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inquiryNilutamide Basic information Product Name: Nilutamide Synonyms: Anandron, RU-23908, 5,5-Dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-imidazolidinedione;ANANDRON;5,5-DIMETHYL-3-[4-N
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Nilutamide CAS:63612-50-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
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2-Fluoro-5-nitrobenzotrifluoride
5,5-dimethyl(trimethylsilyl)hydantoin
nilutamide
Conditions | Yield |
---|---|
Stage #1: 2-Fluoro-5-nitrobenzotrifluoride With cesium fluoride In N,N-dimethyl-formamide for 0.166667h; Inert atmosphere; Stage #2: 5,5-dimethyl(trimethylsilyl)hydantoin In N,N-dimethyl-formamide at 60℃; for 16h; |
nilutamide
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran; water at 120℃; under 37503.8 Torr; for 15h; chemoselective reaction; | 96% |
With formic acid; triethylamine In tetrahydrofuran at 100℃; for 15h; Inert atmosphere; Sealed tube; chemoselective reaction; | 96% |
With formic acid; triethylamine for 24h; chemoselective reaction; | 94% |
With tin(ll) chloride In ethanol |
methanesulfonic acid 9-(4,4,5,5,5-pentafluoro-pentyl-sulfanyl)-nonyl ester
nilutamide
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{9-[(4,4,5,5,5-pentafluoropentyl)thio]nonyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Stage #1: nilutamide With sodium hydride In N,N-dimethyl-formamide at 23℃; for 1h; Inert atmosphere; Stage #2: methanesulfonic acid 9-(4,4,5,5,5-pentafluoro-pentyl-sulfanyl)-nonyl ester In N,N-dimethyl-formamide for 15h; Inert atmosphere; | 72% |
1,5-diiodopentane
nilutamide
1-(5-iodopentyl)-5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Stage #1: nilutamide With sodium hydride In N,N-dimethyl-formamide at 23℃; for 1h; Inert atmosphere; Stage #2: 1,5-diiodopentane In N,N-dimethyl-formamide for 15h; Inert atmosphere; | 47% |
1,4-dibromo-butane
nilutamide
1,1'-butane-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)-phenyl]imidazolidine-2,4-dione}
Conditions | Yield |
---|---|
Stage #1: nilutamide With sodium hydride In N,N-dimethyl-formamide at 23℃; for 0.5h; Inert atmosphere; Stage #2: 1,4-dibromo-butane In N,N-dimethyl-formamide at 55℃; for 1h; Inert atmosphere; | 45% |
acrylic acid n-butyl ester
nilutamide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; copper(II) acetate monohydrate In 2-methyltetrahydrofuran at 100℃; for 18h; Sealed tube; | 14% |
nilutamide
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{9-[(4,4,5,5,5-pentafluoropentyl)sulphinyl]nonyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: Oxone / water; tetrahydrofuran / 0.33 h View Scheme |
nilutamide
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{9-[(4,4,5,5,5-pentafluoropentyl)sulphonyl]nonyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: Oxone / water; tetrahydrofuran / 0.33 h 3.1: Oxone / water; tetrahydrofuran / 3.5 h / 23 °C View Scheme |
nilutamide
3-[4-amino-3-(trifluoromethyl)phenyl]-5,5-dimethyl-1-{9-[(4,4,5,5,5-pentafluoropentyl)thio]nonyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: tin(II) chloride dihdyrate / ethyl acetate / 5.5 h / Reflux View Scheme |
nilutamide
N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 6 h / 23 °C View Scheme |
nilutamide
N-[(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(oxido)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: Oxone / water; tetrahydrofuran / 0.33 h 3.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 6 h / 23 °C View Scheme |
nilutamide
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{9-[S-(4,4,5,5,5-pentafluoropentyl)sulphonimidoyl]nonyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: Oxone / water; tetrahydrofuran / 0.33 h 3.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 6 h / 23 °C 4.1: potassium carbonate; methanol / 15 h / 23 °C View Scheme |
nilutamide
N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)thio]-nonyl}imidazolidin-1-yl)-2-(trifluoromethyl)phenyl]acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: tin(II) chloride dihdyrate / ethyl acetate / 5.5 h / Reflux 3.1: dichloromethane / 1 h / 23 °C View Scheme |
nilutamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: tin(II) chloride dihdyrate / ethyl acetate / 5.5 h / Reflux 3.1: dichloromethane / 15 h / 23 °C 3.2: 3 h / 23 °C 3.3: 17 h / 23 °C View Scheme |
1,5-diiodopentane
nilutamide
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{5-[(4,4,5,5,5-pentafluoropentyl)thio]pentyl}imidazolidine-2,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere 1.2: 15 h / Inert atmosphere 2.1: potassium tert-butylate / methanol / 0.5 h / 23 °C / Inert atmosphere 2.2: 24 h / Inert atmosphere View Scheme |
nilutamide
Conditions | Yield |
---|---|
With [(COD)Ir(dimethylphenylphosphine)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)]PF6; deuterium In dichloromethane at 20℃; for 1h; Inert atmosphere; Sealed tube; regioselective reaction; | |
With η4-cycloocta-1,5-diene(1,3-dimesitylimidazoline-2-ylidene)(triphenylphosphine)iridium(I) hexafluorophosphate; deuterium In dichloromethane at 25℃; for 1h; Catalytic behavior; Reagent/catalyst; Solvent; regioselective reaction; |
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