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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
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inquiryProduct website: http://www.finerchem.com/pro01en/id/826.html Product Name 3-Chlorophenylboronic acid CAS No. 63503-60-6 Appearance
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inquiry3-Chlorophenylboronic acid CAS No.:63503-60-6 Name: 3-Chlorophenylboronic acid Molecular Structure Molecular Formula: C6H6BClO2
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inquiry3-Chlorophenylboronic acid Basic information Product Name: 3-Chlorophenylboronic acid Synonyms: RARECHEM AH PB 0179;M-CHLOROPHENYLBORONIC ACID;AKOS BRN-0010;3-CHLOROPHENYLBORNIC ACID;3-C
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inquiryName: 3-Chlorophenylboronic acid Synonyms: 3-Chloro benzene boronic acid CAS:63503-60-6 MF: C6H6BClO2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Syntheses Material Intermediat
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
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inquiry3-Chlorophenylboronic acid CAS: 63503-60-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
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inquiryProduct Name: 3-Chlorophenylboronic acid Synonyms: B-(3-chlorophenyl)-boronic acid;3-Chlorobenzeneboronic acid 98%;3-Chlorophenylboronic;3-Chlorophenylboornic acid;RARECHEM AH PB 0179;3-CHLOROPHENYLBORNIC ACID;3-CHLOROPHENYLBORONIC ACID;3-CHLOR
Cas:63503-60-6
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inquiryConditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -30℃; Inert atmosphere; Flow reactor; Stage #2: Trimethyl borate In tetrahydrofuran; hexane at -30℃; Inert atmosphere; Flow reactor; | 97% |
Stage #1: 1-bromo-3-chlorobenzene With isopropylmagnesium chloride; lithium chloride; 3-butyl-1-methylimidazolium acetate In tetrahydrofuran at 5 - 10℃; for 3h; Inert atmosphere; Stage #2: Trimethyl borate In tetrahydrofuran at 0℃; for 4h; Inert atmosphere; Stage #3: With hydrogenchloride In water at 5℃; for 0.5h; Inert atmosphere; | 66.43 g |
borane
(3-chlorophenyl)magnesium bromide
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With water In tetrahydrofuran slow addn. of 10 mmol of the Grignard reagent to a stirred soln. of borane in THF (40 mmol); the mixt. was poured into ice-water and acidified with 10% HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;; | 82% |
1-bromo-3-chlorobenzene
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With n-butyllithium In tetrahydrofuran; hexane Inert atmosphere; Stage #2: With Trimethyl borate In tetrahydrofuran; hexane Inert atmosphere; | 57% |
With Trimethyl borate | |
With Trimethyl borate |
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With sulfuric acid In ethanol; toluene at 0 - 40℃; Solvent; Reagent/catalyst; | 57% |
With water at 98℃; for 2h; | 14.37 g |
(3-chlorophenyl)magnesium bromide
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With boron trifluoride |
3-iodochlorobenzene
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
(i) (UV-irradiation), BBr3, (ii) aq. NaOH; Multistep reaction; |
Conditions | Yield |
---|---|
With water; magnesium In tetrahydrofuran a 2.0 M soln. of borane (40 mmol) in THF was added to flame dried Mg turnings (12 mmol) at 0°C; slow addn. of the aryl bromide (10 mmol)in THF; stirring at room temp. for 12-16 h; the mixt. was poured into ice-water and acidified with 10% HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;; |
1-bromo-3-chlorobenzene
Trimethyl borate
A
3-chlorophenylboronic acid
B
(3-bromophenyl)boronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -78 - -70℃; for 0.5h; Inert atmosphere; Stage #2: Trimethyl borate In tetrahydrofuran at -70℃; for 4h; Stage #3: With hydrogenchloride In water Overall yield = 24.6 g; |
1-bromo-3-chlorobenzene
Triisopropyl borate
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With iodine; magnesium In tetrahydrofuran for 5h; Inert atmosphere; Reflux; Stage #2: Triisopropyl borate In tetrahydrofuran at -40 - 0℃; Inert atmosphere; Stage #3: With water at 98℃; for 2h; Inert atmosphere; |
1-bromo-3-chlorobenzene
boric acid tributyl ester
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With iodine; magnesium In tetrahydrofuran for 5h; Inert atmosphere; Reflux; Stage #2: boric acid tributyl ester In tetrahydrofuran at -40 - 0℃; Inert atmosphere; Stage #3: With water at 98℃; for 2h; Inert atmosphere; |
3-chlorophenylboronic acid
ethylene glycol
3-chlorophenylboronic acid ethylene glycol ester
Conditions | Yield |
