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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Perchloryl fluoride

Cas:7616-94-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Perchloryl fluoride

Cas:7616-94-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

PERCHLORYL FLUORIDE

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

PERCHLORYL FLUORIDE

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

Hot selling products CAS 7616-94-6 with fast delivery

Cas:7616-94-6

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

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Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

7616-94-6

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Trading Company

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Nanjing Raymon Biotech Co., Ltd.

PERCHLORYL FLUORIDEAppearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier li

PERCHLORYL FLUORIDE

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Trading Company

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Sparrow Chemical Co.,Ltd

Our company provides the best service for our customers. Under the premise of ensuring quality and delivery date, give customers the best price. The company is more willing to meet our customers. If you want to visit our factories and warehouses, we

Perchlorylfluoride

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Trading Company

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Chemical Co.Ltd

PERCHLORYL FLUORIDEAppearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them fr

PERCHLORYL FLUORIDE

Cas:7616-94-6

Min.Order:0

Negotiable

Type:Trading Company

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Trans Intl Chem Shop

99

Perchloryl fluoride

Cas:7616-94-6

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Synthetic route

potassium perchlorate

potassium perchlorate

antimony pentafluoride
7783-70-2

antimony pentafluoride

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) heating at 105°C;;97%
In neat (no solvent) heating at 105°C;;97%
potassium chlorate
3811-04-9

potassium chlorate

fluorine
7782-41-4

fluorine

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) below -20°C;; passing ClO3F over KI; cooling at -183°C; distillation at -183 - 130°C in vacuum;;60%
In neat (no solvent) below -20°C;; passing ClO3F over KI; cooling at -183°C; distillation at -183 - 130°C in vacuum;;60%
potassium chlorate
3811-04-9

potassium chlorate

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

dichlorine hexaoxide

dichlorine hexaoxide

C

chlorine dioxide
10049-04-4, 25052-55-5

chlorine dioxide

D

chlorine monofluoride
7790-89-8

chlorine monofluoride

E

chlorine
7782-50-5

chlorine

Conditions
ConditionsYield
In neat (no solvent) byproducts: O2; transport reaction: passing F2-N2 mixture over KClO3 at 25 - 60°C;; washing with NaOH; passing ClO3F through Na2S2O3 soln.; drying over NaOH and P2O5;;A 45%
B n/a
C n/a
D n/a
E n/a
perchloric acid
7601-90-3

perchloric acid

antimony pentafluoride
7783-70-2

antimony pentafluoride

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In water reaction of 60 - 62% aq. HClO4 with SbF5 at 90 - 100°C;;36%
In water reaction of 60 - 62% aq. HClO4 with SbF5 at 90 - 100°C;;36%
In neat (no solvent) reaction of 1 mol perchlorate and 3 - 10 mol SbF5 at 100 - 120°C; cooling down;; washing with Na2S2O3; condenstion at temp. of liquid air;;36-53
perchloric acid
7601-90-3

perchloric acid

fluorine
7782-41-4

fluorine

A

difluoroether
7783-41-7

difluoroether

B

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In water
dichlorine hexaoxide

dichlorine hexaoxide

fluorine
7782-41-4

fluorine

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) at 20 - 40°C;;0%
In neat (no solvent) at 20 - 40°C;;0%
hydrogen fluoride
7664-39-3

hydrogen fluoride

sodium perchlorate

sodium perchlorate

A

difluoroether
7783-41-7

difluoroether

B

perchloryl fluoride
7616-94-6

perchloryl fluoride

C

hydrogen
1333-74-0

hydrogen

D

oxygen
80937-33-3

oxygen

E

chlorine
7782-50-5

chlorine

Conditions
ConditionsYield
In neat (no solvent) Electrolysis; electrolysis of NaClO4 soln. in HF at 0 - 30°C;; condensation with liquid air; washing with Na2S2O3 soln.;;
In neat (no solvent) Electrolysis; electrolysis of NaClO4 soln. in HF at 0 - 30°C;; condensation with liquid air; washing with Na2S2O3 soln.;;
sodium perchlorate

sodium perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
Carbonyl fluoride
353-50-4

