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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiry2-(4-methoxy-3-prop-2-enyl-phenyl)-4-prop-2-enyl-phenol cas 68592-15-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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4-O-MethylhonokiolAppearance:Oil Storage:4℃ Package:Brown reagent bottle with plastic screw cap Application:analysis,activity test,Botanical Reference Materials,Standard materials Transportation:By express (Door to door) such as FEDEX, DHL, EMS for s
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inquiry4-allyl-2-bromo-phenol
methylhonokiol
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; ruphos In 1,2-dimethoxyethane; water at 130℃; for 0.166667h; Suzuki-Miyaura coupling; Microwave irradiation; | 72% |
With palladium diacetate; potassium carbonate; ruphos In 1,2-dimethoxyethane; water at 130℃; Reagent/catalyst; Solvent; Temperature; Suzuki-Miyaura Coupling; Sealed tube; Microwave irradiation; | 72% |
4-allyl-2-bromo-phenol
4-methoxy-3-allyl-1-phenylboronic acid
methylhonokiol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In 1,2-dimethoxyethane; water Suzuki coupling; Reflux; Inert atmosphere; | 52% |
2-allyl-4-bromo-1-methoxybenzene
1-allyl-4-oxocyclohexa-2,5-dienylethanoate
methylhonokiol
Conditions | Yield |
---|---|
Stage #1: 2-allyl-4-bromo-1-methoxybenzene With magnesium; ethylene dibromide In diethyl ether for 1h; Reflux; Stage #2: 1-allyl-4-oxocyclohexa-2,5-dienylethanoate In diethyl ether at 0℃; for 0.5h; | 50% |
Honokiol
methyl iodide
A
3,5′-diallyl-2′-methoxy-[1,1′-biphenyl]-4-ol
B
methylhonokiol
C
Dimethylhonokiol
Conditions | Yield |
---|---|
With potassium carbonate In water; dimethyl sulfoxide at 60℃; | A 50% B 20% C 15% |
With sodium hydroxide In water; dimethyl sulfoxide at 60℃; | A 46% B 20% C 30% |
With caesium carbonate In water; dimethyl sulfoxide at 60℃; Reagent/catalyst; | A 21% B 35% C 15% |
Honokiol
diazomethyl-trimethyl-silane
A
3,5′-diallyl-2′-methoxy-[1,1′-biphenyl]-4-ol
B
methylhonokiol
C
Dimethylhonokiol
Conditions | Yield |
---|---|
In methanol | A 13% B 13% C 47% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 41% |
2-[(2R,4aR,8R,8aR)-8-(5,3'-Diallyl-4'-methoxy-biphenyl-2-yloxy)-4a,8-dimethyl-decahydro-naphthalen-2-yl]-propan-2-ol
A
methylhonokiol
B
eudesm-4-en-11-ol
Conditions | Yield |
---|---|
With trifluoroacetic acid In benzene for 10h; Ambient temperature; | A 6 mg B 2 mg |
eudeshonokiol B
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / 36 h / Ambient temperature 2: 6 mg / CF3COOH / benzene / 10 h / Ambient temperature View Scheme |
Estragole
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: boron trichloride-dimethyl sulfide / trans-1,2-dichloroethylene; dichloromethane / 18 h / Reflux 2.1: acetic acid / 8 h 3.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux 3.2: 0.5 h / 0 °C View Scheme | |
Multi-step reaction with 3 steps 1: methyl magnesium iodide / 180 °C 2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; isopropylmagnesium chloride / diethyl ether / 24 h / -78 - 20 °C 3: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation View Scheme | |
Multi-step reaction with 3 steps 1.1: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere 2.1: isopropylmagnesium chloride / diethyl ether / 1.05 h / -78 °C / Inert atmosphere 2.2: 21 h / -78 - 20 °C 3.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme |
4-(prop-2-enyl)phenol
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetic acid / 8 h 2.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux 2.2: 0.5 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; isopropylmagnesium chloride / diethyl ether / 24 h / -78 - 20 °C 2: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation View Scheme | |
Multi-step reaction with 2 steps 1.1: isopropylmagnesium chloride / diethyl ether / 1.05 h / -78 °C / Inert atmosphere 1.2: 21 h / -78 - 20 °C 2.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: isopropylmagnesium chloride / diethyl ether / 0.67 h / -78 °C / Inert atmosphere 1.2: 2.5 h / 20 °C / Inert atmosphere 2.1: potassium carbonate; palladium diacetate; ruphos / 1,2-dimethoxyethane; water / 130 °C / Sealed tube; Microwave irradiation View Scheme |
