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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply o-phenylenediacetonitrile

Cas:613-73-0

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,2-Phenylenediacetonitrile

Cas:613-73-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: 1,2-Bis(cyanomethyl)benzene Synonyms: 1,2-Bis(cyanomethyl)benzene, o-Xylylene dicyanide;Phthalic diacetonitrile;2,2'-(2,1-Phenylene)bisacetonitrile;2,2'-o-Phenylenebis(acetonitrile);o-Phenylenediacetonitrile;o-Phe

613-73-0 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Kilogram

FOB Price: $8900.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 613-73-0 with competitive price

Cas:613-73-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

1,2-Bis(cyanomethyl)benzene CAS:613-73-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic

1,2-Bis(cyanomethyl)benzene CAS:613-73-0

Cas:613-73-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:613-73-0

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Kilogram

FOB Price: $30.0 / 50.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

2-[2-(cyanomethyl)phenyl]acetonitrile

Cas:613-73-0

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

o-Phenylenediacetonitrile

Cas:613-73-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,2-Bis(cyanomethyl)benzene Cas no.613-73-0 98%

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

o-Phenylenediacetonitrile

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

o-Xylylene Dicyanide

Cas:613-73-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene Application:613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Other

inquiry

HANGZHOU TIANYE CHEMICALS CO., LTD.

We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Pharm intermediate

o-Phenylenediacetonitrile

Cas:613-73-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

1,2-Bis(cyanomethyl)benzene cas 613-73-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

1,2-Bis(cyanomethyl)benzene cas 613-73-0

Cas:613-73-0

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzeneAppearance:white powder Storage:Normal temperature Package:Woven bag Application:Benzene derivates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount

613-73-0 C10H8N2 1,2-Bis(cyanomethyl)benzene

Cas:613-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,2-Phenylenediacetonitrile

Cas:613-73-0

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

phenylacetonitrile
140-29-4

phenylacetonitrile

acetonitrile
75-05-8

acetonitrile

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Conditions
ConditionsYield
for 3h; Irradiation;0.05%
2-methylbenzyl bromide
89-92-9

2-methylbenzyl bromide

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

tetraethylammoniumcyanide
13435-20-6

tetraethylammoniumcyanide

α,α'-dibromo-o-xylene
91-13-4

α,α'-dibromo-o-xylene

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Conditions
ConditionsYield
In dichloromethane
potassium cyanide
151-50-8

potassium cyanide

α,α'-dibromo-o-xylene
91-13-4

α,α'-dibromo-o-xylene

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

potassium cyanide
151-50-8

potassium cyanide

o-xylylene dibromide

o-xylylene dibromide

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Conditions
ConditionsYield
With ethanol; water
o-xylene
95-47-6

o-xylene

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bromine / water / UV-irradiation
2: ethanol; water / 2 h / Reflux
View Scheme
sodium cyanide
773837-37-9

sodium cyanide

α,α'-dibromo-o-xylene
91-13-4

α,α'-dibromo-o-xylene

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Conditions
ConditionsYield
In ethanol; water for 2h; Reflux;
N-cyanomorpholine
1530-89-8

N-cyanomorpholine

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

2-morpholino-9H-indeno[2,1-d]pyrimidin-4-amine
1616963-14-4

2-morpholino-9H-indeno[2,1-d]pyrimidin-4-amine

Conditions
ConditionsYield
With potassium tert-butylate In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 2h; Inert atmosphere;96%
1,10-phenanthroline-5,6-dione
27318-90-7

1,10-phenanthroline-5,6-dione

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

Naphtho[2,3-f][1,ω]phenanthroline-9,14-dicarbonitrile

Naphtho[2,3-f][1,ω]phenanthroline-9,14-dicarbonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol at 20℃; for 36h; Condensation;90%
bis(acetonitrile)diiodotricarbonyltungsten(II)
113350-36-0, 102382-37-6

bis(acetonitrile)diiodotricarbonyltungsten(II)

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

triphenylphosphine
603-35-0

triphenylphosphine

[WI2(CO)3(C6H4(CH2CN)2)(P(C6H5)3)]

[WI2(CO)3(C6H4(CH2CN)2)(P(C6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of PPh3, 1 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;89%
C36H22O2

C36H22O2

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

C46H26N2

C46H26N2

Conditions
ConditionsYield
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere;88%
MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

triphenylphosphine
603-35-0

triphenylphosphine

[MoI2(CO)3(C6H4(CH2CN)2)(P(C6H5)3)]

[MoI2(CO)3(C6H4(CH2CN)2)(P(C6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of PPh3, 1 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;86%
bis(acetonitrile)diiodotricarbonyltungsten(II)
113350-36-0, 102382-37-6

bis(acetonitrile)diiodotricarbonyltungsten(II)

triphenyl-arsane
603-32-7

triphenyl-arsane

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[WI2(CO)3(C6H4(CH2CN)2)(As(C6H5)3)]

