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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

Biphenyl-3-sulfonyl chloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

[1,1'-Biphenyl]-3-sulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3-Phenylbenzenesulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2-FLUORO-4-(TRIFLUOROMETHYL)PHENOL

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

[1,1'-Biphenyl]-3-sulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Biphenyl-3-sulphonyl chloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Phenylbenzenesulfonylchloride 65685-01-0

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-PHENYLBENZENESULFONYL CHLORIDE

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-PHENYLBENZENESULFONYL CHLORIDE

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

[1,1'-Biphenyl]-3-sulfonyl chloride

Cas:65685-01-0

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Hanhong Scientific Co.,Ltd.

factory,reasonable price Appearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:pharmaceutical intermediates Transportation:by courier,air or sea Port:S

[1,1'-Biphenyl]-3-sulfonyl chloride65685-01-0

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1.Best service, high quality and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). ? 3. It's customers' right to choose the packing way for his products fro

Best price/ Biphenyl-3-sulphonyl chloride CAS NO.65685-01-0

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

3-PHENYLBENZENESULFONYL CHLORIDE

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

[1,1'-Biphenyl]-3-sulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

biphenyl-3-sulfonyl chloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

coolpharm Ltd

Cool Pharm Ltd, found in 2013,is a high-tech enterprise which provides customer synthesis service for domestic and international pharmaceutical companies according to international standards. Our business includes research , development, process opti

[1,1'-Biphenyl]-3-sulfonyl chloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Other

inquiry

Chemical Co.Ltd

Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

[1,1'-Biphenyl]-3-sulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Interchim S.A.

more information,please contact us

[1,1'-Biphenyl]-3-sulfonylchloride

Cas:65685-01-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

[1,1'-biphenyl]-3-yl(benzyl)sulfane
94306-39-5

[1,1'-biphenyl]-3-yl(benzyl)sulfane

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
With N-chloro-succinimide; acetic acid In water at 20℃;59%
With N-chloro-succinimide; acetic acid In water at 20℃;59%
3-bromobiphenyl
2113-57-7

3-bromobiphenyl

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride; tert.-butyl lithium In diethyl ether at -78 - 20℃; for 7h;49%
In tetrahydrofuran
Multi-step reaction with 2 steps
1: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 100 °C / Inert atmosphere; Sealed tube
2: N-chloro-succinimide; acetic acid / water / 20 °C
View Scheme
3-bromobiphenyl
2113-57-7

3-bromobiphenyl

tert.-butyl lithium
594-19-4

tert.-butyl lithium

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In hexane; ethyl acetate49%
3-bromobiphenyl
2113-57-7

3-bromobiphenyl

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride; tert.-butyl lithium In hexane; ethyl acetate49%
1-Bromo-3-iodobenzene
591-18-4

1-Bromo-3-iodobenzene

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethanol; toluene / 2 h / 90 °C / Inert atmosphere; Sealed tube
2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 100 °C / Inert atmosphere; Sealed tube
3: N-chloro-succinimide; acetic acid / water / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethanol; toluene / 2 h / 90 °C / Inert atmosphere; Sealed tube
2: N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 100 °C / Inert atmosphere; Sealed tube
3: N-chloro-succinimide; acetic acid / water / 20 °C
View Scheme
phenylboronic acid
98-80-6

phenylboronic acid

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethanol; toluene / 2 h / 90 °C / Inert atmosphere; Sealed tube
2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 100 °C / Inert atmosphere; Sealed tube
3: N-chloro-succinimide; acetic acid / water / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethanol; toluene / 2 h / 90 °C / Inert atmosphere; Sealed tube
2: N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 100 °C / Inert atmosphere; Sealed tube
3: N-chloro-succinimide; acetic acid / water / 20 °C
View Scheme
4-(N-cyclohexylcarbonyl-N-(2-methyl-3-phenyl-2-(E)-propenyl)aminomethyl)piperidine trifluoroacetic acid salt

4-(N-cyclohexylcarbonyl-N-(2-methyl-3-phenyl-2-(E)-propenyl)aminomethyl)piperidine trifluoroacetic acid salt

