DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:5911-08-0
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
CAS RN.: 5911-08-0 EINECS: 227-632-1 Molecular Weight:
Cas:5911-08-0
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:5911-08-0
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5911-08-0
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inquiryProduct name: Cylopropylmethyl chloride CAS No: 5911-08-0 Molecular Formula: C4H7Cl Molecular Weight: 90.55 Application: Organic intermediates for pharma, agrochemical, and synthesis raw materials. Appearance: Colorless Liquid Storage:RT.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:5911-08-0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:5911-08-0
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inquiryCylopropylmethyl chloride CAS:5911-08-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:5911-08-0
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5911-08-0
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
Cas:5911-08-0
Min.Order:100 Metric Ton
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:5911-08-0
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:5911-08-0
Min.Order:0
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inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:5911-08-0
Min.Order:100 Gram
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Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:5911-08-0
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:5911-08-0
Min.Order:10 Gram
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inquiryCylopropylmethyl/5911-08-0/99% purity in stockAppearance:white powder Storage:Shading, sealed, dry place. Package:according to customers' requirements Application:pharmaceutical intermediates raw material Transportation:By air(EMS or EUB or FedEx or
Cas:5911-08-0
Min.Order:1 Gram
Negotiable
Type:Other
inquiryProduct name: Cyclopropylmethyl Chloride CAS No.:5911-08-0 Molecule Formula:C4H7Cl Molecule Weight:90.55 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:5911-08-0
Min.Order:1 Kilogram
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:5911-08-0
Min.Order:0
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Type:Trading Company
inquiryCylopropylmethyl chloride Basic information Product Name: Cylopropylmethyl chloride Synonyms: CYCLOPROPYLMETHYL CHLORIDE;(CHLOROMETHYL)CYCLOPROPANE;Cyclopropane, (chloromethyl)-;Cyclopropane,(chloromethyl)-;Cylopropylmethylchloride;Cyclopropyl
Cas:5911-08-0
Min.Order:1 Gram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:5911-08-0
Min.Order:1 Kilogram
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:5911-08-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:5911-08-0
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryWuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
Conditions | Yield |
---|---|
With phenylphosphorus tetrachloride In chloroform at 0℃; for 0.0833333h; | 98% |
With 1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine at 0 - 20℃; for 3.25h; | 95% |
With 1,3,5-trichloro-2,4,6-triazine In acetonitrile at -10 - 25℃; for 5h; Solvent; Temperature; | 94% |
tetrachloromethane
tri(cyclopropylmethyl)phosphite
A
3-butenyl chloride
B
Phosphoric acid tricyclopropylmethyl ester
C
Trichloromethyl-phosphonic acid dicyclopropylmethyl ester
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In toluene at 80℃; Further byproducts given; | A 16% B 2% C 80% D 64% |
Cyclopropylmethanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
A 15% B 18% C 80% |
cyclopropylmethyl
A
3-butenyl chloride
B
1,3-dichlorobutane
C
1,2,4-trichlorobutane
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With chlorine In benzene Rate constant; Product distribution; Irradiation; other chlorinating agents; | A 10.3% B 6.2% C 19.1% D 34.4% |
methylcyclopropane
A
3-butenyl chloride
B
1,3-dichlorobutane
C
1,2,4-trichlorobutane
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With chlorine In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; Irradiation; | A 10.3% B 6.2% C 19.1% D 34.4% |
With tert-butylhypochlorite In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; for 2.5h; Irradiation; | A 17% B 3.2% C 6.5% D 24.2% |
Conditions | Yield |
---|---|
With phosphorus pentachloride | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With chlorine Irradiation; | |
With chlorine at -196.1℃; Quantum yield; Irradiation; var. magnetic field; |
chlorocyclobutane
potassium acetate
acetic acid
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 100℃; Rate constant; Solvolyse und Isomerisierung; |
diazomethane
3-chloroprop-1-ene
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
Cu catalyst |
3,4-dichlorobut-1-ene
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
(i) 9-bora-bicyclo<3.3.1>nonane, THF, (ii) aq. NaOH; Multistep reaction; |
tetrachloromethane
tri(cyclopropylmethyl)phosphite
A
3-butenyl chloride
B
Dicyclopropylcarbinyl-phosphonat
C
Phosphoric acid tricyclopropylmethyl ester
D
Trichloromethyl-phosphonic acid dicyclopropylmethyl ester
E
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In toluene at 80℃; for 4h; Product distribution; Mechanism; | A 16 % Chromat. B 2 % Chromat. C 2 % Chromat. D 80 % Chromat. E 64 % Chromat. |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
