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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

4-Isoxazolecarbonylchloride, 5-methyl-

Cas:67305-24-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

5-Methyl-4-Isoxazolecarbonyl Chloride

Cas:67305-24-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

CAS No.67305-24-2 Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Sc

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE CAS:67305-24-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qua

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE CAS:67305-24-2

Cas:67305-24-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

4-Isoxazolecarbonylchloride, 5-methyl-

Cas:67305-24-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

4-Isoxazolecarbonylchloride, 5-methyl-

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-Isoxazolecarbonylchloride, 5-methyl-

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

5-Methyl-4-isoxazolecarbonyl chloride

Cas:67305-24-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

5-Methyl-4-isoxazolecarbonyl chloride

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Manufacturers

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

5-Methyl-4-isoxazolecarboxylic acid chloride

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Cas no.67305-24-2 98% 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

5-Methyl-4-isoxazolecarbonyl chloride

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

5-Methyl-isoxazole-4-carbonyl chloride

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hubei Langyou International Trading Co., Ltd

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE Application:CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Other

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

4-Isoxazolecarbonylchloride, 5-methyl- cas 67305-24-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-Isoxazolecarbonylchloride, 5-methyl- cas 67305-24-2

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDEAppearance:Powder Storage:Room temperature Package:1KG -200KG Drum with pallet Application:Pharma intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount

CAS No.67305-24-2 5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

67305-24-2

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

5-Methyl-4-isoxazolecarbonyl chloride 67305-24-2

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

5-Methyl-4-isoxazolecarbonyl chloride 67305-24-2

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5-METHYL-4-ISOXAZOLECARBONYL CHLORIDE

Cas:67305-24-2

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

5-methyl-1,2-oxazole-4-carboxylic acid
42831-50-5

5-methyl-1,2-oxazole-4-carboxylic acid

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

Conditions
ConditionsYield
With thionyl chloride In toluene99%
With thionyl chloride at 70℃; for 1h;96%
With thionyl chloride at 50℃;96%
5-methylisoxazole-4-carboxylic acid ethyl ester
51135-73-0

5-methylisoxazole-4-carboxylic acid ethyl ester

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 270 g / conc. HCl / acetic acid; H2O / 10 h / Heating
2: 47 percent / thionyl chloride / 3 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: hydrogenchloride
2: thionyl chloride / Reflux
View Scheme
Multi-step reaction with 2 steps
1: sulfuric acid / water / 20 h / 20 °C / Reflux
2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 12 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: hydrogenchloride
2: thionyl chloride / N-methyl-acetamide
View Scheme
2-ethoxymethylene-3-oxobutanoic acid ethyl ester
3788-94-1

2-ethoxymethylene-3-oxobutanoic acid ethyl ester

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 350 g / hydroxylamine hydrochloride, sodium acetate trihydrate / ethanol; H2O / 0 °C
2: 270 g / conc. HCl / acetic acid; H2O / 10 h / Heating
3: 47 percent / thionyl chloride / 3 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: hydroxylamine hydrochloride
2: hydrogenchloride
3: thionyl chloride / Reflux
View Scheme
Multi-step reaction with 3 steps
1: hydroxylamine hydrochloride; sodium acetate / methanol; water / 0 - 20 °C
2: sulfuric acid / water / 20 h / 20 °C / Reflux
3: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 12 h / Reflux
View Scheme
4-trifluoromethylphenylamine
455-14-1

4-trifluoromethylphenylamine

A

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

B

Leflunomide
75706-12-6

Leflunomide

Conditions
ConditionsYield
With sodium hydrogencarbonate In water
5-methyl-1,2-oxazole-4-carboxylic acid
42831-50-5

5-methyl-1,2-oxazole-4-carboxylic acid

of toluene

of toluene

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

Conditions
ConditionsYield
With thionyl chloride
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2,4-dichlorophenoxyacetylhydrazine
28236-62-6

2,4-dichlorophenoxyacetylhydrazine

N'-(2-(2,4-dichlorophenoxy)acetyl)-5-methylisoxazole-4-carbohydrazide
1417515-26-4

N'-(2-(2,4-dichlorophenoxy)acetyl)-5-methylisoxazole-4-carbohydrazide

Conditions
ConditionsYield
In tetrahydrofuran for 0.166667h; Time; Reagent/catalyst; Temperature; Microwave irradiation;99%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

3-amino-5-bromo-benzofuran-2-carbonitrile
636992-54-6

3-amino-5-bromo-benzofuran-2-carbonitrile

N-(5-bromo-2-cyanobenzofuran-3-yl)-5-methylisoxazole-4-carboxamide
803684-89-1

N-(5-bromo-2-cyanobenzofuran-3-yl)-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 2h;96.6%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

