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Win-Win chemical Co.Ltd

Stock products, own laboratory Product number PC00174 English Name Cyclopropylacetonitrile CAS Number 6542-60-5 Purity 97% M

Cyclopropylacetonitrile cas no. 6542-60-5 97%

Cas:6542-60-5

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:1 Kilogram

FOB Price: $3.0

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Cyclopropaneacetonitrile

Cas:6542-60-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale priceCAS 6542-60-5 with high quality products

Cas:6542-60-5

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Cyclopropaneacetonitrile

Cas:6542-60-5

Min.Order:1 Gram

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Qingdao Beluga Import and Export Co., LTD

Cyclopropylacetonitrile CAS:6542-60-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

Cyclopropylacetonitrile CAS:6542-60-5

Cas:6542-60-5

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Cyclopropaneacetonitrile

Cas:6542-60-5

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Cyclopropaneacetonitrile

Cas:6542-60-5

Min.Order:0

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Cyclopropaneacetonitrile

Cas:6542-60-5

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0 Metric Ton

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Type:Other

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:10 Gram

FOB Price: $100.0

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Henan Tianfu Chemical Co., Ltd.

2-Cyclopropylacetonitrile; Cyclopropylacetonitril; CYCLOPROPYLACETONITRILE; CPAN CAS No.: 6542-60-5 Molecular formula: C5H7N Molecular weight: 81.12 Cyclopropanil Boiling point 142-144 °C (lit.) Density 0.878 g/mL at 25 °C (

2-Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:100 Gram

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:1 Gram

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:1 Metric Ton

FOB Price: $1.5

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:1 Metric Ton

FOB Price: $1.0

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0

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GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Cyclopropyl acetonitrile

Cas:6542-60-5

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Cyclopropylacetonitrile

Cas:6542-60-5

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat

Cyclopropylacetonitrile

Cas:6542-60-5

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Cyclopropylacetonitrile

Cas:6542-60-5

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Cyclopropaneacetonitrile

Cas:6542-60-5

Min.Order:0

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Hubei Langyou International Trading Co., Ltd

Cyclopropylacetonitrile Application:Cyclopropylacetonitrile

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0

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Type:Other

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Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

Cyclopropylacetonitrile CAS No.6542-60-5

Cas:6542-60-5

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DB BIOTECH CO., LTD

best seller Application:API

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0

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Hangzhou Fandachem Co.,Ltd

Cyclopropylacetonitrile cas 6542-60-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Cyclopropylacetonitrile cas 6542-60-5

Cas:6542-60-5

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Cyclopropylacetonitrile

Cas:6542-60-5

Min.Order:0

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

Cyclopropylacetonitrile

Cas:6542-60-5

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Hunan Longxianng Runhui Trading Co.,Ltd

CyclopropylacetonitrileAppearance:white powder Storage:Shading, sealed, dry place. Package:aluminous bag Application:API Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL f

Cyclopropylacetonitrile

Cas:6542-60-5

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Synthetic route

potassium cyanide

potassium cyanide

cyclopropylcarbinyl bromide
7051-34-5

cyclopropylcarbinyl bromide

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
In dimethyl sulfoxide at 110℃; for 5h; Inert atmosphere;82%
cyclopropylacetaldehyde oxime
530133-49-4

cyclopropylacetaldehyde oxime

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
With acetic anhydride In ethyl acetate at 25℃; for 3.5h; Heating / reflux;76.7%
sodium cyanide
143-33-9

sodium cyanide

cyclopropylcarbinyl bromide
7051-34-5

cyclopropylcarbinyl bromide

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
phase transfer;75%
In dimethyl sulfoxide at 120℃;41%
In dimethyl sulfoxide for 3h;
sodium cyanide
143-33-9

sodium cyanide

chloro(cyclopropyl)methane
5911-08-0

chloro(cyclopropyl)methane

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
In dimethyl sulfoxide Heating;50%
potassium cyanide
151-50-8

potassium cyanide

cyclopropylcarbinyl bromide
7051-34-5

cyclopropylcarbinyl bromide

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
With ethanol
Cyclopropylmethanol
2516-33-8