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

C35H44N2O3S

C35H44N2O3S

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 16h;98%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

3-(4-(aminomethyl)benzyl)-7-ethyl-1H-purine-2,6(3H,7H)-dione trifluoroacetic acid salt

3-(4-(aminomethyl)benzyl)-7-ethyl-1H-purine-2,6(3H,7H)-dione trifluoroacetic acid salt

N-(4-((7-ethyl-2,6-dioxo-1H-purin-3(2H,6H,7H)-yl)methyl)benzyl)-[1,1′-biphenyl]-3-sulfonamide

N-(4-((7-ethyl-2,6-dioxo-1H-purin-3(2H,6H,7H)-yl)methyl)benzyl)-[1,1′-biphenyl]-3-sulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 12h;96%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

(1,1′-biphenyl)-3-sulfonamide
91569-33-4

(1,1′-biphenyl)-3-sulfonamide

Conditions
ConditionsYield
With ammonium hydroxide In dichloromethane; water at 20℃; for 6.5h; Cooling with ice;93%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

3,4,5-Trimethoxyaniline
24313-88-0

3,4,5-Trimethoxyaniline

N-(3,4,5-trimethoxyphenyl)biphenyl-3-sulfonamide
1311195-74-0

N-(3,4,5-trimethoxyphenyl)biphenyl-3-sulfonamide

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide91.7%
With triethylamine In N,N-dimethyl-formamide91.7%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

N-methyl-4-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]aniline
1481-11-4

N-methyl-4-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]aniline

biphenyl-3-sulfonic acid methyl-[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-amide

biphenyl-3-sulfonic acid methyl-[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-amide

Conditions
ConditionsYield
With 2,6-dimethylpyridine In acetone at 60℃; for 24h;90%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

C13H15N3O

C13H15N3O

(biphenyl-3-yl)sulfonyl-(R)-phenylalanylaminocyclopropane nitrile

(biphenyl-3-yl)sulfonyl-(R)-phenylalanylaminocyclopropane nitrile

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 20h; Inert atmosphere;89%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

C10H17N3O

C10H17N3O

(biphenyl-3-yl)sulfonyl-(R)-leucylaminocyclopropane nitrile

(biphenyl-3-yl)sulfonyl-(R)-leucylaminocyclopropane nitrile

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 20h; Inert atmosphere;78%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

(-)-alpha-Methyltryptamine
7795-52-0

(-)-alpha-Methyltryptamine

(R)-N-(1-(1H-indol-3-yl)propan-2-yl)-[1,1'-biphenyl]-3-sulfonamide

(R)-N-(1-(1H-indol-3-yl)propan-2-yl)-[1,1'-biphenyl]-3-sulfonamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h;77%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

4-Aminosalicylic acid
65-49-6

4-Aminosalicylic acid

4-[(biphenyl-3-ylsulfonyl)amino]-2-hydroxybenzoic acid
1353433-22-3

4-[(biphenyl-3-ylsulfonyl)amino]-2-hydroxybenzoic acid

Conditions
ConditionsYield
With pyridine In dichloromethane at 60℃; for 4h;74%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

(S)-2-amino-N-(1-cyanocyclopropyl)-3-phenylpropanamide

(S)-2-amino-N-(1-cyanocyclopropyl)-3-phenylpropanamide

(biphenyl-3-yl)sulfonyl-(S)-phenylalanylaminocyclopropane nitrile

(biphenyl-3-yl)sulfonyl-(S)-phenylalanylaminocyclopropane nitrile

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 20h; Inert atmosphere;71%
methyl 4-{3-[2-(2-aminoethyl)-5-chloro-1-(diphenylmethyl)-1H-indol-3-yl]propyl}benzoate
540522-70-1

methyl 4-{3-[2-(2-aminoethyl)-5-chloro-1-(diphenylmethyl)-1H-indol-3-yl]propyl}benzoate

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

methyl 4-[3-(1-benzhydryl-2-{2-[(1,1'-biphenyl-3-ylsulfonyl)amino]ethyl}-5-chloro-1H-indol-3-yl)propyl]benzoate
1019217-38-9

methyl 4-[3-(1-benzhydryl-2-{2-[(1,1'-biphenyl-3-ylsulfonyl)amino]ethyl}-5-chloro-1H-indol-3-yl)propyl]benzoate

