis(cyanomethyl)benzene cas 613-73-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Cas:613-73-0
Min.Order:0
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inquiry613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzeneAppearance:white powder Storage:Normal temperature Package:Woven bag Application:Benzene derivates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount
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Conditions | Yield |
---|---|
for 3h; Irradiation; | 0.05% |
tetraethylammoniumcyanide
α,α'-dibromo-o-xylene
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
In dichloromethane |
Conditions | Yield |
---|---|
With ethanol; water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bromine / water / UV-irradiation 2: ethanol; water / 2 h / Reflux View Scheme |
Conditions | Yield |
---|---|
In ethanol; water for 2h; Reflux; |
N-cyanomorpholine
1,2-phenylenediacetonitrile
2-morpholino-9H-indeno[2,1-d]pyrimidin-4-amine
Conditions | Yield |
---|---|
With potassium tert-butylate In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 2h; Inert atmosphere; | 96% |
1,10-phenanthroline-5,6-dione
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 20℃; for 36h; Condensation; | 90% |
bis(acetonitrile)diiodotricarbonyltungsten(II)
1,2-phenylenediacetonitrile
triphenylphosphine
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of PPh3, 1 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 89% |
Conditions | Yield |
---|---|
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of PPh3, 1 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 86% |
bis(acetonitrile)diiodotricarbonyltungsten(II)
triphenyl-arsane
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of AsPh3, 3 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 85% |
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
In dichloromethane ligand was added to soln. of W-complex in CH2Cl2, stirred for 20 h in Schlenk apparatus; filtered, vol. was reduced in vacuo, layered with Et2O, cooled to -17°C for 5 ds; elem. anal.; | 85% |
ethanol
1,2-phenylenediacetonitrile
ethyl 2-[2-(2-ethoxy-2-oxoethyl)phenyl]acetate
Conditions | Yield |
---|---|
With sulfuric acid for 7h; Heating; | 84% |
With sulfuric acid for 7h; Heating; | 73% |
With sulfuric acid for 6h; Heating / reflux; | 70.6% |
1,4-di-tert-butyl-1,4-diazabutadiene
1,2-phenylenediacetonitrile
A
naphthalene-1,4-dicarbonitrile
B
tert-butylamine
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 120℃; for 1h; | A 82% B n/a |
N,N'-Bis(2,4-dimethylphenyl)glyoxaldiimin
1,2-phenylenediacetonitrile
A
naphthalene-1,4-dicarbonitrile
B
2,4-Xylidine
Conditions | Yield |
---|---|
With potassium hydroxide In N,N-dimethyl acetamide at 20℃; for 15h; Mechanism; var. glyoxaldiimines; | A 82% B n/a |
With potassium hydroxide In N,N-dimethyl acetamide at 20℃; for 15h; | A 82% B n/a |
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of POPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 82% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of AsPh3, 3 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 80% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of SbPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 80% |
1,2-phenylenediacetonitrile
3,6-dibromo-phenanthrene-9,10-dione
Conditions | Yield |
---|---|
With sodium methylate In methanol; N,N-dimethyl-formamide at 20℃; | 80% |
Conditions | Yield |
---|---|
Stage #1: 1,2-phenylenediacetonitrile With acetamide; acetic acid at 50℃; under 760.051 Torr; for 0.5h; Stage #2: With tetrakis(acetonitrile)palladium(II) tetrafluoroborate at 50℃; under 1 - 3 Torr; for 2h; | 79% |
With sulfuric acid |
ethanol
1,2-phenylenediacetonitrile
2-Amino-3-ethyl-3H-indene-1-carbonitrile
Conditions | Yield |
---|---|
rhodium(III) chloride; sodium carbonate; triphenylphosphine for 24h; Heating; | 78% |
1,2-phenylenediacetonitrile
2-amino-1H-indene-1-carbonitrile
Conditions | Yield |
---|---|
With carbonylhydridotris(triphenylphosphine)iridium(I) In tetrahydrofuran at 30℃; for 12h; | 76% |
With ethanol; sodium ethanolate |
bis(acetonitrile)diiodotricarbonyltungsten(II)
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; 1h, room temp., molar ratio: 1:2; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 75% |
triphenyl phosphite
bis(acetonitrile)diiodotricarbonyltungsten(II)
1,2-phenylenediacetonitrile
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; addn. of POPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 73% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: NCCH3; 1h, room temp., molar ratio: 1:2; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.; | 72% |
di(tert-butyl)chlorophosphine
1,2-phenylenediacetonitrile
N-[2,2-di-tert-butyl-2λ5-indeno[1,2-d][1,2]azaphosphol-3(8H)-ylidene]-P,P-di-tert-butylphosphinous amide
Conditions | Yield |
---|---|
Stage #1: 1,2-phenylenediacetonitrile With sodium hydride In tetrahydrofuran Inert atmosphere; Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran Inert atmosphere; | 70% |
N-methyl-acetamide
1,2-phenylenediacetonitrile
naphthalene-1,4-dicarbonitrile
Conditions | Yield |
---|---|
68.5% |
9,10-dioxo-9,10-dihydrophenanthrene-3-carboxylic acid
1,2-phenylenediacetonitrile
9,14-dicyanobenzo[b]triphenylene-3-carboxylic acid
Conditions | Yield |
---|---|
With sodium methylate In methanol; N,N-dimethyl-formamide at 40℃; for 6h; | 68% |
N1,N2-bis(o-tolyl)ethane-1,2-diimine
1,2-phenylenediacetonitrile
A
naphthalene-1,4-dicarbonitrile
B
o-toluidine
Conditions | Yield |
---|---|
With sodium methylate In N,N-dimethyl acetamide at 25℃; for 15h; | A 67% B n/a |
1,2-phenylenediacetonitrile
A
2-Cyanmethyl-phenylessigsaeure
B
o-xylylenediamide
Conditions | Yield |
---|---|
With water for 24h; Rhodococcus rhodochrous AJ270; | A 11% B 65% |
Conditions | Yield |
---|---|
With potassium phosphate buffer; Rhodococcus sp. AJ270 at 30℃; for 24h; | A 65% B 11% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide | 63% |
1,2-phenylenediacetonitrile
4,5,6,7-tetrahydrocyclobuta[b]naphthalene-1,2-dione
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 0.0833333h; Condensation; Heating; | 62% |
Conditions | Yield |
---|---|
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere; | 62% |
Conditions | Yield |
---|---|
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere; | 62% |
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