3-butenyl chloride
B
allylcarbinyl ethyl ether
C
chlorocyclobutane
D
cyclobutyl ethyl ether
E
cyclopropylcarbinyl ethyl ether
F
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 25℃; Thermodynamic data; Kinetics; Product distribution; Ea, effect of solvents; |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
allylcarbinyl ethyl ether
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Further byproducts given; | A 1 % Chromat. B 22 % Chromat. C 28 % Chromat. D 42 % Chromat. |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
chlorocyclobutane
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Further byproducts given; | A 5 % Chromat. B 22 % Chromat. C 28 % Chromat. D 42 % Chromat. |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate; mercury dichloride 1.) CH2Cl2, 20 deg C, 2.) 20 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
cyclopropylcarbinol hypochlorite
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With triphenyl phosphite In dichloromethane at -78℃; | A 1.5 % Chromat. B 8.5 % Chromat. C 90 % Chromat. |
cyclobutyl hypochlorite
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With triphenyl phosphite In dichloromethane at -78℃; | A 5 % Chromat. B 29 % Chromat. C 66 % Chromat. |
3-cyclopropylmethoxy-3-chlorodiaziridine
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; | A 7 % Chromat. B 15 % Chromat. C 78 % Chromat. |
With tetrabutylammonium tetrafluoroborate In acetonitrile at 25℃; | A 9 % Chromat. B 27 % Chromat. C 64 % Chromat. |
With tetrabutylammonium tetrafluoroborate In acetonitrile at 25℃; | A 9 % Chromat. B 27 % Chromat. C 64 % Chromat. |
methylcyclopropane
chlorine
A
3-butenyl chloride
B
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at -20℃; | |
at 50℃; |
thionyl chloride
Cyclopropylmethanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
pyridine
thionyl chloride
Cyclopropylmethanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
thionyl chloride
cyclobutanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
pyridine
thionyl chloride
cyclobutanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
ethanol
A
chlorocyclobutane
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Product distribution; Further Variations:; Solvents; |
ethanol
cyclobutoxychlorocarbene
A
chlorocyclobutane
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Product distribution; Further Variations:; Solvents; |
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Product distribution; Kinetics; Further Variations:; Solvents; | |
In 1,2-dichloro-ethane at 25℃; Kinetics; | |
In acetonitrile at 25℃; Product distribution; Further Variations:; Solvents; | A 10 % Chromat. B 19 % Chromat. C 71 % Chromat. |
cyclobutoxychlorocarbene
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 25℃; Kinetics; | |
In acetonitrile at 25℃; Product distribution; Kinetics; Further Variations:; Solvents; | |
In acetonitrile at 25℃; Product distribution; Further Variations:; Solvents; | A 10 % Chromat. B 35 % Chromat. C 55 % Chromat. |
3-cyclopropylmethoxy-3-chlorodiaziridine
A
3-butenyl chloride
B
chlorocyclobutane
C
1,4-dichlorobutane
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 365℃; Product distribution; | A 4.9 % Chromat. B 22.9 % Chromat. C 28.9 % Chromat. D 43.4 % Chromat. |
5,6-bis(3-fluoro-4-methoxyphenyl)-2H-pyridazin-3-one
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
100% |
1-(4-hydroxy-2,6-dimethylphenyl)ethanone
chloro(cyclopropyl)methane
1-(4-(cyclopropylmethoxy)-2,6-dimethylphenyl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 16h; Inert atmosphere; | 99% |
4-cyanophenol
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; | 98% |
6-nitro-3,4-dihydro-1H-quinolin-2-one
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
Stage #1: 6-nitro-3,4-dihydro-1H-quinolin-2-one With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: chloro(cyclopropyl)methane With potassium iodide In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 94% |
Stage #1: 6-nitro-3,4-dihydro-1H-quinolin-2-one With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: chloro(cyclopropyl)methane With potassium iodide In N,N-dimethyl-formamide at 120℃; for 2h; | 94% |
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 94% |
Stage #1: 6-nitro-3,4-dihydro-1H-quinolin-2-one With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: chloro(cyclopropyl)methane With potassium iodide In N,N-dimethyl-formamide at 120℃; Inert atmosphere; | 94% |
5-(3-fluoro-4-methoxyphenyl)-6-(4-methoxyphenyl)-2H-pyridazin-3-one
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
93.8% |
N-norcodeine hydrochloride
chloro(cyclopropyl)methane
17-(cyclopropylmethyl)-7,8-didehydro-4,5α-epoxy-3-methoxymorphinan-6α-ol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 100℃; for 18h; | 93% |
6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazine-3-one
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
93% |
11-oxo(10H)-pyrrolo<2,1-c><1,2,5>benzothiadiazepine 5,5-dioxide
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone for 24h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With 1-Phenylprop-1-yne; copper dichloride In tetrahydrofuran at 70℃; for 12h; | 90% |