5-bromo-2-methoxy-benzyl alcohol
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Oxalyl bromide; Triphenylphosphine oxide / chloroform / 7 h 2.1: [2,2]bipyridinyl; copper(l) iodide / benzene / 5 - 20 °C 3.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux 3.2: 0.5 h / 0 °C View Scheme |
4-bromo-2-(bromomethyl)-1-methoxybenzene
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: [2,2]bipyridinyl; copper(l) iodide / benzene / 5 - 20 °C 2.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux 2.2: 0.5 h / 0 °C View Scheme |
2-allyl-4-bromophenol
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: potassium carbonate / acetone / 0.5 h 1.2: 4 h / 20 °C 2.1: n-butyllithium; Triisopropyl borate / tetrahydrofuran; hexane / 2 h / -78 - 20 °C 2.2: 0.5 h / 20 °C 3.1: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation View Scheme | |
Multi-step reaction with 4 steps 1.1: potassium carbonate / acetone / 0.25 h / Inert atmosphere 1.2: 1.5 h / Reflux 2.1: n-butyllithium / tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere 2.2: 2 h / -78 - 20 °C 3.1: hydrogenchloride; water / tetrahydrofuran 4.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium carbonate / acetone / 0.5 h 1.2: 4 h / 20 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 20 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: potassium carbonate; palladium diacetate; ruphos / 1,2-dimethoxyethane; water / 130 °C / Sealed tube; Microwave irradiation View Scheme |
2-allyl-4-bromo-1-methoxybenzene
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-butyllithium; Triisopropyl borate / tetrahydrofuran; hexane / 2 h / -78 - 20 °C 1.2: 0.5 h / 20 °C 2.1: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation View Scheme | |
Multi-step reaction with 3 steps 1.1: n-butyllithium / tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 - 20 °C 2.1: hydrogenchloride; water / tetrahydrofuran 3.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme |
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride; water / tetrahydrofuran 2: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme |
4-(allyloxy)bromobenzene
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Reflux 2.1: potassium carbonate / acetone / 0.25 h / Inert atmosphere 2.2: 1.5 h / Reflux 3.1: n-butyllithium / tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere 3.2: 2 h / -78 - 20 °C 4.1: hydrogenchloride; water / tetrahydrofuran 5.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere View Scheme |
Honokiol
dimethyl sulfate
A
3,5′-diallyl-2′-methoxy-[1,1′-biphenyl]-4-ol
B
methylhonokiol
Conditions | Yield |
---|---|
With potassium hydroxide Microwave irradiation; |
4-bromo-phenol
methylhonokiol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / acetone / 5 h / Reflux 2.1: potassium carbonate / acetone / 0.5 h 2.2: 4 h / 20 °C 3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 20 °C / Inert atmosphere 3.2: 0.5 h / Inert atmosphere 4.1: potassium carbonate; palladium diacetate; ruphos / 1,2-dimethoxyethane; water / 130 °C / Sealed tube; Microwave irradiation View Scheme |
methylhonokiol
4'-methoxy-3',5-di-n-propyl-[1,1'-biphenyl]-2-ol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; | 99% |
With palladium 10% on activated carbon; hydrogen In methanol for 1h; | 98% |
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; under 760.051 Torr; for 21h; | 97% |
With palladium on activated charcoal; hydrogen | 97% |
methylhonokiol
4'-O-methyl-3-nitro-honokiol
Conditions | Yield |
---|---|
With nitric acid In hexane; water at 20℃; | 99% |
With nitric acid In ethyl acetate |
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 20℃; for 3h; | 98% |
2-methyl-but-2-ene
methylhonokiol
4'-methoxy-3',5-bis(3-methylbut-2-en-1-yl)-[1,1'-biphenyl]-2-ol
Conditions | Yield |
---|---|
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In dichloromethane for 24h; Inert atmosphere; | 95% |
acetic anhydride
methylhonokiol