Cyclopropylmethanol

sodium cyanide
143-33-9

sodium cyanide

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
(i) PBr3, (ii) NaCN, aq. EtOH; Multistep reaction;
but-3-enenitrile
109-75-1

but-3-enenitrile

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Conditions
ConditionsYield
With palladium diacetate In diethyl ether for 0.166667h; Yield given;
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-(cyclopropyl)ethylamine
62893-54-3

2-(cyclopropyl)ethylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride; sulfuric acid In diethyl ether for 2h; Heating;99%
With lithium aluminium tetrahydride; sulfuric acid In diethyl ether at 20℃; for 2h; Heating / reflux;70%
With lithium aluminium tetrahydride; sulfuric acid In diethyl ether for 2h; Heating / reflux;70%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

rac-3-bromocyclohexene
1521-51-3

rac-3-bromocyclohexene

N-(cyclohex-2-en-1-yl)-2-cyclopropylacetamide

N-(cyclohex-2-en-1-yl)-2-cyclopropylacetamide

Conditions
ConditionsYield
With water; silver trifluoromethanesulfonate at 0℃; for 1h; Ritter Amidation; chemoselective reaction;97%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

cyclopropylacetic acid
5239-82-7

cyclopropylacetic acid

Conditions
ConditionsYield
With water; potassium hydroxide In ethanol at 90℃; for 18h;96%
With dihydrogen peroxide; sodium hydroxide In water at 0℃; for 48h; Reflux; Inert atmosphere;83%
With dihydrogen peroxide; sodium hydroxide In water Reflux;81%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

4-t-butoxy-3-methyl-2,5-difluoropyridine
169749-84-2

4-t-butoxy-3-methyl-2,5-difluoropyridine

2-(4-tert-butoxy-5-fluoro-3-methyl-2-pyridinyl)-2-cyclopropylacetonitrile
169749-85-3

2-(4-tert-butoxy-5-fluoro-3-methyl-2-pyridinyl)-2-cyclopropylacetonitrile

Conditions
ConditionsYield
Stage #1: 4-t-butoxy-3-methyl-2,5-difluoropyridine With lithium diisopropyl amide In tetrahydrofuran; hexane at -51 - 17℃; Metallation;
Stage #2: 2-cyclopropylacetonitrile In tetrahydrofuran; hexane at -51 - 17℃; Methylation;
93%
With lithium diisopropyl amide 1.) THF, -78 deg C, 15 min, 2.) THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h; Yield given. Multistep reaction;
Stage #1: With n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -78℃; for 0.5h;
Stage #2: 2-cyclopropylacetonitrile; 4-t-butoxy-3-methyl-2,5-difluoropyridine In tetrahydrofuran; hexanes at -78 - 20℃; for 2h;
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

4-tert-butoxy-2,5-difluoro-3-methoxypyridine
477700-61-1

4-tert-butoxy-2,5-difluoro-3-methoxypyridine

(4-tert-butoxy-5-fluoro-3-methoxypyridin-2-yl)cyclopropylacetonitrile
477700-63-3

(4-tert-butoxy-5-fluoro-3-methoxypyridin-2-yl)cyclopropylacetonitrile

Conditions
ConditionsYield
With lithium diisopropyl amide93%
With lithium diisopropyl amide 1.) THF, -78 deg C, 15 min, 2.) THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h; Multistep reaction;
With n-butyllithium; ammonium chloride; diisopropylamine In tetrahydrofuran
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

N-cyclohexenyl-N-(4-methoxybenzyl)furan-2-carboxamide
1350894-64-2

N-cyclohexenyl-N-(4-methoxybenzyl)furan-2-carboxamide

4-(cyclopropylmethyl)-2-(furan-2-yl)-5,6,7,8-tetrahydroquinazoline
1350894-77-7

4-(cyclopropylmethyl)-2-(furan-2-yl)-5,6,7,8-tetrahydroquinazoline

Conditions
ConditionsYield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 25℃; Inert atmosphere;91%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

phenylmagnesium bromide

phenylmagnesium bromide

2-cyclopropyl-1-phenylethanone
6739-22-6

2-cyclopropyl-1-phenylethanone

Conditions
ConditionsYield
90%
(i) Et2O, (ii) H2O; Multistep reaction;
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