Carbonyl fluoride

lithium perchlorate

lithium perchlorate

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
With cesium fluoride byproducts: CO2, Cl2; A mixture of LiClO4 and CsF (as HF getter) was treated in a stainless steel cylinder with COF2; heating up to 120°C;0%
lithium perchlorate

lithium perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
chlorine trifluoride
7790-91-2

chlorine trifluoride

uranium(VI) trioxide

uranium(VI) trioxide

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

uranium hexafluoride
7783-81-5

uranium hexafluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
chlorine trifluoride
7790-91-2

chlorine trifluoride

uranium oxide

uranium oxide

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

uranium hexafluoride
7783-81-5

uranium hexafluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
chlorine trifluoride
7790-91-2

chlorine trifluoride

uranium dioxide

uranium dioxide

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

uranium hexafluoride
7783-81-5

uranium hexafluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
boron trifluoride
7637-07-2

boron trifluoride

potassium perchlorate

potassium perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
hydrogen fluoride
7664-39-3

hydrogen fluoride

potassium perchlorate

potassium perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
potassium perchlorate

potassium perchlorate

antimony(III) fluoride
7783-56-4

antimony(III) fluoride

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
potassium perchlorate

potassium perchlorate

antimony pentafluoride
7783-70-2

antimony pentafluoride

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) reaction of 1 mol perchlorate and 3 - 10 mol SbF5 at 100 - 120°C; cooling down;; washing with Na2S2O3; condenstion at temp. of liquid air;;36-53
potassium perchlorate

potassium perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In not given
In fluorosulphonic acid mixt. of KClO4 in fluorosulfonic acid stirred under gradual warming up to about 95°C; FClO3 was flushed with moderate N2 flow; purified through column filled with sodium thiosulfate and ascarite;
In neat (no solvent) heating KClO4 and HSO3F (10:100) at 110°C;;52-60
magnesium(II) perchlorate

magnesium(II) perchlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
In neat (no solvent) heating perchlorate with excess of HSO3F;;>80
chloryl fluoride
13637-83-7

chloryl fluoride

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
With water In water byproducts: H2;
potassium chlorate
3811-04-9

potassium chlorate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) heating KClO3 and 98% HSO3F at 85°C;; passing ClO3F through thiosulfate soln. and over solid KOH; condensation at temp. of liquid air;;
In neat (no solvent) heating KClO3 and 98% HSO3F at 85°C;; passing ClO3F through thiosulfate soln. and over solid KOH; condensation at temp. of liquid air;;
perchloric anhydride
12015-53-1

perchloric anhydride

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

chloryl fluoride
13637-83-7

chloryl fluoride

C

chlorine monofluoride
7790-89-8

chlorine monofluoride

D

oxygen
80937-33-3

oxygen

E

chlorine
7782-50-5

chlorine

Conditions
ConditionsYield
In neat (no solvent) Kinetics; thermal decompn. of Cl2O7 in presence of enough amounts of F2 at 100 - 120°C; reaction mechanism described;;
perchloric anhydride
12015-53-1

perchloric anhydride

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

chloryl fluoride
13637-83-7

chloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) thermal decompn. in prescence of F2;;
perchloric anhydride
12015-53-1

perchloric anhydride

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

chloryl fluoride
13637-83-7

chloryl fluoride

C

chlorine monofluoride
7790-89-8

chlorine monofluoride

Conditions
ConditionsYield
In neat (no solvent) decompn. of Cl2O7 in presence of F2 at 100 - 120°C;;
In neat (no solvent) decompn. of Cl2O7 in presence of F2 at 100 - 120°C;;
perchloric anhydride
12015-53-1

perchloric anhydride

fluorine
7782-41-4

fluorine

perchloryl fluoride
7616-94-6

perchloryl fluoride

Conditions
ConditionsYield
In neat (no solvent) formation as intermediate at 100 - 120°C;;
In neat (no solvent) formation as intermediate at 100 - 120°C;;
potassium chlorate
3811-04-9

potassium chlorate

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

dichlorine hexaoxide

dichlorine hexaoxide

Conditions
ConditionsYield
In neat (no solvent) formation of Cl2O6 as by-product;;
In neat (no solvent) formation of Cl2O6 as by-product;;
potassium chlorate
3811-04-9

potassium chlorate

fluorine
7782-41-4

fluorine

A

perchloryl fluoride
7616-94-6

perchloryl fluoride

B

chloryl fluoride
13637-83-7

chloryl fluoride

C

chlorine monofluoride
7790-89-8

chlorine monofluoride

D

chlorine
7782-50-5

chlorine

Conditions
ConditionsYield
In neat (no solvent) at -40°C;;
In neat (no solvent) at -40 or 100°C;; fractionated distillation;;
In neat (no solvent) at -40°C;;
In neat (no solvent) at -40 or 100°C;; fractionated distillation;;
perchloryl fluoride
7616-94-6

perchloryl fluoride

potassium trinitromethanide
14268-23-6

potassium trinitromethanide

fluorotrinitromethane
1840-42-2

fluorotrinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;77%
In N,N-dimethyl-formamide77%
In acetone77%
perchloryl fluoride
7616-94-6