chloro(cyclopropyl)methane
6-bromo-2-(2-cyclopropanemethyl)isoquinolin-1(2H)-one
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 50℃; for 3h; | 90% |
chloro(cyclopropyl)methane
5,6-bis(4-Methoxyphenyl)-4-ethoxy-carbonyl-2H-pyridazin-3-one
5,6-bis(4-methoxyphenyl)-2-cyclopropylmethyl-4-ethoxycarbonyl-2H-pyridazin-3-one
Conditions | Yield |
---|---|
89.1% |
Conditions | Yield |
---|---|
Stage #1: (1r,4r)-4-(tritylamino)cyclohexanol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: chloro(cyclopropyl)methane In tetrahydrofuran at 20℃; for 6h; | 86.4% |
chloro(cyclopropyl)methane
(-)-17-(cyclopropylmethyl)-3,14β-dimethoxy-4,5-α-epoxy-5β-methylmorphinan-6-one
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 22h; | 86% |
chloro(cyclopropyl)methane
AR-M390
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 25℃; for 0.5h; | 86% |
Conditions | Yield |
---|---|
With phenylphosphorus tetrachloride In chloroform at 0℃; for 0.0833333h; | 98% |
With 1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine at 0 - 20℃; for 3.25h; | 95% |
With 1,3,5-trichloro-2,4,6-triazine In acetonitrile at -10 - 25℃; for 5h; Solvent; Temperature; | 94% |
tetrachloromethane
tri(cyclopropylmethyl)phosphite
A
3-butenyl chloride
B
Phosphoric acid tricyclopropylmethyl ester
C
Trichloromethyl-phosphonic acid dicyclopropylmethyl ester
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In toluene at 80℃; Further byproducts given; | A 16% B 2% C 80% D 64% |
Cyclopropylmethanol
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
A 15% B 18% C 80% |
cyclopropylmethyl
A
3-butenyl chloride
B
1,3-dichlorobutane
C
1,2,4-trichlorobutane
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With chlorine In benzene Rate constant; Product distribution; Irradiation; other chlorinating agents; | A 10.3% B 6.2% C 19.1% D 34.4% |
methylcyclopropane
A
3-butenyl chloride
B
1,3-dichlorobutane
C
1,2,4-trichlorobutane
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With chlorine In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; Irradiation; | A 10.3% B 6.2% C 19.1% D 34.4% |
With tert-butylhypochlorite In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; for 2.5h; Irradiation; | A 17% B 3.2% C 6.5% D 24.2% |
Conditions | Yield |
---|---|
With phosphorus pentachloride | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With chlorine Irradiation; | |
With chlorine at -196.1℃; Quantum yield; Irradiation; var. magnetic field; |
chlorocyclobutane
potassium acetate
acetic acid
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 100℃; Rate constant; Solvolyse und Isomerisierung; |
diazomethane
3-chloroprop-1-ene
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
Cu catalyst |
3,4-dichlorobut-1-ene
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
(i) 9-bora-bicyclo<3.3.1>nonane, THF, (ii) aq. NaOH; Multistep reaction; |
tetrachloromethane
tri(cyclopropylmethyl)phosphite
A
3-butenyl chloride
B
Dicyclopropylcarbinyl-phosphonat
C
Phosphoric acid tricyclopropylmethyl ester
D
Trichloromethyl-phosphonic acid dicyclopropylmethyl ester
E
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In toluene at 80℃; for 4h; Product distribution; Mechanism; | A 16 % Chromat. B 2 % Chromat. C 2 % Chromat. D 80 % Chromat. E 64 % Chromat. |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
3-butenyl chloride
B
allylcarbinyl ethyl ether
C
chlorocyclobutane
D
cyclobutyl ethyl ether
E
cyclopropylcarbinyl ethyl ether
F
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In ethanol; acetonitrile at 25℃; Thermodynamic data; Kinetics; Product distribution; Ea, effect of solvents; |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
allylcarbinyl ethyl ether
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Further byproducts given; | A 1 % Chromat. B 22 % Chromat. C 28 % Chromat. D 42 % Chromat. |
ethanol
3-cyclopropylmethoxy-3-chlorodiaziridine
A
chlorocyclobutane
B
cyclobutyl ethyl ether
C
cyclopropylcarbinyl ethyl ether
D
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
at 25℃; Further byproducts given; | A 5 % Chromat. B 22 % Chromat. C 28 % Chromat. D 42 % Chromat. |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate; mercury dichloride 1.) CH2Cl2, 20 deg C, 2.) 20 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
cyclopropylcarbinol hypochlorite
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With triphenyl phosphite In dichloromethane at -78℃; | A 1.5 % Chromat. B 8.5 % Chromat. C 90 % Chromat. |
cyclobutyl hypochlorite
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
With triphenyl phosphite In dichloromethane at -78℃; | A 5 % Chromat. B 29 % Chromat. C 66 % Chromat. |
3-cyclopropylmethoxy-3-chlorodiaziridine
A
3-butenyl chloride
B
chlorocyclobutane
C
chloro(cyclopropyl)methane
Conditions | Yield |
---|---|
In acetonitrile at 25℃; | A 7 % Chromat. B 15 % Chromat. C 78 % Chromat. |
With tetrabutylammonium tetrafluoroborate In acetonitrile at 25℃; | A 9 % Chromat. B 27 % Chromat. C 64 % Chromat. |
With tetrabutylammonium tetrafluoroborate In acetonitrile at 25℃; | A 9 % Chromat. B 27 % Chromat. C 64 % Chromat. |
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