3',5-diallyl-4'-methoxy-[1,1'-biphenyl]-2-yl acetate
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 0.333333h; Inert atmosphere; | 93% |
With pyridine | 87% |
Conditions | Yield |
---|---|
With caesium carbonate; triethylamine; potassium iodide In acetone at 20℃; for 24h; | 89% |
methylhonokiol
4'-methoxy-3',5-bis(oxiran-2-ylmethyl)-[1,1'-biphenyl]-2-ol
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In benzene | 87% |
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid In dichloromethane at -78 - 20℃; for 24h; Inert atmosphere; | 53% |
methylhonokiol
prenyl bromide
3',5-diallyl-4'-methoxy-2-((3-methylbut-2-en-1-yl)oxy)-1,1'-biphenyl
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: prenyl bromide In N,N-dimethyl-formamide at 20℃; for 5h; | 86% |
bis(trichloromethyl) carbonate
methylhonokiol
benzylamine
3',5-diallyl-4'-methoxy-[1,1'-biphenyl]-2-yl benzylcarbamate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; methylhonokiol With pyridine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: benzylamine In dichloromethane at 20℃; for 12h; Inert atmosphere; | 81% |
morpholine
bis(trichloromethyl) carbonate
methylhonokiol
3',5-diallyl-4'-methoxy-[1,1'-biphenyl]-2-yl morpholine-4-carboxylate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; methylhonokiol With pyridine In dichloromethane at 0 - 20℃; for 2h; Stage #2: morpholine In dichloromethane at 20℃; for 12h; | 68% |
methylhonokiol
3'-bromo-3,5'-diallyl-2'-hydroxy-4-methoxy-1,1'-biphenyl
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With isopropylmagnesium chloride In tetrahydrofuran; diethyl ether at -78℃; for 0.666667h; Inert atmosphere; Stage #2: With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In tetrahydrofuran; diethyl ether at 20℃; for 2h; Inert atmosphere; | 66% |
bis(trichloromethyl) carbonate
methylhonokiol
1-amino-2-propene
3',5-diallyl-4'-methoxy-[1,1'-biphenyl]-2-yl allylcarbamate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; methylhonokiol With pyridine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: 1-amino-2-propene In dichloromethane at 20℃; for 12h; Inert atmosphere; | 65% |
methylhonokiol
isopropyl bromide
3',5-diallyl-2-isopropoxy-4'-methoxy-1,1'-biphenyl
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: isopropyl bromide In N,N-dimethyl-formamide at 20℃; for 4h; | 60% |
bis(trichloromethyl) carbonate
methylhonokiol
benzyl-methyl-amine
3',5-diallyl-4'-methoxy-[1,1'-biphenyl]-2-yl benzyl(methyl)carbamate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; methylhonokiol With pyridine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: benzyl-methyl-amine In dichloromethane at 20℃; for 12h; Inert atmosphere; | 59% |
methylhonokiol
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile Reflux; | 48% |
With potassium carbonate In acetone at 50℃; |
methylhonokiol
3',5-di-(2,3-dihydroxypropyl)-4'-methoxy-biphenyl-2-ol
Conditions | Yield |
---|---|
With pyridine; osmium(VIII) oxide; trimethylamine-N-oxide In water; tert-butyl alcohol for 2h; Inert atmosphere; Reflux; | 40% |
methylhonokiol
5-allyl-3'-(3-hydroxypropyl)-4'-methoxy-[1,1'-biphenyl]-2-ol
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With borane-THF In tetrahydrofuran at 0 - 20℃; for 2.08333h; Inert atmosphere; Stage #2: With dihydrogen peroxide; sodium hydroxide In tetrahydrofuran; water at -10 - 70℃; for 2h; Inert atmosphere; | 36% |
methylhonokiol
3',5-diallyl-3-chloro-4'-methoxy-[1,1'-biphenyl]-2-ol
Conditions | Yield |
---|---|
Stage #1: methylhonokiol With isopropylmagnesium chloride In tetrahydrofuran; diethyl ether at -78 - 20℃; for 0.666667h; Inert atmosphere; Stage #2: With 1,3-dichloro-5,5-dimethylhydantoin In tetrahydrofuran; diethyl ether at 20℃; for 2h; Inert atmosphere; | 32% |
methylhonokiol
A
4'-methoxy-3'-((Z)-1-propenyl)-5-(2-propenyl)biphenyl-2-ol
B
4'-methoxy-3'-((E)-1-propenyl)-5-(2-propenyl)biphenyl-2-ol
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran for 21h; Inert atmosphere; Reflux; | |
With potassium tert-butylate In tetrahydrofuran |
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