CAS No.594-11-6,methylcyclopropane Suppliers

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methylcyclopropane

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Cyclopropane, methyl-

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

METHYLCYCLOPROPANE

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methylcyclopropane

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Bluecrystal chem-union

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Cyclopropane, methyl-

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Antimex Chemical Limied

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Cyclopropane, methyl-

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Henan Kanbei Chemical Co.,LTD

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methylcyclopropane

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Chemsigma International Co.,Ltd.

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methylcyclopropane

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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methylcyclopropane

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Synthetic route

: 14104-20-2
silver tetrafluoroborate

: 116840-62-1
C5H5(CO)2FeCH2CH2CH(CH3)Br

: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
In benzene-d6 byproducts: AgBr; Addn. of a soln. of iron compound to a frozen suspn. of AgBF4 at liquid nitrogen temp., sealing NMR tube under high vac., warming to room temp. and shaking.; Not isolated, NMR, MS, GC.;	70%

: 64-17-5
ethanol

: 106359-12-0
5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 18387-24-1
5,5-dimethyl-5-sila-2-hexanol

B: 594-11-6
methylcyclopropane

C: (3-Ethoxy-butyl)-trimethyl-silane

Conditions

Conditions	Yield
With water Product distribution; Rate constant; Mechanism; competitive reaction; use (R)-(-)-enriched compound, add of LiClO4, KOH, KOBs, LiOBs;	A 63% B 20% C 17%

...Expand

: 87145-50-4
(η5-cyclopentadienyl)dicarbonylrhenacyclopentane

A: 106-98-9
1-butylene

B: tricarbonylcyclopentadienylrhenium

C: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
In benzene-d6 thermolysis of Re-complex in benzene-d6 in sealed tube at 100°C; identified by (1)H NMR gas chromy.;	A <1 B 50% C 40%

...Expand

: 75-89-8
2,2,2-trifluoroethanol

: 106359-12-0
5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 18387-24-1
5,5-dimethyl-5-sila-2-hexanol

B: 594-11-6
methylcyclopropane

C: Trimethyl-[3-(2,2,2-trifluoro-ethoxy)-butyl]-silane

Conditions

Conditions	Yield
With water at 25℃; Rate constant; Product distribution; Mechanism; competitive reaction; use (R)-(-)-enriched compound, add of LiClO4, KOH, KOBs, LiOBs;	A 26% B 27% C 47%

...Expand

: bis(pentamethylcyclopentadienyl)titanacyclopentane(CH2CH2)

A: 74-85-1
ethene

B: 3404-63-5
2-ethyl-1,3-butadiene

C: 594-11-6
methylcyclopropane

D: 106-99-0
buta-1,3-diene

Conditions

Conditions	Yield
In neat (no solvent, solid phase) placing of Ti-compd. in a Schlenk tube, rapid heating up to 200°C under reduced pressure in an oil bath; condensing of products in a NMR tube, detected by (1)H NMR, GLC and MS;	A 43% B 16% C 19% D 31%

...Expand

: Cyclopropylmethyl-phosphonic acid isopropyl ester 2-thioxo-2H-pyridin-1-yl ester

A: 106-98-9
1-butylene

B: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With 2,2'-azobis(isobutyronitrile); 2-methylpropan-2-thiol In benzene Heating;	A 3% B 0.2%

: 2465-56-7
methylene

: 187737-37-7
propene

A: 106-98-9
1-butylene

B: 590-18-1
(Z)-2-Butene

C: 624-64-6
trans-2-Butene

D: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
Produkt5: Isobutylen;

...Expand

: 1190-22-3
1,3-dichlorobutane

: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With N-methyl-acetamide; zinc at 60 - 70℃;

: 107-80-2
1,3-dibromobutane

: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With copper In tetrahydrofuran at -70℃; for 0.166667h; further reaction with other α,ω-dihaloalkanes at other temperatures;	97 % Chromat.
With ethanol; zinc
With propan-1-ol; water; zinc

: 2465-56-7
methylene

: 75-19-4
cyclopropane

A: 106-98-9
1-butylene

B: 590-18-1
(Z)-2-Butene

C: 624-64-6
trans-2-Butene

D: 594-11-6
methylcyclopropane

...Expand

: 513-36-0
isobutyryl chloride

: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With n-heptane; sodium; di-n-propylmercury

