As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:78-99-9
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inquiryProName: 1,1-dichloropropane CasNo: 78-99-9 Appearance: detailed in specifications Application: An important raw material and intermed... DeliveryTime: prompt PackAge: according to the clients requirement Port: Shanghai ProductionCapacity: 1
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Conditions | Yield |
---|---|
at 400℃; bei der Chlorierung; |
propane
A
1,2-Dichloropropane
B
2,2-dichloropropane
C
1,1-dichloropropane
D
1,3-Dichloropropane
Conditions | Yield |
---|---|
at 400℃; Product distribution; thermische Chlorierung; | |
at 400℃; Product distribution; thermische Chlorierung; |
Conditions | Yield |
---|---|
With phosphorus pentachloride |
Conditions | Yield |
---|---|
With hydrogenchloride; iron(III) chloride at 25℃; im Dunkeln; |
Conditions | Yield |
---|---|
Irradiation; |
1-Chloropropane
A
1,2-Dichloropropane
B
1,1-dichloropropane
C
1,3-Dichloropropane
Conditions | Yield |
---|---|
With chlorine In 1,2-dichloro-benzene at 0℃; Product distribution; oth. temperatures; | |
With N-chloropiperidine; 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 30℃; Product distribution; Rate constant; Irradiation; relative rate constants, position selectivity, substrate selectivity; | |
With chlorine In benzene at -10.1℃; Product distribution; dependence of the selectivity of chlorination on the conc. of benzene; | |
With sulfuryl dichloride; dibenzoyl peroxide | |
With chlorine Ambient temperature; Irradiation; |
propionaldehyde
A
1,1-dichloropropane
B
N-chlorocarbonyl-carbonimidic acid dichloride
Conditions | Yield |
---|---|
With iron(III) chloride; perchloro-2-aza-1-propene |
Conditions | Yield |
---|---|
With chlorine at 305℃; |
propane
chlorine
tetraethyllead(IV)
A
1-Chloropropane
B
isopropyl chloride
C
1,1-dichloropropane
Conditions | Yield |
---|---|
at 136 - 140℃; Product distribution; | |
at 136 - 140℃; Product distribution; |
propane
chlorine
A
1-Chloropropane
B
1,1-dichloropropane
C
1,1,1-trichloropropane
D
1,1,1,2-tetrachloropropane
Conditions | Yield |
---|---|
at 360 - 395℃; |
propane
chlorine
A
1-Chloropropane
B
1,1-dichloropropane
C
1,1,1-trichloropropane
D
1,1,1,2-tetrachloropropane
Conditions | Yield |
---|---|
at 230 - 347℃; |
propane
chlorine
A
1-Chloropropane
B
1,1-dichloropropane
C
1,1,1-trichloropropane
D
1,1,1,2-tetrachloropropane
Conditions | Yield |
---|---|
at 230 - 347℃; |
1-Chloropropane
chlorine
A
1,2-Dichloropropane
B
1,1-dichloropropane
C
1,3-Dichloropropane
Conditions | Yield |
---|---|
With diacetyl peroxide at 80℃; for 6h; Inert atmosphere; Autoclave; Green chemistry; | 98.1% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 150℃; for 0.333333h; microwave irradiation; | 95% |
1,1-dichloropropane
Conditions | Yield |
---|---|
With Mg In tetrahydrofuran; pentane to soln. of Mo(N(t-Bu)(3,5-C6H3Me2))3 in THF added CH3CH2CHCl2 under Ar;mixt. stirred for 1.5 h at room temp. in presence of magnesium; solvent removed in vac. and residue redissolved in pentane; ppt. removed by filtration and filtrate concd. in vac.; elem. anal.; | 91% |
With magnesium In tetrahydrofuran at 20℃; for 2.58333h; Inert atmosphere; | 54% |
With magnesium In tetrahydrofuran treatment of Mo(N(t-Bu)C6H3Me3)3 with excess 1,1-dichlopropane (2 equiv.) in the presence of Mg in THF at room temp.; |
(4S,5S)-Dimethyl 2-(2-chlorophenyl)-1,3-dioxolane-4,5-dicarboxylate
1,1-dichloropropane
2-O-(2-chlorobenzyl)-D-threitol
Conditions | Yield |
---|---|
With sodium hydroxide; aluminium trichloride In dichloro-1-propanol; water | 81% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 150℃; for 0.333333h; microwave irradiation; | 79% |
Conditions | Yield |
---|---|
With potassium phosphate In N,N-dimethyl-formamide at 130℃; for 4h; Sealed tube; | 23% |
tetrahydrocannabinolic acid
1,1-dichloropropane
Conditions | Yield |
---|---|
With potassium phosphate In N,N-dimethyl-formamide at 130℃; for 4h; Sealed tube; | 7% |
1,2-Dichloropropane
2,2-dichloropropane
1,1-dichloropropane
octachloropropane
Conditions | Yield |
---|---|
durch Einleiten von Chlor unter Belichtung und allmaehlicher Erhoehung der Reaktionstemperatur auf 200grad; |
Conditions | Yield |
---|---|
With alkali metalammonium; ammonia |
Conditions | Yield |
---|---|
With hydrogen fluoride; mercury(II) oxide | |
With pyridine; hydrogen fluoride; mercury(II) oxide |
Conditions | Yield |
---|---|
With hydrogen fluoride; mercury(II) oxide |
Conditions | Yield |
---|---|
With chlorine im Sonnenlichte; | |
With chlorine | |
With antimonypentachloride |
Conditions | Yield |
---|---|
at 100℃; alkoh.Kali; |
1,1-dichloropropane
1-bromo-2,2-dichloropropane
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 15℃; Irradiation; competition reaction with neopentane and tert-butyl chloride; relative rate constants for mediated brominations; additives - Br2, CH2CCl2, BrCCl3; |
1,1-dichloropropane
A
trans-1-Chloropropen
B
1,2-Dichloropropane
C
cis-1-chloropropene
D
3-chloroprop-1-ene
Conditions | Yield |
---|---|
With potassium chloride; sodium chloride; zinc(II) chloride at 400℃; for 0.5h; Product distribution; other gem-dichloroalkanes; var. molten salt catalysts; var. temps.; | A 8.8 % Chromat. B 12.8 % Chromat. C 19.4 % Chromat. D 3.0 % Chromat. |
Conditions | Yield |
---|---|
With n-butyllithium In hexane; pentane 1.) -40 - -30 deg C; 2.) -30 deg C to -10 deg C, 3 h; | 1.06 g |
Conditions | Yield |
---|---|
Geschwindigkeit; |
Conditions | Yield |
---|---|
Geschwindigkeit; |
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