4-trifluoromethylphenylamine
455-14-1

4-trifluoromethylphenylamine

Leflunomide
75706-12-6

Leflunomide

Conditions
ConditionsYield
In diethyl ether for 0.5h; Ambient temperature;93%
With sodium hydrogencarbonate In N,N-dimethyl acetamide; toluene86%
With sodium hydrogencarbonate In water; toluene at 20 - 60℃; for 18h;43%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

3-amino[1]benzofuran-2-carbonitrile
62208-67-7

3-amino[1]benzofuran-2-carbonitrile

N-(2-cyanobenzofuran-3-yl)-5-methylisoxazole-4-carboxamide
803684-90-4

N-(2-cyanobenzofuran-3-yl)-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 2h;90.9%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-amino-5-phenyl-1,3,4-thiadiazole
2002-03-1

2-amino-5-phenyl-1,3,4-thiadiazole

N-(5-phenyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-89-0

N-(5-phenyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-amino-5-phenyl-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
90.1%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

(E)-3-[3-Amino-2-(4-cyano-benzoyl)-benzofuran-5-yl]-but-2-enoic acid [2-(3,4-dimethoxy-phenyl)-ethyl]-amide

(E)-3-[3-Amino-2-(4-cyano-benzoyl)-benzofuran-5-yl]-but-2-enoic acid [2-(3,4-dimethoxy-phenyl)-ethyl]-amide

(E)-N-(2-(4-cyanobenzoyl)-5-{2-[2-(3,4-dimethoxyphenyl)ethylcarbamoyl]-1-methylvinyl}benzofuran-3-yl)-5-methylisoxazole-4-carboxamide

(E)-N-(2-(4-cyanobenzoyl)-5-{2-[2-(3,4-dimethoxyphenyl)ethylcarbamoyl]-1-methylvinyl}benzofuran-3-yl)-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 7h;90%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

5-(4-nitrophenyl)-1,3,4-thiadiazol-2-amine
833-63-6

5-(4-nitrophenyl)-1,3,4-thiadiazol-2-amine

N-(5-(4-nitrophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023697-03-1

N-(5-(4-nitrophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 5-(4-nitrophenyl)-1,3,4-thiadiazol-2-amine In dichloromethane for 0.5h; Irradiation; Further stages.;
88.8%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-amino-5-(2-chlorophenyl)-1,3,4-thiadiazole
828-81-9

2-amino-5-(2-chlorophenyl)-1,3,4-thiadiazole

N-(5-(2-chlorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-95-8

N-(5-(2-chlorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-amino-5-(2-chlorophenyl)-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
88.4%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-amino-5-(4-chlorophenyl)-1,3,4-thiadiazole
28004-62-8

2-amino-5-(4-chlorophenyl)-1,3,4-thiadiazole

N-(5-(4-chlorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-97-0

N-(5-(4-chlorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-amino-5-(4-chlorophenyl)-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
87.6%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

5-amino-2-methyl-N-(2-(4-(4-methylpiperazin-1-yl)phenylamino)pyrimidin-5-yl)benzamide
925897-75-2

5-amino-2-methyl-N-(2-(4-(4-methylpiperazin-1-yl)phenylamino)pyrimidin-5-yl)benzamide

5-methyl-N-(4-methyl-3-((2-(4-(4-methylpiperazin-1-yl)phenylamino)pyrimidin-5-yl)carbamoyl)phenyl)isoxazole-4-carboxamide

5-methyl-N-(4-methyl-3-((2-(4-(4-methylpiperazin-1-yl)phenylamino)pyrimidin-5-yl)carbamoyl)phenyl)isoxazole-4-carboxamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;86%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

benzylamine
100-46-9

benzylamine

N-benzyl-5-methylisoxazole-4-carboxamide

N-benzyl-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 40℃; for 24h;86%
ammonium thiocyanate

ammonium thiocyanate

2-amino-5-ethyl-1,3,4-thiadiazole
14068-53-2

2-amino-5-ethyl-1,3,4-thiadiazole

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

N-(5-ethyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-85-6

N-(5-ethyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-amino-5-ethyl-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
85.8%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

5-(3-methylphenyl)-1,3,4-thiadiazol-2-amine
76074-47-0

5-(3-methylphenyl)-1,3,4-thiadiazol-2-amine

N-(5-m-tolyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023697-01-9

N-(5-m-tolyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 5-(3-methylphenyl)-1,3,4-thiadiazol-2-amine In dichloromethane for 0.5h; Irradiation; Further stages.;
85.6%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-amino-5-cyclopropyl-1,3,4-thiadiazole
57235-50-4

2-amino-5-cyclopropyl-1,3,4-thiadiazole

N-(5-cyclopropyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-87-8

N-(5-cyclopropyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-amino-5-cyclopropyl-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
84.6%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

