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inquiryChemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 4-Chloro-2-methoxyphenylboronic acid CAS 762287-57-0 IN STOCK 4-Chloro-2-methoxybenzeneboronic acid CAS 762287-57-0 762287-57-0
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/45.html Product Name 4-Chloro-2-methoxyphenylboronic acid CAS No. 762287-57-0
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inquiryo-Cresol CAS:762287-57-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceuti
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiry4-Chloro-2-methoxyphenylboronic acid Basic information Product Name: 4-Chloro-2-methoxyphenylboronic acid Synonyms: 4-CHLORO-2-METHOXYBENZENEBORONIC ACID;4-CHLORO-2-METHOXYPHENYLBORONIC ACID;4-Chloro-2-methoxyphenylboronic acid 762287-57-0;762
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryOur Company main product 一:suzuki reaction customization 二:Boronic acid derivative ①:phenylboronic acid derivative ②:Phenylboronic acid pinacol ester derivative ③:Potassium phenyltrifluoroborate derivative ④:Phenylboronic acid MIDA ester derivative
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inquiryPuyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiry2-bromo-5-chloroanisole
Trimethyl borate
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
Stage #1: 2-bromo-5-chloroanisole With n-butyllithium In tetrahydrofuran; hexane at -30℃; Inert atmosphere; Flow reactor; Stage #2: Trimethyl borate In tetrahydrofuran; hexane at -30℃; Inert atmosphere; Flow reactor; | 98% |
Stage #1: 2-bromo-5-chloroanisole With n-butyllithium In tetrahydrofuran at -78℃; for 0.666667h; Inert atmosphere; Stage #2: Trimethyl borate In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; | 73% |
Stage #1: 2-bromo-5-chloroanisole With n-butyllithium In tetrahydrofuran at -80℃; for 1h; Stage #2: Trimethyl borate In tetrahydrofuran at 20℃; | 70% |
Stage #1: 2-bromo-5-chloroanisole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: Trimethyl borate In tetrahydrofuran; hexane at 20℃; for 24h; | 50% |
2-bromo-5-chloroanisole
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
Stage #1: 2-bromo-5-chloroanisole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: With triisopropyl borate Stage #3: With hydrogenchloride In water; ethyl acetate |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With [Rh(OH)(cod)]2 In 1,4-dioxane; water at 80℃; for 2h; | 100% |
(4-chloro-2-methoxyphenyl)boronic acid
1-bromo-2,3-difluorobenzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 110℃; | 99% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 110℃; | 99% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 110℃; | 99% |
(4-chloro-2-methoxyphenyl)boronic acid
1,3-dibromo-2-fluorobenzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 110℃; | 98% |
With tetrakis(triphenylphosphine) palladium(0); tetrabutyl-ammonium chloride; potassium carbonate In ethanol; water; toluene at 78℃; for 8h; Inert atmosphere; | 76% |
2,3,5,6-tetrachloropyridine
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane for 6h; Inert atmosphere; Reflux; | 95% |
(4-chloro-2-methoxyphenyl)boronic acid
5-bromo-N-methyl-N-(2,2,6,6-tetramethylpiperidin-4-yl)-1,3,4-thiadiazol-2-amine
5-(4-chloro-2-methoxyphenyl)-N-methyl-N-(2,2,6,6-tetramethylpiperidin-4-yl)-1,3,4-thiadiazol-2-amine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water at 80℃; for 18h; Inert atmosphere; | 89% |
(4-chloro-2-methoxyphenyl)boronic acid
(4-chloro-2-hydroxyphenyl)boronic acid
Conditions | Yield |
---|---|
Stage #1: (4-chloro-2-methoxyphenyl)boronic acid With boron tribromide In dichloromethane at 20℃; for 1h; Stage #2: With water In dichloromethane | 87% |
Stage #1: (4-chloro-2-methoxyphenyl)boronic acid With boron tribromide In dichloromethane at -78 - 20℃; Inert atmosphere; Stage #2: With methanol In dichloromethane at -78℃; Inert atmosphere; | |
With boron tribromide In dichloromethane at 0 - 20℃; for 19h; |
(4-chloro-2-methoxyphenyl)boronic acid
2-[3-bromo-4-(2-fluorobenzyl)-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]-N-{1-methyl-1-[(3-trifluoromethyl)phenyl]ethyl}-acetamide
2-[3-(4-chloro-2-methoxyphenyl)-4-(2-fluorobenzyl)-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]-N-[1-methyl-1-(3-trifluoromethyl-phenyl)ethyl]-acetamide
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In water; N,N-dimethyl-formamide at 90℃; for 5h; Inert atmosphere; | 83% |
(4-chloro-2-methoxyphenyl)boronic acid
4-bromo-3-(4-hydroxyphenyl)thiophene-2-carbaldehyde
4-bromo-3-(4-hydroxyphenyl)thiophene-2-carbaldehyde
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene at 100℃; | 79% |
(4-chloro-2-methoxyphenyl)boronic acid
C19H15ClN2O2