C22H22N2O2
1350894-62-0

C22H22N2O2

C19H19N3
1350894-75-5

C19H19N3

Conditions
ConditionsYield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 25℃; Inert atmosphere;90%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

benzoic acid tert-butyl ester
774-65-2

benzoic acid tert-butyl ester

N-(tert-butyl)cyclopropanecarboxamide
15924-91-1

N-(tert-butyl)cyclopropanecarboxamide

Conditions
ConditionsYield
With zinc perchlorate In neat (no solvent) at 50℃; for 5h; Ritter Amidation;90%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

2-cyclopropyl-1-phenylethanone
6739-22-6

2-cyclopropyl-1-phenylethanone

Conditions
ConditionsYield
Stage #1: 2-cyclopropylacetonitrile; phenylmagnesium bromide In diethyl ether at 0 - 20℃;
Stage #2: With hydrogenchloride; water In tetrahydrofuran; diethyl ether for 12h;
89%
Stage #1: 2-cyclopropylacetonitrile; phenylmagnesium bromide In diethyl ether at 0℃; for 2h;
Stage #2: With hydrogenchloride In diethyl ether; water for 12h;
70%
Stage #1: 2-cyclopropylacetonitrile; phenylmagnesium bromide In diethyl ether at 0 - 20℃;
Stage #2: With hydrogenchloride In diethyl ether; water for 12h;
70%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

methyl 2-amino-4,5-dimethoxybenzoate
26759-46-6

methyl 2-amino-4,5-dimethoxybenzoate

2-(cyclopropylmethyl)-6,7-dimethoxyquinazolin-4-ol
1448676-62-7

2-(cyclopropylmethyl)-6,7-dimethoxyquinazolin-4-ol

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane at 100℃; for 15h; Inert atmosphere;85%
bromobenzene
108-86-1

bromobenzene

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-cyclopropyl-1-phenylethanone
6739-22-6

2-cyclopropyl-1-phenylethanone

Conditions
ConditionsYield
Stage #1: bromobenzene With magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux;
Stage #2: 2-cyclopropylacetonitrile In tetrahydrofuran at 20℃; Inert atmosphere;
Stage #3: With sulfuric acid for 2h; Reflux;
85%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

(E)-2-cyclopropyl-N’-hydroxyacetimidamide

(E)-2-cyclopropyl-N’-hydroxyacetimidamide

Conditions
ConditionsYield
With hydroxylamine In ethanol for 1h; Reflux;85%
With hydroxylamine In ethanol for 1h; Reflux;85%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

diphenyl acetylene
501-65-5

diphenyl acetylene

2-(cyclopropylmethyl)-3,4,5,6-tetraphenylpyridine

2-(cyclopropylmethyl)-3,4,5,6-tetraphenylpyridine

Conditions
ConditionsYield
With 1,4-di(diphenylphosphino)-butane; cobalt(II) iodide; zinc In N,N-dimethyl acetamide at 80℃; for 24h; Inert atmosphere;85%
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

(2Z)-2-cyclopropyl-3-(dimethylamino)prop-2-enenitrile

(2Z)-2-cyclopropyl-3-(dimethylamino)prop-2-enenitrile

Conditions
ConditionsYield
at 100℃; for 46h;83.5%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-Cyclopropylethylamine hydrochloride

2-Cyclopropylethylamine hydrochloride

Conditions
ConditionsYield
With fac-[(CO)3Mn(iPr2P(CH2)2PiPr2)(triflato)]; potassium tert-butylate; hydrogen In iso-butanol at 110℃; under 5171.62 Torr; for 0.25h; Catalytic behavior; Glovebox; Schlenk technique; Inert atmosphere; Autoclave;83%
Multi-step reaction with 2 steps
1.1: BH3 / tetrahydrofuran / 14 h / Heating
1.2: MeOH / 2 h / Heating
1.3: CH2Cl2 / 14 h / 20 °C
2.1: HCl / dioxane; CH2Cl2 / 14 h / 20 °C
View Scheme
With hydrogenchloride; borane In tetrahydrofuran; 1,4-dioxane; dichloromethane
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

C22H22N2O2
1350894-61-9

C22H22N2O2

C19H19N3
1350894-74-4

C19H19N3

Conditions
ConditionsYield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 25℃; Inert atmosphere;83%
ethanol
64-17-5

ethanol

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-cyclopropyl-1-ethoxy-1-ethanimine hydrochloride
21572-78-1

