CAS No.875-72-9,2-methylideneadamantane Suppliers

Simagchem Corporation

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High quality 2-Methylideneadamantane supplier in China

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As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

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Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

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2-MethylideneadamantaneAppearance:Colorless or Light yellow liquid Storage:Keep away of light,cool place Package:25kg/drum;200kg/drum Application:Fine Chemical Transportation:Sea/air/courier

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2-METHYLIDENEADAMANTANEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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2-Methylideneadamantane CAS NO.875-72-9

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Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

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Synthetic route

: 2-Benzenesulfonylmethylene-adamantane

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With ethanol; magnesium; mercury dichloride for 2h; Ambient temperature;	99%
With ethanol; magnesium; mercury dichloride for 2h; Ambient temperature; other substrates;	99%

: 702-98-7
2-methyladamantan-2-ol

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With potassium hydrogensulfate at 100℃; under 150 - 200 Torr;	96%
With phosphoric acid	85%
With toluene-4-sulfonic acid In toluene for 1h; Heating;	65%

: 700-58-3
2-Adamantanone

: 61078-14-6
1-methyl-2-(methylsulfonyl)-1H-benzo[d]imidazole

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 1h; Reagent/catalyst; Temperature; Time; Inert atmosphere;	96%
With sodium hexamethyldisilazane In N,N-dimethyl-formamide at -55 - 20℃; Reagent/catalyst; Temperature; Inert atmosphere;	95%

: 700-58-3
2-Adamantanone

: 917-54-4
methyllithium

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With thionyl chloride Product distribution; other alkyllithiums, other hindered ketones;	94%
With thionyl chloride 1.) Et2O, -78 deg C, 30 min, 2.) a) -78 deg C, 5 min, b) RT, 30 min; Yield given. Multistep reaction;

: 58540-98-0
2-Trimethylsilanylmethyl-adamantan-2-ol

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
Nafion-H In dichloromethane for 1h; Ambient temperature;	88%
(i) nBuLi, THF, hexane, (ii) MeSO2Cl; Multistep reaction;

: 700-58-3
2-Adamantanone

: 75-09-2
dichloromethane

A: 875-72-9
2-methylideneadamantane

B: 700-57-2
1-adamantanol

Conditions

Conditions	Yield
With titanium tetrachloride; magnesium In tetrahydrofuran at 0 - 20℃; for 0.833333h;	A 86% B 6%

...Expand

: 74381-15-0
4(e)-Chloro-2-methyleneadamantane

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In cyclohexane for 20h; Heating;	79.1%

: 27852-61-5
2-bromo-2-methyladamantane

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With 2,4,6-triphenylverdazyl In acetonitrile for 48h; Ambient temperature;	73%
In sulfolane at 30℃; Rate constant; Kinetics; Thermodynamic data; other temperatures; ΔH(excit.), ΔS(excit.); other aprotic solvents;
With 1,3,5-triphenylverdazyl In cyclohexanone at 25℃; Thermodynamic data; Kinetics; Further Variations:; Solvents;

: 31934-34-6
2',5'-dihydrospiro

A: 875-72-9
2-methylideneadamantane

B: 56169-89-2
spiro

C: 97462-11-8
homoadamantane-2-thione

Conditions

Conditions	Yield
In xylene at 80℃; for 30h;	A 3% B 70% C 16%
In xylene	A 3 % Spectr. B 63 % Spectr. C 14 % Spectr.
In xylene at 80℃; for 30h; Product distribution; Rate constant; thermolysis in xylene, in benzyl alcohol or piperidine; kinetic of thermolysis in xylene; regiochemistry of cycloaddition of diazomethane to adamantanethione; kinetic of thermolysis of 2',5'-dihydrospiro;	A 3 % Spectr. B 64 % Spectr. C 14 % Spectr.

...Expand

: 31934-34-6
C11H16N2S

A: 875-72-9
2-methylideneadamantane

B: 97462-11-8
homoadamantane-2-thione

C: 56169-89-2
C11H16S

Conditions

Conditions	Yield
In xylene at 80℃; for 30h;	A 3% B 16% C 70%

...Expand

: 700-58-3
2-Adamantanone

: 74-95-3
1,2-dibromomethane

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With titanium tetrachloride; zinc In tetrahydrofuran; dichloromethane at -40℃;	66%
With titanium tetrachloride; zinc In tetrahydrofuran; dichloromethane Ambient temperature;

: 700-58-3
2-Adamantanone

: 2065-66-9
methyl-triphenylphosphonium iodide

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
Stage #1: methyl-triphenylphosphonium iodide With n-butyllithium In tetrahydrofuran at 20℃; for 0.25h; Stage #2: 2-Adamantanone In tetrahydrofuran at 20℃; for 2h; Inert atmosphere;	66%
Stage #1: methyl-triphenylphosphonium iodide With n-butyllithium In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: 2-Adamantanone In tetrahydrofuran at 20℃; for 2h; Inert atmosphere;	66%