Conditions | Yield |
---|---|
Stage #1: (4-chloro-2-methoxyphenyl)boronic acid; C19H15ClN2O2 In 1,4-dioxane at 20℃; for 0.0833333h; Suzuki-Miyaura Coupling; Inert atmosphere; Stage #2: With palladium diacetate; sodium carbonate; triphenylphosphine In 1,4-dioxane at 20 - 110℃; for 3.5h; Suzuki-Miyaura Coupling; Inert atmosphere; | 78% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water at 90℃; for 1h; Suzuki Coupling; Microwave irradiation; Inert atmosphere; | 78% |
(4-chloro-2-methoxyphenyl)boronic acid
(3aR,6aS)-tert-butyl 5-(6-chloropyridazin-3-yl)hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate In 1,4-dioxane; water at 90℃; Suzuki Coupling; Inert atmosphere; | 77% |
4-chloropyridine N-oxide
(4-chloro-2-methoxyphenyl)boronic acid
4-(4-chloro-2-methoxyphenyl)pyridine 1-oxide
Conditions | Yield |
---|---|
With potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In dimethyl sulfoxide at 120℃; for 3h; | 74% |
(4-chloro-2-methoxyphenyl)boronic acid
2-bromo-1-chlorobenzene
6-chloro-2'-chlorobiphenyl-2-yl methyl ether
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 82℃; Suzuki Coupling; | 73% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 100℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 71% |
(4-chloro-2-methoxyphenyl)boronic acid
1-iodo-4-bromo-naphthalene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; | 70% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 70℃; for 5h; | 64% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 70℃; for 5h; | 64% |
(4-chloro-2-methoxyphenyl)boronic acid
5-bromo-2-iodo-benzoic acid methyl ester
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 100℃; for 12h; | 64% |
(4-chloro-2-methoxyphenyl)boronic acid
methyl 2-(4-chloro-6-methyl-2-phenylpyrimidin-5-yl)pentanoate
methyl 2-(4-(4-chloro-2-methoxyphenyl)-6-methyl-2-phenylpyrimidin-5-yl)pentanoate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water for 2.5h; Sealed tube; | 60% |
(4-chloro-2-methoxyphenyl)boronic acid
5-amino-3-cyano-1-(2,6-dichloro-4-trifluoromethylphenyl)pyrazole
5-amino-4-(4-chloro-2-methoxyphenyl)-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-1H-pyrazole-3-carbonitrile
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; sodium hydrogencarbonate In ethanol; water at 80℃; for 18h; Inert atmosphere; | 60% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,4-dioxane; water at 105℃; for 8h; Inert atmosphere; | 53% |
(4-chloro-2-methoxyphenyl)boronic acid
3,3,3-trifluoro-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate In toluene at 110℃; for 10h; Schlenk technique; Inert atmosphere; | 49% |
(4-chloro-2-methoxyphenyl)boronic acid
3-bromo-7-methoxy-4-methylcoumarin
Conditions | Yield |
---|---|
With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; sodium carbonate In tetrahydrofuran; water at 95℃; Inert atmosphere; | 48% |
With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; sodium carbonate In tetrahydrofuran; water at 95℃; Inert atmosphere; | 48% |
(4-chloro-2-methoxyphenyl)boronic acid
4-(Bromomethyl)-2,5-difluoro-N-(methylsulfonyl)benzamide
4-(4-Chloro-2-methoxybenzyl)-2,5-difluoro-N-(methylsulfonyl)benzamide
Conditions | Yield |
---|---|
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 6h; Inert atmosphere; Reflux; | 36% |
(4-chloro-2-methoxyphenyl)boronic acid
5-bromo-N-(1,3,4-thiadiazol-2-yl)-3,4-dihydroisoquinoline-2(1H)-sulfonamide
(3,4-difluorophenyl)boronic acid
5-(3',4'-difluoro-3-methoxy-[1,1'-biphenyl]-4-yl)-N-(1,3,4-thiadiazol-2-yl)-3,4-dihydroisoquinoline-2(1H)-sulfonamide
Conditions | Yield |
---|---|
Stage #1: (4-chloro-2-methoxyphenyl)boronic acid; 5-bromo-N-(1,3,4-thiadiazol-2-yl)-3,4-dihydroisoquinoline-2(1H)-sulfonamide With potassium phosphate; bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II) In 1,4-dioxane; water at 150℃; for 0.5h; Microwave irradiation; Stage #2: (3,4-difluorophenyl)boronic acid In 1,4-dioxane; water at 150℃; for 0.5h; Microwave irradiation; Stage #3: With hydrogenchloride In 1,4-dioxane for 0.166667h; | 35% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,4-dioxane; water at 105℃; for 6h; Inert atmosphere; | 34% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate In 1,4-dioxane; water at 90℃; for 1h; Inert atmosphere; Microwave irradiation; | 23% |
(4-chloro-2-methoxyphenyl)boronic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate In 1,4-dioxane; water at 50℃; for 4h; Inert atmosphere; | 12.35% |
(4-bromo-2-chlorophenyl)(pyrrolidin-1-yl)methanone
(4-chloro-2-methoxyphenyl)boronic acid
1-[(3,5'-dichloro-2'-methoxy-[1,1'-biphenyl]-4-yl)carbonyl]-pyrrolidine
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; toluene for 16h; Heating / reflux; |
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