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inquiryHigh purity CAS 635-22-3 4-Chloro-3-nitroaniline in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Flu
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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4-Chloro-3-nitroaniline cas 635-22-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:ochre powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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Conditions | Yield |
---|---|
With isopropyl alcohol; potassium hydroxide for 0.166667h; Microwave irradiation; regioselective reaction; | 98% |
With isopropyl alcohol; potassium hydroxide for 0.366667h; Microwave irradiation; chemoselective reaction; | 95% |
With potassium hydroxide; nickel-incorporated hexagonal mesoporous aluminophosphate In isopropyl alcohol at 82.84℃; for 3h; | 88% |
Conditions | Yield |
---|---|
With sodium nitrate; sulfuric acid at 0 - 5℃; for 3h; | 94% |
With sulfuric acid; guanidine nitrate at 0 - 5℃; for 1h; | 75% |
With sulfuric acid; nitric acid | |
durch Nitrierung; |
di-tert-butyl dicarbonate
1-azido-3-nitro-4-chlorobenzene
A
4-Chloro-3-nitroaniline
Conditions | Yield |
---|---|
With Decaborane; palladium on activated charcoal In methanol at 20℃; for 3h; | A 68% B 30% |
Conditions | Yield |
---|---|
With hydrogen; iron; acetic acid; palladium dichloride In ethanol at 20 - 25℃; under 258.6 - 2327.2 Torr; | A n/a B 61% |
With benzophenone; triethylamine In isopropyl alcohol for 2h; Product distribution; Irradiation; | A 18% B n/a |
With hydrogenchloride; ethanol; tin(ll) chloride |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at -20℃; |
chloroform
acetic acid-(2,4,N-trichloro-anilide)
3-nitro-aniline
4-Chloro-3-nitroaniline
acetic acid-(2,4,N-trichloro-anilide)
3-nitro-aniline
4-Chloro-3-nitroaniline
Conditions | Yield |
---|---|
With chloroform |
sulfuric acid
nitric acid
4-chloro-aniline
4-Chloro-3-nitroaniline
Conditions | Yield |
---|---|
Electrolysis; |
Conditions | Yield |
---|---|
Electrolysis; |
hydrogenchloride
1-chloro-2,4-dinitro-benzene
A
4-Chloro-3-nitroaniline
B
2-chloro-6-nitroaniline
methanol
chlorine
3-nitro-aniline
A
4-Chloro-3-nitroaniline
B
2,4,6-trichloro-3-nitro-aniline
C
2-nitro-4-amino-1,5-dichlorobenzene
acetic acid
3-nitro-aniline
A
4-Chloro-3-nitroaniline
B
2,4,6-trichloro-3-nitro-aniline
C
2,6-dichloro-3-nitroaniline
D
2,4-dichloro-3-nitroaniline
sulfuric acid
nitric acid
4-chloro-aniline
A
4-Chloro-3-nitroaniline
B
4-Chloro-2-nitroaniline
Conditions | Yield |
---|---|
at -20℃; |
Conditions | Yield |
---|---|
With calcium hypochlorite; acetic acid at 40 - 60℃; |
1-chloro-2,4-dinitro-benzene
A
4-Chloro-3-nitroaniline
B
4-chloro-1,3-phenylenediamine
C
H2NC6H3(Cl)NO2
D
m-phenylenediamine
Conditions | Yield |
---|---|
With hydrogen; Pt/γ-Fe2O3 nanocomposite In methanol at 29.84℃; under 75.0075 Torr; Product distribution; |
Conditions | Yield |
---|---|
With acetic anhydride In diethyl ether; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran | 100% |
With acetic anhydride In diethyl ether; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran | 96% |
Acetylieren; |
4-Chloro-3-nitroaniline
3-chloro-3-oxopropanoic acid methyl ester
N-(4-chloro-3-nitro-phenyl)-malonamic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
4-Chloro-3-nitroaniline
3-(Trifluoromethyl)benzoyl chloride
N-(4-chloro-3-nitrophenyl)-3-(trifluoromethyl)benzamide
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; for 6h; | 100% |
4-Chloro-3-nitroaniline
cyclohexanylcarbonyl chloride
N-(4-chloro-3-nitrophenyl)cyclohexanecarboxamide
Conditions | Yield |
---|---|
Stage #1: 4-Chloro-3-nitroaniline; cyclohexanylcarbonyl chloride With pyridine In dichloromethane at 20℃; for 18h; Stage #2: With hydrogenchloride In dichloromethane; water | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-Chloro-3-nitroaniline; Cyclobutanecarbonyl chloride With pyridine In dichloromethane at 0 - 20℃; for 1h; Stage #2: With potassium carbonate In methanol; water Stage #3: With hydrogen; Raney nickel In methanol under 760.051 Torr; for 18h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-Chloro-3-nitroaniline; Cyclobutanecarbonyl chloride With pyridine In dichloromethane at 0 - 20℃; for 1h; Stage #2: With potassium carbonate In methanol; water for 0.5h; | 100% |
With pyridine In dichloromethane at 0 - 20℃; for 1h; |
formaldehyd
4-Chloro-3-nitroaniline
sodium methylate