[WI2(CO)3(C6H4(CH2CN)2)(As(C6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of AsPh3, 3 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;85%
[WI(CO)(NCMe)(P(OiPr)3)2(η2-MeC2Me)][BPh4]

[WI(CO)(NCMe)(P(OiPr)3)2(η2-MeC2Me)][BPh4]

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[WI(CO)(1,2-C6H4(NCCH2)2)(P(OiPr)3)2(η2-MeC2Me)][BPh4]

[WI(CO)(1,2-C6H4(NCCH2)2)(P(OiPr)3)2(η2-MeC2Me)][BPh4]

Conditions
ConditionsYield
In dichloromethane ligand was added to soln. of W-complex in CH2Cl2, stirred for 20 h in Schlenk apparatus; filtered, vol. was reduced in vacuo, layered with Et2O, cooled to -17°C for 5 ds; elem. anal.;85%
ethanol
64-17-5

ethanol

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

ethyl 2-[2-(2-ethoxy-2-oxoethyl)phenyl]acetate
17532-66-0

ethyl 2-[2-(2-ethoxy-2-oxoethyl)phenyl]acetate

Conditions
ConditionsYield
With sulfuric acid for 7h; Heating;84%
With sulfuric acid for 7h; Heating;73%
With sulfuric acid for 6h; Heating / reflux;70.6%
1,4-di-tert-butyl-1,4-diazabutadiene
28227-42-1, 30834-74-3

1,4-di-tert-butyl-1,4-diazabutadiene

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

A

naphthalene-1,4-dicarbonitrile
3029-30-9

naphthalene-1,4-dicarbonitrile

B

tert-butylamine
75-64-9

tert-butylamine

Conditions
ConditionsYield
In dimethyl sulfoxide at 120℃; for 1h;A 82%
B n/a
N,N'-Bis(2,4-dimethylphenyl)glyoxaldiimin
76509-14-3

N,N'-Bis(2,4-dimethylphenyl)glyoxaldiimin

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

A

naphthalene-1,4-dicarbonitrile
3029-30-9

naphthalene-1,4-dicarbonitrile

B

2,4-Xylidine
95-68-1

2,4-Xylidine

Conditions
ConditionsYield
With potassium hydroxide In N,N-dimethyl acetamide at 20℃; for 15h; Mechanism; var. glyoxaldiimines;A 82%
B n/a
With potassium hydroxide In N,N-dimethyl acetamide at 20℃; for 15h;A 82%
B n/a
triphenyl phosphite
101-02-0

triphenyl phosphite

MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[MoI2(CO)3(C6H4(CH2CN)2)(P(OC6H5)3)]

[MoI2(CO)3(C6H4(CH2CN)2)(P(OC6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of POPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;82%
MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

triphenyl-arsane
603-32-7

triphenyl-arsane

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[MoI2(CO)3(C6H4(CH2CN)2)(As(C6H5)3)]

[MoI2(CO)3(C6H4(CH2CN)2)(As(C6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of AsPh3, 3 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;80%
MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

triphenylantimony
603-36-1

triphenylantimony

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[MoI2(CO)3(C6H4(CH2CN)2)(Sb(C6H5)3)]

[MoI2(CO)3(C6H4(CH2CN)2)(Sb(C6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of SbPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;80%
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromo-9,14-dicyanobenzo[f]tetraphene

3,6-dibromo-9,14-dicyanobenzo[f]tetraphene

Conditions
ConditionsYield
With sodium methylate In methanol; N,N-dimethyl-formamide at 20℃;80%
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

o-xylylenediamide
7500-54-1

o-xylylenediamide

Conditions
ConditionsYield
Stage #1: 1,2-phenylenediacetonitrile With acetamide; acetic acid at 50℃; under 760.051 Torr; for 0.5h;
Stage #2: With tetrakis(acetonitrile)palladium(II) tetrafluoroborate at 50℃; under 1 - 3 Torr; for 2h;
79%
With sulfuric acid
ethanol
64-17-5

ethanol

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

2-Amino-3-ethyl-3H-indene-1-carbonitrile
80900-31-8

2-Amino-3-ethyl-3H-indene-1-carbonitrile

Conditions
ConditionsYield
rhodium(III) chloride; sodium carbonate; triphenylphosphine for 24h; Heating;78%
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

2-amino-1H-indene-1-carbonitrile
189242-48-6

2-amino-1H-indene-1-carbonitrile

Conditions
ConditionsYield
With carbonylhydridotris(triphenylphosphine)iridium(I) In tetrahydrofuran at 30℃; for 12h;76%
With ethanol; sodium ethanolate
bis(acetonitrile)diiodotricarbonyltungsten(II)
113350-36-0, 102382-37-6

bis(acetonitrile)diiodotricarbonyltungsten(II)

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[WI2(CO)3(C6H4(CH2CN)2)2]