Conditions
ConditionsYield
With sodium hydrogencarbonate In dichloromethane; water Schotten-Baumann reaction;65%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

4-chloro-3-methyl-5-amino isoxazole
166964-09-6

4-chloro-3-methyl-5-amino isoxazole

N-(4-chloro-3-methyl-5-isoxazolyl)-3-biphenylsulfonamide

N-(4-chloro-3-methyl-5-isoxazolyl)-3-biphenylsulfonamide

Conditions
ConditionsYield
63%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

6-((2-chloro-6-fluorobenzyl)oxy)indoline

6-((2-chloro-6-fluorobenzyl)oxy)indoline

1-([1,1’-biphenyl]-3-ylsulfonyl)-6-((2-chloro-6-fluorobenzyl)oxy)indoline

1-([1,1’-biphenyl]-3-ylsulfonyl)-6-((2-chloro-6-fluorobenzyl)oxy)indoline

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;63%
methyl 4-{2-[2-(2-aminoethyl)-1-benzhydryl-5-chloro-1H-indol-3-yl]ethoxy}benzoate amine
540522-69-8

methyl 4-{2-[2-(2-aminoethyl)-1-benzhydryl-5-chloro-1H-indol-3-yl]ethoxy}benzoate amine

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

methyl 4-[2-(1-benzhydryl-2-{2-[(1,1'-biphenyl-3-ylsulfonyl)amino]ethyl}-5-chloro-1H-indol-3-yl)ethoxy]benzoate
1019216-96-6

methyl 4-[2-(1-benzhydryl-2-{2-[(1,1'-biphenyl-3-ylsulfonyl)amino]ethyl}-5-chloro-1H-indol-3-yl)ethoxy]benzoate

Conditions
ConditionsYield
With sodium hydrogencarbonate In dichloromethane; water Schotten-Baumann reaction;61%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

C15H21N3O

C15H21N3O

(biphenyl-3-yl)sulfonyl-(S)-leucylphenylalanine nitrile

(biphenyl-3-yl)sulfonyl-(S)-leucylphenylalanine nitrile

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 20h; Inert atmosphere;58%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

N-(1-cyanocyclopropyl)-L-leucinamide

N-(1-cyanocyclopropyl)-L-leucinamide

(biphenyl-3-yl)sulfonyl-(S)-leucylaminocyclopropane nitrile

(biphenyl-3-yl)sulfonyl-(S)-leucylaminocyclopropane nitrile

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 20h; Inert atmosphere;51%
4-(4-chlorophenyl)-2-thiazolamine
2103-99-3

4-(4-chlorophenyl)-2-thiazolamine

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

N-[4-(4-chlorophenyl)thiazol-2-yl]-3-phenylbenzenesulfonamide

N-[4-(4-chlorophenyl)thiazol-2-yl]-3-phenylbenzenesulfonamide

Conditions
ConditionsYield
With pyridine at 80℃; for 8h;47%
N-Boc-trans-1,4-bis(aminomethyl)cyclohexane

N-Boc-trans-1,4-bis(aminomethyl)cyclohexane

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

tert-butyl [(trans-4-{[(biphenyl-3-ylsulfonyl)amino]methyl}cyclohexyl)methyl]carbamate

tert-butyl [(trans-4-{[(biphenyl-3-ylsulfonyl)amino]methyl}cyclohexyl)methyl]carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;42%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

5'-amino-6'-chloro-N-methyl-[3,3'-bipyridine]-5-carboxamide

5'-amino-6'-chloro-N-methyl-[3,3'-bipyridine]-5-carboxamide

5’-([1,1'-biphenyl]-3-sulfonamido)-6'-chloro-N-methyl-[3,3'-bipyridine]-5-carboxamide

5’-([1,1'-biphenyl]-3-sulfonamido)-6'-chloro-N-methyl-[3,3'-bipyridine]-5-carboxamide

