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inquiryHigh quality and compeititive price Antifungal agent Itraconazole Assay above 98.5% Appearance:white powder Package:5-25kg/drum Application:Antifungal agent Port:GuangZhou
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inquiryItems Standard Result Description Awhite or almost white powder Awhite powder Identification:
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Itraconazole Basic information Product Name: Itraconazole Synonyms: SPORANOX;R51211;ORICONAZOLE;TRIASPORIN;-1-ylmethyl)-1,3-dioxolan-4-yl)methoxy)phenyl)-1-piperazinyl)phenyl)-2,4-dihyd;
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(-)-(R)-2,4dihydro-4-[4-[4-(4-hydroxyphenyl)-1-piperazinyl]phenyl]-2-(1-methylpropyl)-3H-1,2,4-triazol 3-one
itraconazole
Conditions | Yield |
---|---|
Stage #1: (-)-(R)-2,4dihydro-4-[4-[4-(4-hydroxyphenyl)-1-piperazinyl]phenyl]-2-(1-methylpropyl)-3H-1,2,4-triazol 3-one With hydrazine hydrate; sodium hydroxide In N,N-dimethyl-formamide at 40℃; for 0.666667h; Inert atmosphere; Stage #2: Toluene-4-sulfonic acid (2R,4R)-2-(2,4-dichloro-phenyl)-2-[1,2,4]triazol-1-ylmethyl-[1,3]dioxolan-4-ylmethyl ester In N,N-dimethyl-formamide at 60℃; for 1.5h; | 90.5% |
s-butyl bromide
cis-4-<4-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>phenyl>-2,4-dihydro-3H-1,2,4-triazol-3-one
itraconazole
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide for 14h; | 46% |
itraconazole
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: sulfuric acid / tert-butyl methyl ether / 3.5 h / 25 - 60 °C 2.1: iodine; sodium hydrogencarbonate / ethanol / -15 - -10 °C 3.1: dimethyl sulfoxide / 25 h / 20 - 100 °C 4.1: hydrogenchloride; palladium on activated charcoal; hydrogen / methanol; water / 18 h / 20 °C / 1500.15 Torr 5.1: triethylamine / dichloromethane / 24.33 h / 20 °C / Reflux 6.1: sodium hydroxide; hydrazine hydrate / N,N-dimethyl-formamide / 0.67 h / 40 °C / Inert atmosphere 6.2: 1.5 h / 60 °C View Scheme |
itraconazole
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: iodine; sodium hydrogencarbonate / ethanol / -15 - -10 °C 2.1: dimethyl sulfoxide / 25 h / 20 - 100 °C 3.1: hydrogenchloride; palladium on activated charcoal; hydrogen / methanol; water / 18 h / 20 °C / 1500.15 Torr 4.1: triethylamine / dichloromethane / 24.33 h / 20 °C / Reflux 5.1: sodium hydroxide; hydrazine hydrate / N,N-dimethyl-formamide / 0.67 h / 40 °C / Inert atmosphere 5.2: 1.5 h / 60 °C View Scheme |
itraconazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: dimethyl sulfoxide / 25 h / 20 - 100 °C 2.1: hydrogenchloride; palladium on activated charcoal; hydrogen / methanol; water / 18 h / 20 °C / 1500.15 Torr 3.1: triethylamine / dichloromethane / 24.33 h / 20 °C / Reflux 4.1: sodium hydroxide; hydrazine hydrate / N,N-dimethyl-formamide / 0.67 h / 40 °C / Inert atmosphere 4.2: 1.5 h / 60 °C View Scheme |
itraconazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogenchloride; palladium on activated charcoal; hydrogen / methanol; water / 18 h / 20 °C / 1500.15 Torr 2.1: triethylamine / dichloromethane / 24.33 h / 20 °C / Reflux 3.1: sodium hydroxide; hydrazine hydrate / N,N-dimethyl-formamide / 0.67 h / 40 °C / Inert atmosphere 3.2: 1.5 h / 60 °C View Scheme |
itraconazole
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: magnesium; iodine / tert-butyl methyl ether / 2 h / 0 - 56 °C / Inert atmosphere; Reflux 1.2: 5 h / -10 - 30 °C 2.1: sulfuric acid / tert-butyl methyl ether / 3.5 h / 25 - 60 °C 3.1: iodine; sodium hydrogencarbonate / ethanol / -15 - -10 °C 4.1: dimethyl sulfoxide / 25 h / 20 - 100 °C 5.1: hydrogenchloride; palladium on activated charcoal; hydrogen / methanol; water / 18 h / 20 °C / 1500.15 Torr 6.1: triethylamine / dichloromethane / 24.33 h / 20 °C / Reflux 7.1: sodium hydroxide; hydrazine hydrate / N,N-dimethyl-formamide / 0.67 h / 40 °C / Inert atmosphere 7.2: 1.5 h / 60 °C View Scheme |
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile for 4h; Inert atmosphere; Reflux; | 60% |
3,5-dimethyl-4-hydroxybenzyl bromide
itraconazole
Conditions | Yield |
---|---|
In chloroform; acetonitrile |
Conditions | Yield |
---|---|
In ethanol UV-irradiation; Microbiological reaction; |
Conditions | Yield |
---|---|
In acetonitrile UV-irradiation; |
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