(4-Chloro-3-nitro-phenyl)-methoxymethyl-amine
Conditions | Yield |
---|---|
97% |
4-Chloro-3-nitroaniline
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
In ethanol at 50℃; for 72h; | 96% |
In tetrahydrofuran for 12h; Reflux; | 78% |
In tetrahydrofuran for 20h; Reflux; | 78% |
Conditions | Yield |
---|---|
With D-galacturonic acid; potassium carbonate; copper(I) bromide In water; dimethyl sulfoxide at 80 - 100℃; Inert atmosphere; Green chemistry; | 96% |
4-Chloro-3-nitroaniline
acetic anhydride
N-(4-chloro-3-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With nickel dichloride at 20℃; for 0.166667h; Neat (no solvent); | 95% |
With sulfuric acid for 2h; Heating; | 81% |
In dichloromethane at 20℃; for 2h; | 80% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 95% |
With triethylamine In dichloromethane at 20℃; | |
With triethylamine In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In water at 20℃; for 0.0333333h; Catalytic behavior; | 95% |
With sodium tetrahydroborate In water at 20℃; for 0.5h; chemoselective reaction; | 91% |
With sodium tetrahydroborate; water; nickel at 20℃; for 2.5h; | 90% |
With hydrogen In ethanol at 80℃; under 15001.5 Torr; for 7h; Catalytic behavior; chemoselective reaction; |
thiophene-2-carbaldehyde
2-acetyl-5-chlorothiophene
4-Chloro-3-nitroaniline
C17H12Cl2N2O3S2
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 94.2% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 94.1% |
4-Chloro-3-nitroaniline
sodium methansulfinate
Conditions | Yield |
---|---|
Stage #1: 4-Chloro-3-nitroaniline With tetrafluoroboric acid; sodium nitrite In water at 0℃; for 1.08333h; Stage #2: sodium methansulfinate In dichloromethane at 0 - 20℃; | 94% |
Stage #1: 4-Chloro-3-nitroaniline With tetrafluoroboric acid In water for 0.25h; Stage #2: With sodium nitrite In water at 0℃; for 0.5h; Stage #3: sodium methansulfinate In dichloromethane at 0 - 20℃; |
thiophene-2-carbaldehyde
2-Acetyl-5-bromothiophene
4-Chloro-3-nitroaniline
C17H12BrClN2O3S2
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 92.6% |
4-Chloro-3-nitroaniline
methanesulfonyl chloride
N-(4-chloro-3-nitrophenyl)methanesulfonamide
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran for 24h; | 92% |
With pyridine In tetrahydrofuran for 24h; | 92% |
With pyridine for 4h; Ambient temperature; | |
With pyridine In tetrahydrofuran at 20℃; for 12h; |
Conditions | Yield |
---|---|
In toluene for 3h; Heating; | 92% |
With triethylamine In dichloromethane at 0 - 20℃; | 80% |
With triethylamine In dichloromethane at 0 - 20℃; | 80% |
With triethylamine In dichloromethane at 0 - 20℃; for 20h; | |
With triethylamine In ethanol at 0 - 90℃; for 3h; |
4-Chloro-3-nitroaniline
4-sulfanylphenol
4-(4-amino-2-nitro-phenylsulfanyl)-phenol
Conditions | Yield |
---|---|
With caesium carbonate In dimethyl sulfoxide at 100℃; for 16h; | 92% |
With potassium carbonate In ethanol for 6h; Heating; | 5% |
4-Chloro-3-nitroaniline
1-(4-fluorophenyl)ethanone
benzaldehyde
C21H16ClFN2O3
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 91.5% |
2-Acetyl-5-bromothiophene
4-Chloro-3-nitroaniline
benzaldehyde
C19H14BrClN2O3S
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 91% |
4-Chloro-3-nitroaniline
4-(pyridin-4-yl)benzaldehyde
triethyl phosphite
diethyl (4-chloro-3-nitrophenylamino)(4-(pyridine-4-yl)phenyl)methylphosphonate
Conditions | Yield |
---|---|
With poly(ethylene glycol)sulfonic acid In toluene at 40 - 50℃; for 2.5h; Kabachnik-Fields reaction; | 91% |
4-Chloro-3-nitroaniline
Conditions | Yield |
---|---|
In ethanol at 80℃; for 2h; | 91% |
In ethanol at 80℃; for 2h; |
4-Chloro-3-nitroaniline
thiophene-2-carbonyl isothiocyanate
Conditions | Yield |
---|---|
at 27℃; for 2h; | 91% |
furfural
2-Acetyl-5-bromothiophene
4-Chloro-3-nitroaniline
C17H12BrClN2O4S
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 90% |
furfural
4-Chloro-3-nitroaniline
1-(4-fluorophenyl)ethanone
C19H14ClFN2O4
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 0 - 50℃; Mannich reaction; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dihydro-1,4-benzodioxin-6-carboxylic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: 4-Chloro-3-nitroaniline With pyridine In dichloromethane at 20℃; for 3h; | 90% |
Conditions | Yield |
---|---|
Stage #1: potassium thioacyanate; acetyl chloride In water; acetone for 3h; Stage #2: 4-Chloro-3-nitroaniline In water; acetone for 5h; Reflux; | 90% |
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