: 873869-19-3
1-(tert-butyl)-5-(methylsulfonyl)-1H-tetrazole

: 700-58-3
2-Adamantanone

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
With caesium carbonate In tetrahydrofuran; N,N-dimethyl-formamide at 70℃; for 16h;	57%

: 700-58-3
2-Adamantanone

: 19493-09-5
Methylenetriphenylphosphorane

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
In dimethyl sulfoxide at 56℃; for 2h;	55%

: 700-58-3
2-Adamantanone

: 1779-49-3
Methyltriphenylphosphonium bromide

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; Stage #2: 2-Adamantanone In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere;	50%
With phenyllithium 1.) ether, 30 min, 2.) 2 h; Yield given. Multistep reaction;
With n-butyllithium In diethyl ether; hexane 1.) 30 min, 2.) room temperature, 30 min; reflux 17 h;	80 % Spectr.

: 68251-94-5
ω-(Bromomethylene)adamantane

A: 875-72-9
2-methylideneadamantane

B: 94052-77-4
1,2-diadamantylideneethane

Conditions

Conditions	Yield
With lithium; copper(I) bromide In diethyl ether for 3h; Heating;	A n/a B 21%

: 700-58-3
2-Adamantanone

: 74-88-4
methyl iodide

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
(i) Ph3P, (ii) nBuLi, (iii) /BRN= 1210235/; Multistep reaction;

: 67-56-1
methanol

: 27852-61-5
2-bromo-2-methyladamantane

A: 875-72-9
2-methylideneadamantane

B: 51086-30-7
2-methyl-2-methoxyadamantane

Conditions

Conditions	Yield
at 25℃; Rate constant; Mechanism; other proton-donating and aprotic solvents;

...Expand

: 700-58-3
2-Adamantanone

: 1779-49-3
Methyltriphenylphosphonium bromide

A: 875-72-9
2-methylideneadamantane

B: 700-57-2
1-adamantanol

Conditions

Conditions	Yield
With n-butyllithium In hexane; toluene Product distribution; Mechanism; 1.) 30 min, 2.) room temperature, 30 min; reflux, 17 h; other solvents, other reagents, time; other ketones;

...Expand

: 700-58-3
2-Adamantanone

: 875-72-9
2-methylideneadamantane

Conditions

Conditions	Yield
Wittig reaction conditions;
Multi-step reaction with 2 steps 1: diethyl ether / 18 h / Ambient temperature 2: 65 percent / p-toluenesulfonic acid / toluene / 1 h / Heating View Scheme
Multi-step reaction with 2 steps 1: diethyl ether; pentane / 0.17 h / 0 °C 2: 88 percent / Nafion-H / CH2Cl2 / 1 h / Ambient temperature View Scheme

: 75-85-4
tert-Amyl alcohol

: 27852-61-5
2-bromo-2-methyladamantane

A: 875-72-9
2-methylideneadamantane

B: 2-(1,1-Dimethyl-propoxy)-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 64-17-5
ethanol

: 27852-61-5
2-bromo-2-methyladamantane

A: 875-72-9
2-methylideneadamantane

B: 2-methyl-2-adamantanyl ethyl ether

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 702-98-7
2-methyladamantan-2-ol

A: 700-58-3
2-Adamantanone

B: 24557-02-6
2-methyl-1-adamantanol

C: 875-72-9
2-methylideneadamantane

D: 21365-85-5
E,Z-4-methyl-1-adamantanol

Conditions

Conditions	Yield
With potassium hydroxide; nitric acid; trifluoroacetic acid 1) 65 deg C, 3.5 h, 2) 95 deg C, 2.5 h; Yield given. Multistep reaction. Yields of byproduct given;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 2154-65-6
1,3,5-triphenylverdazyl

A: 875-72-9
2-methylideneadamantane

B: 51940-11-5
2,4,6-triphenylverdazylium bromide

C: 22459-57-0
2,4,6-triphenylverdazyl

Conditions

Conditions	Yield
In acetonitrile at 25℃; Kinetics; Thermodynamic data; oth. solvents, effect of addition of var. salts, oth. temperature, ΔH(activ.), ΔS(activ.);

...Expand

: 38424-20-3
2-tert-butyl-2-adamantanol

A: 875-72-9
2-methylideneadamantane

B: 13376-19-7
2-isobutylidene-adamantane

C: 83782-92-7
1-(2-adamantyl)-2-methylprop-1-ene

Conditions

Conditions	Yield
With hydrogenchloride In chloroform at 200℃; Heating; Further byproducts given;	A 10 % Chromat. B n/a C n/a
With hydrogenchloride In chloroform at 150℃; for 48h; Product distribution; other reagent (HBr), reaction time, temperature;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 67-63-0
isopropyl alcohol

A: 875-72-9
2-methylideneadamantane

B: 2-Isopropoxy-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 78-92-2, 15892-23-6
iso-butanol

A: 875-72-9
2-methylideneadamantane

B: 2-sec-Butoxy-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 100-51-6
benzyl alcohol