Conditions
ConditionsYield
With pyridine at 20℃; for 6h; Inert atmosphere;38%
hexan-1-amine
111-26-2

hexan-1-amine

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

methyl 1-(3-(chloromethyl)phenyl)-5-((trans)-2-(1-methyl-1H-1,2,3-triazol-4-yl)cyclopropyl)-1H-pyrazole-4-carboxylate

methyl 1-(3-(chloromethyl)phenyl)-5-((trans)-2-(1-methyl-1H-1,2,3-triazol-4-yl)cyclopropyl)-1H-pyrazole-4-carboxylate

1-(3-((N-hexyl-[1,1'-biphenyl]-3-ylsulfonamido)methyl)phenyl)-5-((trans)-2-(1-methyl-1H-1,2,3-triazol-4-yl)cyclopropyl)-1H-pyrazole-4-carboxylic acid

1-(3-((N-hexyl-[1,1'-biphenyl]-3-ylsulfonamido)methyl)phenyl)-5-((trans)-2-(1-methyl-1H-1,2,3-triazol-4-yl)cyclopropyl)-1H-pyrazole-4-carboxylic acid

Conditions
ConditionsYield
Stage #1: hexan-1-amine; biphenyl-3-sulfonyl chloride With N-ethyl-N,N-diisopropylamine In acetonitrile for 0.0166667h;
Stage #2: methyl 1-(3-(chloromethyl)phenyl)-5-((trans)-2-(1-methyl-1H-1,2,3-triazol-4-yl)cyclopropyl)-1H-pyrazole-4-carboxylate With sodium hydride In acetonitrile; mineral oil at 140℃; for 0.0166667h; Microwave irradiation;
Stage #3: With potassium hydroxide In water; acetonitrile; mineral oil Microwave irradiation;
32%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

novenamine hydrochloride

novenamine hydrochloride

C31H32N2O11S

C31H32N2O11S

Conditions
ConditionsYield
With pyridine at -40 - 23℃; for 12h; Inert atmosphere; Sealed tube;32%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

4-bromo-3-methyl-5-aminoisoxazole
33084-49-0

4-bromo-3-methyl-5-aminoisoxazole

N-(4-bromo-3-methyl-5-isoxazolyl)-3-biphenylsulfonamide

N-(4-bromo-3-methyl-5-isoxazolyl)-3-biphenylsulfonamide

Conditions
ConditionsYield
22%
biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

sodium methylate
124-41-4

sodium methylate

biphenyl-3-sulfonic acid methyl ester

biphenyl-3-sulfonic acid methyl ester

Conditions
ConditionsYield
With methanol
5-ethoxy-pyrrolidin-2-one
39662-63-0

5-ethoxy-pyrrolidin-2-one

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

1-(Biphenyl-3-sulfonyl)-5-ethoxy-pyrrolidin-2-one
111711-71-8

1-(Biphenyl-3-sulfonyl)-5-ethoxy-pyrrolidin-2-one

Conditions
ConditionsYield
With n-butyllithium 1.) THF, hexane, -70 deg C, 45 min, 2.) THF, hexane, -70 deg C, 2 h; Yield given. Multistep reaction;
5-amino-3,4-dimethylisoxazol
19947-75-2

5-amino-3,4-dimethylisoxazol

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

N-(3,4-dimethyl-5-isoxazolyl)-3-biphenylsulfonamide

N-(3,4-dimethyl-5-isoxazolyl)-3-biphenylsulfonamide

biphenyl-3-sulfonyl chloride
65685-01-0

biphenyl-3-sulfonyl chloride

3-(3-(S)-amino-2-oxopyrrolidin-1-ylmethyl)benzonitrile hydrochloride

3-(3-(S)-amino-2-oxopyrrolidin-1-ylmethyl)benzonitrile hydrochloride

Biphenyl-3-sulfonic acid [(S)-1-(3-cyano-benzyl)-2-oxo-pyrrolidin-3-yl]-amide
1027145-58-9

Biphenyl-3-sulfonic acid [(S)-1-(3-cyano-benzyl)-2-oxo-pyrrolidin-3-yl]-amide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 2h; Condensation; amidation;

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