perchloryl fluoride

trinitromethane; sodium salt

trinitromethane; sodium salt

fluorotrinitromethane
1840-42-2

fluorotrinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;77%
In N,N-dimethyl-formamide77%
In acetone77%
In methanol at 20°C 11 h;17.7%
perchloryl fluoride
7616-94-6

perchloryl fluoride

trinitromethane; ammonium salt
19836-32-9

trinitromethane; ammonium salt

fluorotrinitromethane
1840-42-2

fluorotrinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;77%
In N,N-dimethyl-formamide77%
In acetone77%
perchloryl fluoride
7616-94-6

perchloryl fluoride

<4-(Dimethylamino)phenyl>trimethylstannan

<4-(Dimethylamino)phenyl>trimethylstannan

trimethyltin fluoride

trimethyltin fluoride

Conditions
ConditionsYield
In tetrahydrofuran byproducts: dimethylphenylamine, N-(4-chloriohenyl)-N-methyl-formamide; dimethyl-(4-trimethylstannanylphenyl)amine dissolved in dry THF was cooled at -60°C; FClO3/N2 mixt. passed through soln. for about 35 min; soln. warmed up to ambient temp. under stirring and stirred at about 60°C for 20 min (closed ....; isolated by semi-preparative thin-layer chromy. (silica gel 60, petroleum ether/ethyl acetate 10:1);52%
perchloryl fluoride
7616-94-6

perchloryl fluoride

trinitromethane; lithium salt

trinitromethane; lithium salt

fluorotrinitromethane
1840-42-2

fluorotrinitromethane

Conditions
ConditionsYield
In methanol at 20°C 10 h;47%
perchloryl fluoride
7616-94-6

perchloryl fluoride

(4-methoxyphenyl)trimethylstannane
940-00-1

(4-methoxyphenyl)trimethylstannane

A

bis(4-methoxyphenyl)dimethylstannane
61726-36-1

bis(4-methoxyphenyl)dimethylstannane

B

trimethyltin fluoride

trimethyltin fluoride

Conditions
ConditionsYield
In tetrahydrofuran byproducts: methoxybenzene; (4-methoxyphenyl)trimethylstannane dissolved in dry THF was cooled at -60°C; FClO3/N2 mixt. passed through soln. for about 35 min; soln. warmed up to ambient temp. under stirring and stirred at about 60°C for 20 min (closed conditions) or; isolated by semi-preparative thin-layer chromy. (silica gel 60, petroleum ether/ethyl acetate 10:1);A n/a
B 40%
perchloryl fluoride
7616-94-6

perchloryl fluoride

A

trimethyltin fluoride

trimethyltin fluoride

B

bis-(4-(tert-butoxycarbonylamino)phenyl)dimethylstannane

bis-(4-(tert-butoxycarbonylamino)phenyl)dimethylstannane

Conditions
ConditionsYield
In tetrahydrofuran byproducts: phenylcarbamic acid tert-butyl ester; (4-trimethylstannanylphenyl)carbamic acid tert-butyl ester dissolved in dry THF was cooled at -60°C; FClO3/N2 mixt. passed through soln. for about 35 min; soln. warmed up to ambient temp. under stirring and stirred at about 60°C for 20 min; isolated by semi-preparative thin-layer chromy. (silica gel 60, petroleum ether/ethyl acetate 10:1);A 40%
B n/a
perchloryl fluoride
7616-94-6

perchloryl fluoride

Na(1+)*CBr(NO2)2(1-)=NaCBr(NO2)2
19282-10-1

Na(1+)*CBr(NO2)2(1-)=NaCBr(NO2)2

fluoro bromo dinitromethane
22632-20-8

fluoro bromo dinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;36%
In N,N-dimethyl-formamide36%
In acetone36%
perchloryl fluoride
7616-94-6

perchloryl fluoride

bromo-dinitro-methane; ammonium salt

bromo-dinitro-methane; ammonium salt

fluoro bromo dinitromethane
22632-20-8

fluoro bromo dinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;36%
In N,N-dimethyl-formamide36%
In acetone36%
perchloryl fluoride
7616-94-6

perchloryl fluoride

bromo-dinitro-methane; potassium salt
24280-12-4

bromo-dinitro-methane; potassium salt

fluoro bromo dinitromethane
22632-20-8

fluoro bromo dinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;36%
In N,N-dimethyl-formamide36%
In acetone36%
perchloryl fluoride
7616-94-6

perchloryl fluoride

Na(1+)*CCl(NO2)2(1-)=NaCCl(NO2)2
19282-07-6

Na(1+)*CCl(NO2)2(1-)=NaCCl(NO2)2

fluorochlorodinitromethane
19845-51-3

fluorochlorodinitromethane

Conditions
ConditionsYield
In further solvent(s) in CH3O(CH2)2OCH3;33%
In N,N-dimethyl-formamide33%
In acetone33%

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