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Conditions | Yield |
---|---|
With chlorine at 60 - 180℃; for 13.5h; Temperature; | 95.2% |
With chlorine at 80 - 180℃; Irradiation; | 87.6% |
With chlorine at 150℃; Irradiation; |
Conditions | Yield |
---|---|
With chlorine at 100℃; Irradiation; |
Conditions | Yield |
---|---|
With hydrogenchloride; zinc(II) chloride |
formaldehyd
toluene
A
1,4-bis(trichloromethyl)benzene
B
o-dichloromethyltrichloromethylbenzene
Conditions | Yield |
---|---|
With hydrogenchloride; zinc(II) chloride at 75℃; |
Conditions | Yield |
---|---|
With aluminium trichloride |
Conditions | Yield |
---|---|
Licht; |
methanol
1,4-bis(trichloromethyl)benzene
1,4-benzenedicarboxylic acid dimethyl ester
Conditions | Yield |
---|---|
at 20℃; for 6h; UV-irradiation; | 99% |
With zinc(II) chloride |
1,4-bis(trichloromethyl)benzene
2-amino-phenol
1,4-bis(2-benzoxazolyl)benzene
Conditions | Yield |
---|---|
With PPA at 100 - 150℃; for 6h; Addition; | 94% |
1,4-bis(trichloromethyl)benzene
2-amino-benzenethiol
1,4-bis(benzothiazol-2-yl)benzene
Conditions | Yield |
---|---|
With PPA at 100 - 150℃; for 6h; Addition; | 94% |
Conditions | Yield |
---|---|
With hydrogen fluoride at 150℃; under 77574.3 Torr; for 7h; | 75% |
With hydrogen fluoride at 150 - 210℃; | |
With hydrogen fluoride; antimonypentachloride at 20℃; | |
With hydrogen fluoride at 150 - 210℃; |
1,4-bis(trichloromethyl)benzene
4-trichloromethylbenzoyl chloride
Conditions | Yield |
---|---|
With isophthalic acid; zinc(II) chloride at 185℃; for 4.5h; | 56% |
With iron(III) chloride | |
With antimonypentachloride; water at 125 - 135℃; | |
With water; iron(III) chloride at 125 - 135℃; |
1,4-bis(trichloromethyl)benzene
formic acid hydrazide
p-phenylene-2,2′-bis-1,3,4-oxadiazole
Conditions | Yield |
---|---|
With pyridine In ethanol for 34h; Heating; | 47% |
Conditions | Yield |
---|---|
With pyridine In ethanol for 27h; Heating; | 41% |
1,4-bis(trichloromethyl)benzene
triethylamine
N1,N1,N4,N4-tetraethylterephthalamide
Conditions | Yield |
---|---|
With heptamethyl Coβ-perchlorato-cob(II)yrinate; tetrabutylammonium perchlorate In acetonitrile at 20℃; for 3h; Electrolysis; | 41% |
Conditions | Yield |
---|---|
With pyridine In ethanol for 19h; Heating; | 38% |
1,4-bis(trichloromethyl)benzene
N-amino-(4-nitrophenyl)carboxamide
5,5'-di(4-nitrophenyl)-1,4-phenylenebis-1,3,4-oxadiazole
Conditions | Yield |
---|---|
With pyridine In ethanol for 20h; Heating; | 36% |
1,4-bis(trichloromethyl)benzene
benzoic acid hydrazide
5,5'-diphenyl-1,4-phenylenebis-1,3,4-oxadiazole
Conditions | Yield |
---|---|
With pyridine In ethanol for 21h; Heating; | 35% |
dicobalt octacarbonyl
1,4-bis(trichloromethyl)benzene
Conditions | Yield |
---|---|
In tetrahydrofuran thermal react. of p-(Cl3C)2C6H4 with Co2(CO)8 in THF; ppt. is washed with CH2Cl2, dried in vac., elem. anal.; | 10% |
1,4-bis(trichloromethyl)benzene
A
1-(chlorodifluoromethyl)-4-(trifluoromethyl)benzene
B
1,4-bis-(difluorochloromethyl)-benzene
C
1-fluorodichloromethyl-4-difluorochloromethyl-benzene
Conditions | Yield |
---|---|
With hydrogen fluoride In 1,2-dichloro-ethane at 45℃; under 2280.15 Torr; for 10h; | A 3.3% B n/a C 4% |
maleic anhydride
1,4-bis(trichloromethyl)benzene
(E)-3-Ureido-but-2-enoic acid ethyl ester
terephthaloyl chloride
Conditions | Yield |
---|---|
at 140℃; |
propan-1-ol
1,4-bis(trichloromethyl)benzene
terephthalic acid dipropyl ester
Conditions | Yield |
---|---|
With zinc(II) chloride |
Conditions | Yield |
---|---|
With zinc(II) chloride |
2-methyl-propan-1-ol
1,4-bis(trichloromethyl)benzene
diisobutyl terephthalate
Conditions | Yield |
---|---|
With zinc(II) chloride |
Conditions | Yield |
---|---|
With titanium(IV) oxide | |
With maleic acid; zinc(II) chloride | |
With water; iron(III) chloride at 125 - 140℃; | |
With aluminium trichloride; water at 125 - 140℃; | |
at 125℃; for 1h; Temperature; |
Conditions | Yield |
---|---|
With zinc(II) chloride |
chloro-trimethyl-silane
1,4-bis(trichloromethyl)benzene
α,α,α,α',α',α'-hexakis(trimethylsilyl)-1,4-xylol
Conditions | Yield |
---|---|
With magnesium | |
With magnesium 1.) THF, 2.) THF, reflux, 70 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
iron(III) chloride In chlorobenzene at 115℃; Rate constant; Kinetics; Mechanism; activation energy, reaction order; |
1,4-bis(trichloromethyl)benzene
1,1,2,2-Tetrachlor-1,2-bis-<4-trichlormethyl-phenyl>-aethan
Conditions | Yield |
---|---|
With pyridine; copper |
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