5-(4-methoxy-phenyl)-[1,3,4]thiadiazol-2-ylamine
1014-25-1

5-(4-methoxy-phenyl)-[1,3,4]thiadiazol-2-ylamine

N-(5-(4-methoxyphenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-99-2

N-(5-(4-methoxyphenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 5-(4-methoxy-phenyl)-[1,3,4]thiadiazol-2-ylamine In dichloromethane for 0.5h; Irradiation; Further stages.;
84.6%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine
59565-54-7

5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine

N-(5-o-tolyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-91-4

N-(5-o-tolyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine In dichloromethane for 0.5h; Irradiation; Further stages.;
84.2%
ammonium thiocyanate

ammonium thiocyanate

5-methyl-1,3,4-thiadiazol-2-amine
108-33-8

5-methyl-1,3,4-thiadiazol-2-amine

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

N-(5-methyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023697-05-3

N-(5-methyl-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 5-methyl-1,3,4-thiadiazol-2-amine In dichloromethane for 0.5h; Irradiation; Further stages.;
83.6%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2,4-dichlorobenzohydrazide
5814-06-2

2,4-dichlorobenzohydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2,4-dichlorophenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2,4-dichlorophenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;83.5%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-methylbenzohydrazide
7658-80-2

2-methylbenzohydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2-methylphenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2-methylphenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;83.5%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

3-methylbenzoyl hydrazine
13050-47-0

3-methylbenzoyl hydrazine

1-(5-methylisoxazoyl-4-carbonyl)-4-(3-methylphenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(3-methylphenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;83.5%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

p-toluic hydrazide
3619-22-5

p-toluic hydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;83.5%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

2-Amino-5-(2-fluorophenyl)-1,3,4-thiadiazole
59565-51-4

2-Amino-5-(2-fluorophenyl)-1,3,4-thiadiazole

N-(5-(2-fluorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-93-6

N-(5-(2-fluorophenyl)-1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: 2-Amino-5-(2-fluorophenyl)-1,3,4-thiadiazole In dichloromethane for 0.5h; Irradiation; Further stages.;
83.5%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

Nicotinic acid hydrazide
553-53-7

Nicotinic acid hydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2-nicotinoyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(2-nicotinoyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;83.2%
[1,3,4]Thiadiazol-2-ylamin
4005-51-0

[1,3,4]Thiadiazol-2-ylamin

ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

N-(1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea
1023696-83-4

N-(1,3,4-thiadiazole-2-yl)-N'-(5-methylisoxazoyl)thiourea

Conditions
ConditionsYield
Stage #1: ammonium thiocyanate; 5-methylisoxazole-4-carbonyl chloride; polyethylene glycol-600 In dichloromethane at 20℃; for 0.333333h; Irradiation;
Stage #2: [1,3,4]Thiadiazol-2-ylamin In dichloromethane for 0.5h; Irradiation; Further stages.;
82.6%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

1-(3-amino-7-methoxy-benzofuran-2-yl)-ethanone
916329-09-4

1-(3-amino-7-methoxy-benzofuran-2-yl)-ethanone

N-(2-acetyl-7-methoxybenzofuran-3-yl)-5-methylisoxazole-4-carboxamide
803684-85-7

N-(2-acetyl-7-methoxybenzofuran-3-yl)-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 2h;81.9%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

3-aminobenzofuran-2-carboxamide
54802-10-7

3-aminobenzofuran-2-carboxamide

N-(2-carbamoylbenzofuran-3-yl)-5-methylisoxazole-4-carboxamide
688756-93-6

N-(2-carbamoylbenzofuran-3-yl)-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 2h;80.7%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

4-chlorobenzoic acid hydrazide
536-40-3

4-chlorobenzoic acid hydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-chlorophenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-chlorophenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;80.1%
5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

N-[6-(3-amino-4-methylphenoxy)imidazo[1,2-b]pyridazin-2-yl]cyclopropanecarboxamide
1005780-53-9

N-[6-(3-amino-4-methylphenoxy)imidazo[1,2-b]pyridazin-2-yl]cyclopropanecarboxamide

N-[5-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-2-methylphenyl]-5-methylisoxazole-4-carboxamide
1005782-77-3

N-[5-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-2-methylphenyl]-5-methylisoxazole-4-carboxamide

Conditions
ConditionsYield
With 1-methyl-pyrrolidin-2-one80%
ammonium thiocyanate

ammonium thiocyanate

5-methylisoxazole-4-carbonyl chloride
67305-24-2

5-methylisoxazole-4-carbonyl chloride

4-fluorobenzoyl hydrazide
456-06-4

4-fluorobenzoyl hydrazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-fluorophenyl)thiosemicarbazide

1-(5-methylisoxazoyl-4-carbonyl)-4-(4-fluorophenyl)thiosemicarbazide

Conditions
ConditionsYield
With PEG-600 In dichloromethane at 20℃; for 1.5h; ultrasonic irradiation;79.2%

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