[WI2(CO)3(C6H4(CH2CN)2)2]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; 1h, room temp., molar ratio: 1:2; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;75%
triphenyl phosphite
101-02-0

triphenyl phosphite

bis(acetonitrile)diiodotricarbonyltungsten(II)
113350-36-0, 102382-37-6

bis(acetonitrile)diiodotricarbonyltungsten(II)

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[WI2(CO)3(C6H4(CH2CN)2)(P(OC6H5)3)]

[WI2(CO)3(C6H4(CH2CN)2)(P(OC6H5)3)]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; addn. of POPh3, 5 min. stirring, addn. of 1,2-C6H4(CH2CN)2, 1 h, room temp., molar ratio: 1:1:1; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;73%
MoI2(CO)3(MeCN)2
102349-56-4

MoI2(CO)3(MeCN)2

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

[MoI2(CO)3(C6H4(CH2CN)2)2]

[MoI2(CO)3(C6H4(CH2CN)2)2]

Conditions
ConditionsYield
In dichloromethane byproducts: NCCH3; 1h, room temp., molar ratio: 1:2; filtration, vac. evapn., recrystn.(CH2CL2-Et2O), elem. anal.;72%
di(tert-butyl)chlorophosphine
13716-10-4

di(tert-butyl)chlorophosphine

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

N-[2,2-di-tert-butyl-2λ5-indeno[1,2-d][1,2]azaphosphol-3(8H)-ylidene]-P,P-di-tert-butylphosphinous amide
1395070-51-5

N-[2,2-di-tert-butyl-2λ5-indeno[1,2-d][1,2]azaphosphol-3(8H)-ylidene]-P,P-di-tert-butylphosphinous amide

Conditions
ConditionsYield
Stage #1: 1,2-phenylenediacetonitrile With sodium hydride In tetrahydrofuran Inert atmosphere;
Stage #2: di(tert-butyl)chlorophosphine In tetrahydrofuran Inert atmosphere;
70%
N-methyl-acetamide
79-16-3

N-methyl-acetamide

N-(tertiary)-butylamine-glyoxalbisaldimine

N-(tertiary)-butylamine-glyoxalbisaldimine

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

naphthalene-1,4-dicarbonitrile
3029-30-9

naphthalene-1,4-dicarbonitrile

Conditions
ConditionsYield
68.5%
9,10-dioxo-9,10-dihydrophenanthrene-3-carboxylic acid
32155-34-3

9,10-dioxo-9,10-dihydrophenanthrene-3-carboxylic acid

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

9,14-dicyanobenzo[b]triphenylene-3-carboxylic acid
1185274-48-9

9,14-dicyanobenzo[b]triphenylene-3-carboxylic acid

Conditions
ConditionsYield
With sodium methylate In methanol; N,N-dimethyl-formamide at 40℃; for 6h;68%
N1,N2-bis(o-tolyl)ethane-1,2-diimine
51479-97-1

N1,N2-bis(o-tolyl)ethane-1,2-diimine

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

A

naphthalene-1,4-dicarbonitrile
3029-30-9

naphthalene-1,4-dicarbonitrile

B

o-toluidine
95-53-4

o-toluidine

Conditions
ConditionsYield
With sodium methylate In N,N-dimethyl acetamide at 25℃; for 15h;A 67%
B n/a
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

A

2-Cyanmethyl-phenylessigsaeure
56066-94-5

2-Cyanmethyl-phenylessigsaeure

B

o-xylylenediamide
7500-54-1

o-xylylenediamide

Conditions
ConditionsYield
With water for 24h; Rhodococcus rhodochrous AJ270;A 11%
B 65%
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

A

o-xylylenediamide
7500-54-1

o-xylylenediamide

B

2-(2-Cyanomethyl-phenyl)-acetamide

2-(2-Cyanomethyl-phenyl)-acetamide

Conditions
ConditionsYield
With potassium phosphate buffer; Rhodococcus sp. AJ270 at 30℃; for 24h;A 65%
B 11%
N-o-toluidine-glyoxalbisaldimine

N-o-toluidine-glyoxalbisaldimine

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

naphthalene-1,4-dicarbonitrile
3029-30-9

naphthalene-1,4-dicarbonitrile

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide63%
1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

4,5,6,7-tetrahydrocyclobuta[b]naphthalene-1,2-dione
273733-05-4

4,5,6,7-tetrahydrocyclobuta[b]naphthalene-1,2-dione

7,8,9,10-tetrahydrodibenzo[b,h]biphenylene-5,12-dicarbonitrile

7,8,9,10-tetrahydrodibenzo[b,h]biphenylene-5,12-dicarbonitrile

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 0.0833333h; Condensation; Heating;62%
C36H20O4

C36H20O4

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

C56H28N4

C56H28N4

Conditions
ConditionsYield
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere;62%
C36H20O4

C36H20O4

1,2-phenylenediacetonitrile
613-73-0

1,2-phenylenediacetonitrile

C56H28N4

C56H28N4

Conditions
ConditionsYield
With sodium methylate In methanol; N,N-dimethyl-formamide at 35℃; for 8h; Inert atmosphere;62%

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