: 96-47-9
2-methyltetrahydrofuran

A: 1487-15-6
2-Methyl-4,5-dihydrofuran

B: 50-00-0
formaldehyd

C: 594-11-6
methylcyclopropane

D: 75-07-0
acetaldehyde

E: 107-87-9
2-Pentanone

F: 75-19-4
cyclopropane

Conditions

Conditions	Yield
at 15℃; Quantum yield; Irradiation;

...Expand

: 64-17-5
ethanol

: 106359-13-1
2-deuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-08-4
2-deuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H21(2)HOSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 64-17-5
ethanol

: 106359-15-3
1,1,1-trideuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-10-8
1,1,1-trideuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H19(2)H3OSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 64-17-5
ethanol

: 106359-14-2
1,1,1,3,3-pentadeuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-09-5
1,1,1,3,3-pentadeuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H17(2)H5OSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 593-53-3
Methyl fluoride

: 4333-56-6
cyclopropyl bromide

A: 74-83-9
methyl bromide

B: 594-11-6
methylcyclopropane

C: 75-19-4
cyclopropane

Conditions

Conditions	Yield
With oxygen under 737 Torr; Product distribution; Mechanism; Irradiation; further with CH3Cl; quenched by NH3;	A 2.29 (unit not given) B 3.30 (unit not given) C 40.50 (unit not given)

...Expand

: 74-85-1
ethene

A: 594-11-6
methylcyclopropane

B: 287-23-0
cyclobutane

C: 106-97-8
n-butane

Conditions

Conditions	Yield
bis(triphenylphosphine)ethylenenickel(0) In toluene at 62℃; for 5h; Irradiation; Yield given. Yields of byproduct given;

...Expand

: 75-89-8
2,2,2-trifluoroethanol

: 106359-13-1
2-deuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-08-4
2-deuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H18(2)HF3OSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 75-89-8
2,2,2-trifluoroethanol

: 106359-15-3
1,1,1-trideuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-10-8
1,1,1-trideuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H16(2)H3F3OSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 75-89-8
2,2,2-trifluoroethanol

: 106359-14-2
1,1,1,3,3-pentadeuterio-5,5-dimethyl-5-sila-2-hexyl p-bromobenzenesulfonate

A: 594-11-6
methylcyclopropane

B: 106359-09-5
1,1,1,3,3-pentadeuterio-5,5-dimethyl-5-sila-2-hexanol

C: C9H14(2)H5F3OSi

Conditions

Conditions	Yield
With water at 25℃; isotope effects;

...Expand

: 2154-76-9
cyclopropylmethyl

A: 106-98-9
1-butylene

B: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With thiophenol Rate constant; Product distribution; different temperatures;

: 2154-76-9
cyclopropylmethyl

: 594-11-6
methylcyclopropane

Conditions

Conditions	Yield
With Benzeneselenol In tetrahydrofuran at 20℃; Rate constant; other solv.;

: 33574-02-6
cyclopropylmethyl iodide

: 38423-82-4
potassium trimethylstannate

A: 594-11-6
methylcyclopropane

B: 17314-38-4
(3-butenyl)trimethylstannane

C: 51675-53-7
(Cyclopropylcarbinyl)trimethylstannane

Conditions

Conditions	Yield
With tert-butylamine In tetrahydrofuran at 0℃; Product distribution; Mechanism; other addend;	A 29 % Chromat. B 62 % Chromat. C 7.2 % Chromat.

...Expand

: 33574-02-6
cyclopropylmethyl iodide

: 16643-09-7
trimethylstannyl sodium

A: 106-98-9
1-butylene

B: 594-11-6
methylcyclopropane

C: 17314-38-4
(3-butenyl)trimethylstannane

D: 51675-53-7
(Cyclopropylcarbinyl)trimethylstannane

Conditions

Conditions	Yield
With tert-butylamine In tetrahydrofuran at 0℃; Product distribution; Mechanism; other addend;	A 2.6 % Chromat. B 58 % Chromat. C 23 % Chromat. D 16 % Chromat.

...Expand

: 33574-02-6
cyclopropylmethyl iodide

: 17946-71-3
lithium trimethylstannyl

A: 106-98-9
1-butylene

B: 594-11-6
methylcyclopropane

C: 17314-38-4
(3-butenyl)trimethylstannane

D: 51675-53-7
(Cyclopropylcarbinyl)trimethylstannane

Conditions

Conditions	Yield
With tert-butylamine In tetrahydrofuran at 0℃; Product distribution; Mechanism; other addend;	A 2.6 % Chromat. B 7.2 % Chromat. C 31 % Chromat. D 51 % Chromat.