---|---|
In tetrahydrofuran for 18h; Heating / reflux; | 100% |
In tetrahydrofuran for 18h; Heating / reflux; | 100% |
In toluene for 3h; Heating; | |
In tetrahydrofuran for 18h; Heating; | |
In tetrahydrofuran at 20℃; for 8h; |
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With sodium carbonate; tris-(o-tolyl)phosphine; palladium diacetate In 1,2-dimethoxyethane; water Suzuki coupling; Heating; | 100% |
9,10-Dibromoanthracene
3-chlorophenylboronic acid
9,10-di(3-chlorophenyl)anthracene
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetra(n-butyl)ammonium hydroxide In 1,4-dioxane; water at 90℃; for 20h; Suzuki coupling; Inert atmosphere; | 100% |
C17H20BrN3O2
3-chlorophenylboronic acid
2-amino-7''-(3-chlorophenyl)-1-methyl-2',3',5',6'-tetrahydro-3'',4''-dihydro-2''H-dispiro[imidazol-4,1''-naphthalen-3'',4'-pyran]-5(1H)-one
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; water at 95℃; | 100% |
ethyl 5-bromo-4-(3-cyano-4-fluorophenyl)-1,3-thiazole-2-carboxylate
3-chlorophenylboronic acid
5-(3-chlorophenyl)-4-(3-cyano-4-fluorophenyl)-1,3-thiazole-2-carboxylic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In 1,2-dimethoxyethane; water at 20℃; for 1h; Reflux; | 100% |
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With potassium phosphate; bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II) In 1,4-dioxane; water at 100℃; for 1h; Suzuki Coupling; | 100% |
3-chlorophenylboronic acid
para-nitrophenyl bromide
3‐chloro‐4′‐nitrobiphenyl
Conditions | Yield |
---|---|
With 1,1',1'',1'''-benzene-1,2,4,5-tetrayltetrakis(methylene)tetrakis-(piperidin-4-ol); palladium diacetate; potassium carbonate In ethanol; water at 20℃; Suzuki-Miyaura Coupling; | 100% |
With Pd/C; potassium carbonate In ethanol; water at 100℃; for 3h; Suzuki-Miyaura Coupling; | 98% |
With dichloro bis(acetonitrile) palladium(II); C10H11N3S; potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1h; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 96% |
With carbon supported Pd nanoparticles; potassium carbonate at 95℃; for 6h; Suzuki-Miyaura Coupling; Sealed tube; |
1-bromo-3-fluoro-5-methoxybenzene
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 90℃; for 0.75h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); sodium carbonate In water; toluene at 75℃; for 16h; Inert atmosphere; | 100% |
3-chlorophenylboronic acid
1-(bromomethyl)-3-fluoro-5-(trifluoromethyl)benzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In Dimethyl ether; water; N,N-dimethyl-formamide at 100℃; for 3.05h; Inert atmosphere; Microwave irradiation; | 100% |
cyclopent-2-enone
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With triethylamine; bis(norbornadiene)rhodium(l)tetrafluoroborate; C46H38N2O5P2 In 1,4-dioxane; water at 25℃; for 2h; Product distribution / selectivity; | 99% |
With potassium hydroxide; C46H38N2O5P2; chlorobis(cyclooctene)rhodium(I) dimer In 1,4-dioxane; water at 50℃; for 16h; Product distribution / selectivity; | 53% |
With potassium hydroxide; (R)-(-)-(3,5-dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalen-4-yl)diethylamine; bis(ethylene)rhodium acetylacetonate In 1,4-dioxane at 50℃; for 6h; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With Pd/C; potassium carbonate In water; N,N-dimethyl-formamide at 40℃; for 5h; Suzuki Coupling; | 99% |
With C24H20Cl2NPPdS; potassium carbonate; palladium In toluene at 100℃; for 1.5h; | 96% |
With sodium carbonate In ethanol; water at 20℃; for 8h; Suzuki-Miyaura Coupling; Inert atmosphere; | 96% |
cyclopent-2-enone
3-chlorophenylboronic acid
(3R)-3-(3-chlorophenyl)cyclopentanone
Conditions | Yield |
---|---|
With di(norbornadiene)rhodium(I) tetrafluoroborate; chiral modified linked BINOL derivative; triethylamine In 1,4-dioxane; water at 25℃; for 2h; | 99% |
3-chlorophenylboronic acid
PCB 11
Conditions | Yield |
---|---|
With potassium acetate; silver(l) oxide In methanol at 40℃; for 15h; | 99% |
With dipotassium peroxodisulfate; potassium carbonate In water; acetone for 2h; | 99% |
With p-benzoquinone; (SIPr)Pd(OAc)2(H2O) In methanol at 20℃; for 24h; | 95% |
Conditions | Yield |
---|---|
With triethylamine; [Rh(ndb)2]BF4; (R)-BINOL-based bidentate phosphoramidite In 1,4-dioxane; water at 25℃; for 2h; | 99% |
3-chlorophenylboronic acid
4,4-ethylenedioxy-1-oxo-1,4-dihydronaphthalene
Conditions | Yield |
---|---|
With chlorobis(ethylene)rhodium(I) dimer; C41H24F12O2P2; potassium hydroxide In water; toluene at 20℃; for 3h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 99% |
With potassium hydroxide; bis(ethylene)rhodium(I) chloride dimer In 1,4-dioxane at 20℃; for 20h; | 95% |