2-cyclopropyl-1-ethoxy-1-ethanimine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In diethyl ether at 0℃; for 24h;82%
With hydrogenchloride at 0℃;
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-cyclopropyl-3-dimethylaminoacrylonitrile
256376-57-5

2-cyclopropyl-3-dimethylaminoacrylonitrile

Conditions
ConditionsYield
at 100℃; for 46h;81%
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical
2564-83-2, 45842-10-2

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

2-cyclopropyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)acetonitrile
1404079-40-8

2-cyclopropyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)acetonitrile

Conditions
ConditionsYield
Stage #1: 2-cyclopropylacetonitrile With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.333333h; Inert atmosphere;
Stage #2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical With ferrocenium hexafluorophosphate In tetrahydrofuran; hexane at -78℃; Inert atmosphere;
80%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

C22H25NO3
1350894-60-8

C22H25NO3

C19H22N2O
1350894-73-3

C19H22N2O

Conditions
ConditionsYield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 25℃; Inert atmosphere;79%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

phenylhydroxamoyl chloride
934-16-7

phenylhydroxamoyl chloride

4-cyclopropyl-3-phenylisoxazol-5-amine

4-cyclopropyl-3-phenylisoxazol-5-amine

Conditions
ConditionsYield
With tert.-butyl lithium In tetrahydrofuran; n-heptane at -78℃; for 0.5h;78%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

acetic anhydride
108-24-7

acetic anhydride

2-cyclopropyl-3-oxobutanenitrile
918907-28-5

2-cyclopropyl-3-oxobutanenitrile

Conditions
ConditionsYield
Stage #1: 2-cyclopropylacetonitrile With lithium diisopropyl amide In tetrahydrofuran; cyclohexane for 0.166667h; cooling;
Stage #2: acetic anhydride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h;
78%
Stage #1: 2-cyclopropylacetonitrile With lithium diisopropyl amide In tetrahydrofuran; cyclohexane for 0.166667h; cooling;
Stage #2: acetic anhydride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Further stages.;
78%
Stage #1: 2-cyclopropylacetonitrile With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #2: acetic anhydride In tetrahydrofuran at -78 - 15℃; for 1h;
Stage #1: 2-cyclopropylacetonitrile With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.666667h;
Stage #2: acetic anhydride In tetrahydrofuran at -78℃; for 0.333333h;
0.98 g
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

dibromamine-T
21849-40-1

dibromamine-T

N-(tert-butyl)-2-cyclopropyl-N'-tosylacetimidamide

N-(tert-butyl)-2-cyclopropyl-N'-tosylacetimidamide

Conditions
ConditionsYield
With potassium carbonate In water at 20℃; for 0.5h;78%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

Diethyl carbonate
105-58-8

Diethyl carbonate

ethyl 2-cyano-2-cyclopropylacetate
42392-67-6

ethyl 2-cyano-2-cyclopropylacetate

Conditions
ConditionsYield
With sodium hydride In toluene for 2h; Heating;77%
With sodium hydride In toluene; mineral oil for 2.67h; Reflux;50 g
With sodium hydride In toluene for 2.5h; Inert atmosphere; Reflux;
With potassium tert-butylate In N,N-dimethyl-formamide at 50℃;130 g
Stage #1: 2-cyclopropylacetonitrile; Diethyl carbonate With sodium hydride In toluene for 2.5h; Inert atmosphere; Reflux;
Stage #2: With acetic acid In toluene at 0℃;
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

C22H25NO3
1350894-59-5

C22H25NO3

C19H22N2O
1350894-72-2

C19H22N2O

Conditions
ConditionsYield
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 25℃; Inert atmosphere;77%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

(Z)-2-cyclopropyl-N-hydroxyacetimidamide

(Z)-2-cyclopropyl-N-hydroxyacetimidamide

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium carbonate In ethanol; water at 80℃; for 12h;77%
2-cyclopropylacetonitrile
6542-60-5

2-cyclopropylacetonitrile

zirconacarborane methyl

zirconacarborane methyl

C22H45B9N2Zr

C22H45B9N2Zr

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 48h; Inert atmosphere;76%

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