...Expand

: 39185-82-5
1,1,3,3-tetrachlorobutane

A: 594-11-6
methylcyclopropane

B: 3100-04-7
Methylcyclopropen

Conditions

Conditions	Yield
With zinc In N,N-dimethyl-formamide at 25 - 30℃; Title compound not separated from byproducts;	A 8 % Chromat. B 56 % Chromat.
With zinc In N,N-dimethyl-formamide at 25 - 30℃; Product distribution; dechlorination of polychloroalkanes containing -CCl2CH2CCl2- group;	A 8 % Chromat. B 56 % Chromat.

: 21981-33-9
1,1,1,3,3-pentachlorobutane

A: 594-11-6
methylcyclopropane

B: 3100-04-7
Methylcyclopropen

Conditions

Conditions	Yield
With zinc In N,N-dimethyl-formamide at 25 - 30℃; Title compound not separated from byproducts;	A 4 % Chromat. B 29 % Chromat.

: 594-11-6
methylcyclopropane

A: 927-73-1
3-butenyl chloride

B: 1190-22-3
1,3-dichlorobutane

C: 1790-22-3
1,2,4-trichlorobutane

D: 5911-08-0
chloro(cyclopropyl)methane

Conditions

Conditions	Yield
With chlorine In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; Irradiation;	A 10.3% B 6.2% C 19.1% D 34.4%
With tert-butylhypochlorite In 1,1,2-Trichloro-1,2,2-trifluoroethane at 20℃; for 2.5h; Irradiation;	A 17% B 3.2% C 6.5% D 24.2%

...Expand

: 594-11-6
methylcyclopropane

A: 927-73-1
3-butenyl chloride

B: 1190-22-3
1,3-dichlorobutane

C: 1790-22-3
1,2,4-trichlorobutane

D: 1-(2,4-Dichloro-butyl)-4,4-dimethyl-piperidine-2,6-dione

Conditions

Conditions	Yield
With 3,3-dimethyl-N-chloroglutarimide In 1,1,2-Trichloro-1,2,2-trifluoroethane at 22℃; for 48h; Irradiation; Further byproducts given;	A 3% B 12.8% C 3% D 20%

...Expand

: 594-11-6
methylcyclopropane

: 1600-27-7
mercury(II) diacetate

: 3-hydroxy-butylmercury (1+); chloride

Conditions

Conditions	Yield
With water und anschliessend mit wss.KCl;

: 594-11-6
methylcyclopropane

: 107-01-7
butene-2

Conditions

Conditions	Yield
With aluminum oxide at 340 - 360℃; mixtures of higher-boiling buten-(2) and lower-boiling butene-(2);

: 594-11-6
methylcyclopropane

: 5408-86-6
2,3-dibromobutane

Conditions

Conditions	Yield
With aluminum oxide at 340 - 360℃; und Behandeln des entstandenen Gemisches von Kohlenwasserstoffen mit Brom; mixtures of/the/ both forms of 2.3-dibromo-butane;

: 594-11-6
methylcyclopropane

: 107-80-2
1,3-dibromobutane

Conditions

Conditions	Yield
With bromine
With bromine; iron
With bromine In tetrachloromethane at 14℃; for 0.5h; Irradiation; in the absence of O2;

: 594-11-6
methylcyclopropane

: 50915-27-0
1-bromo-1-methylcyclopropane

Conditions

Conditions	Yield
With bromine beim Ausschluss von Licht;

: 594-11-6
methylcyclopropane

: 5911-08-0
chloro(cyclopropyl)methane

Conditions

Conditions	Yield
With chlorine Irradiation;
With chlorine at -196.1℃; Quantum yield; Irradiation; var. magnetic field;

: 594-11-6
methylcyclopropane

: 78-92-2, 15892-23-6
iso-butanol

Conditions

Conditions	Yield
With sulfuric acid; water

: 594-11-6
methylcyclopropane

: 75-36-5
acetyl chloride

: 102438-65-3
2-chlorohexan-5-one

Conditions

Conditions	Yield
With aluminium trichloride In dichloromethane

: 594-11-6
methylcyclopropane

: 75-36-5
acetyl chloride

: 19996-54-4
4-chloro-3-methyl-pentan-2-one

Conditions

Conditions	Yield
With aluminium trichloride In dichloromethane

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Dayang Chem (Hangzhou) Co.,Ltd.

Shanghai Upbio Tech Co.,Ltd

Afine Chemicals Limited

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Bluecrystal chem-union

Antimex Chemical Limied

Henan Kanbei Chemical Co.,LTD

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ZHEJIANG JIUZHOU CHEM CO.,LTD

Synthetic route

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