3-chlorophenylboronic acid
o-chloro-N-tosylbenzaldimine
(S)-N-[(2-chlorophenyl)(3-chlorophenyl)methyl]-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With potassium phosphate tribasic trihydrate; (Pd((C10H6N2C7H4CH2C6H5)2)(H2O)2)(2+)*2CF3SO3(1-)=(Pd((C10H6N2C7H4CH2C6H5)2)(H2O)2)(CF3SO3)2 In tetrahydrofuran at 4 - 20℃; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 99% |
methyl o-formylbenzoate
3-chlorophenylboronic acid
3-(3-chlorophenyl)-3H-isobenzofuran-1-one
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); C27H30N2S(1+)*Cl(1-); cesium fluoride In toluene at 80℃; for 1h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With [Pd(dppp)(H2O)2](2+)(BF4(1-))2 In 1,4-dioxane at 20℃; for 0.166667h; Inert atmosphere; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With [Pd(S,S)-bdpp(H2O)2](2+)(BF4(1-))2 In 1,4-dioxane at 20℃; for 0.666667h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With chlorobis(ethylene)rhodium(I) dimer; potassium hydrogen bifluoride; C28H22 In water; toluene at 100℃; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
3-chlorophenylboronic acid
3-monochlorophenol
Conditions | Yield |
---|---|
With water In tetrahydrofuran at 100℃; for 12h; | 99% |
With copper(I) oxide; potassium hydroxide In water at 20℃; for 24h; Green chemistry; | 98% |
With copper(II) ferrite; water; sodium hydroxide at 40℃; for 24h; Green chemistry; | 96% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate In tetrahydrofuran at 50℃; for 22h; Suzuki-Miyaura coupling; Inert atmosphere; chemoselective reaction; | 99% |
cyclopent-2-enone
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With C42H46O6Rh2S2; cesium fluoride In 1,4-dioxane at 20℃; Hayashi-Miyaura reaction; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
Stage #1: 3-chlorophenylboronic acid With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); bis(norbornadiene)rhodium(l)tetrafluoroborate In 1,4-dioxane; water for 2h; Inert atmosphere; Stage #2: cyclopent-2-enone With triethylamine In 1,4-dioxane; water | 89.2% |
With chlorobis(ethylene)rhodium(I) dimer; potassium phosphate tribasic trihydrate; C19H23NOS In 1,4-dioxane; water at 20℃; for 3h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 62% |
Non-3-en-2-on
3-chlorophenylboronic acid
(S)-4-(3-chlorophenyl)nonan-2-one
Conditions | Yield |
---|---|
With chlorobis(ethylene)rhodium(I) dimer; (S,S)-1,1'-(1,7,7-trimethylbicyclo[2.2.1]hepta-2,5-diene-2,5-diyl)dinaphthalene; triethylamine In ethanol at 20℃; for 16h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With bis(ethylene)rhodium(I) chloride dimer; C19H23NOS; potassium hydroxide In 1,4-dioxane; water at 20 - 50℃; for 4h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
di-tert-butyl fumarate
3-chlorophenylboronic acid
(S)-di-tert-butyl-2-(3-chlorophenyl)succinate
Conditions | Yield |
---|---|
Stage #1: 3-chlorophenylboronic acid With chlorobis(ethylene)rhodium(I) dimer; (S,S)-1,7,7-trimethyl-2,5-diphenylbicyclo[2.2.1]hepta-2,5-diene; potassium tert-butylate In methanol; dichloromethane at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: di-tert-butyl fumarate In methanol; dichloromethane; isopropyl alcohol at 60℃; for 1h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
3-chlorophenylboronic acid
para-bromoacetophenone
1-(3'-chlorobiphenyl-4-yl)ethanone
Conditions | Yield |
---|---|
With Pd/C; potassium carbonate In ethanol; water at 100℃; for 3h; Suzuki-Miyaura Coupling; | 99% |
With C20H38Cl2N4P2Pd; caesium carbonate In N,N-dimethyl-formamide at 110℃; for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 72.3% |
With potassium carbonate In ethanol at 70℃; for 4h; Catalytic behavior; Suzuki-Miyaura Coupling; Schlenk technique; Sealed tube; | 95 %Spectr. |
With carbon supported Pd nanoparticles; potassium carbonate at 95℃; for 6h; Suzuki-Miyaura Coupling; Sealed tube; |
tetramethylazacalix[1]-arene[3]pyridine
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With copper(II) perchlorate hexahydrate; triethylamine In dimethyl sulfoxide at 80℃; for 3.5h; | 99% |
3-chlorophenylboronic acid
benzo[e][1,2,3]oxathiazine 2,2-dioxide
Conditions | Yield |
---|---|
With silver tetrafluoroborate; C30H38Cl2NPPd In 1,2-dichloro-ethane at 65℃; for 1h; enantioselective reaction; | 99% |
With nickel(II) perchlorate hexahydrate; (S)-2′-(tert-butyl)-7-(diphenylphosphino)-2,3-dihydro-5′H-spiro[indene-1,4′-oxazole] In 2,2,2-trifluoroethanol at 60℃; for 24h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 97% |
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