A: 875-72-9
2-methylideneadamantane

B: 2-Benzyloxy-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 75-65-0
tert-butyl alcohol

A: 875-72-9
2-methylideneadamantane

B: 2-tert-Butoxy-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 27852-61-5
2-bromo-2-methyladamantane

: 108-93-0
cyclohexanol

A: 875-72-9
2-methylideneadamantane

B: 2-Cyclohexyloxy-2-methyl-adamantane

Conditions

Conditions	Yield
at 25℃; Rate constant;

...Expand

: 875-72-9
2-methylideneadamantane

: 31482-53-8
2-(Bromomethyl)-2-bromoadamantane

Conditions

Conditions	Yield
With bromine In dichloromethane Ambient temperature;	99%
With bromine In tetrachloromethane Ambient temperature; overnight;	82%
With bromine In tetrachloromethane
With bromine In tetrachloromethane at -15℃; Yield given;
With pyridine; bromine In pentane 1.) 1 h, 0 deg C; 2.) 2 h room temperature;	18.2 g

: 381-98-6
trifluoromethyacrylic acid

: 875-72-9
2-methylideneadamantane

: 188739-86-8
2-trifluoromethyl-acrylic acid 2-methyl-adamantan-2-yl ester

Conditions

Conditions	Yield
With sodium hydroxide; sulfuric acid In toluene	93%

: 875-72-9
2-methylideneadamantane

: bis(adamant-2-ylmethyl)phosphinic acid

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; sodium hypophosphite In methanol; water at 120℃; for 10h; Sealed tube;	92%

: 875-72-9
2-methylideneadamantane

: 79-10-7
acrylic acid

: 249562-06-9
acrylic acid-2-methyl-2-adamantyl

Conditions

Conditions	Yield
With sodium hydroxide; sulfuric acid In toluene	91.5%
boron trifluoride diethyl etherate at 0℃; for 1h; Product distribution / selectivity;

: 79-41-4
poly(methacrylic acid)

: 875-72-9
2-methylideneadamantane

: 177080-67-0
2-methyl-2-adamantyl methacrylate

Conditions

Conditions	Yield
With sodium hydroxide; p-toluenesulfonic acid monohydrate In toluene	90.8%
boron trifluoride diethyl etherate at 0℃; for 1h; Product distribution / selectivity;
boron trifluoride diethyl etherate In n-Undecane; toluene at 0℃; for 2h; Product distribution / selectivity;
boron trifluoride diethyl etherate In n-Undecane at 0℃; for 2h; Product distribution / selectivity;

: 875-72-9
2-methylideneadamantane

: 461677-71-4
1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one

: C26H27NO

Conditions

Conditions	Yield
dirhodium tetraacetate In dichloromethane at 20℃; for 0.166667h;	89%

: 875-72-9
2-methylideneadamantane

: 87801-60-3
7-endo-carbomethoxybicyclo<3.3.1>nonan-3-one

Conditions

Conditions	Yield
Stage #1: 2-methylideneadamantane With ferrous(II) sulfate heptahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ozone In methanol; water at -78 - 20℃; for 0.0833333h; Stage #2: With magnesium bis(monoperoxyphthalate)hexahydrate In methanol; water at 0℃; for 2h;	87%

: 3265-14-3
3-diazo-1-methyl-1,3-dihydro-indol-2-one

: 875-72-9
2-methylideneadamantane

: C20H23NO

Conditions

Conditions	Yield
dirhodium tetraacetate In dichloromethane at 20℃; for 0.25h;	85%

: 875-72-9
2-methylideneadamantane

: 76-02-8
Trichloroacetyl chloride

: 123489-40-7
2’,2’-dichlorospiro[adamantane-2,3’-cyclobutane]-1‘-one

Conditions

Conditions	Yield
With triethylamine In hexane for 5h; Heating; also in ether with POCl3 and Zn as reagents;	84%
With zinc In diethyl ether at 20 - 35℃; for 4h; Sonication;
With zinc In diethyl ether at 20 - 35℃; for 2h; Sonication;

: 875-72-9
2-methylideneadamantane

: 762-04-9
phosphonic acid diethyl ester

: 1454661-32-5
diethyl (2-fluoroadamantan-2-yl)methylphosphonate

Conditions

Conditions	Yield
With silver nitrate; acetic acid; Selectfluor In dichloromethane; water at 40℃; for 18h; Schlenk technique; Inert atmosphere;	81%

: 67-56-1
methanol

: 875-72-9
2-methylideneadamantane

: 19489-19-1
3β-Methoxycarbonyl-1α(H),5α(H)-bicyclo[3.3.1]nonan

Conditions

Conditions	Yield
Stage #1: methanol; 2-methylideneadamantane With ozone Stage #2: With ferrous(II) sulfate heptahydrate; thiophenol at -78 - 20℃; for 0.5h;	81%

: 960121-23-7
1,1-bis[(triethylsilyl)dioxy]cyclohexane

: 875-72-9
2-methylideneadamantane

: C17H26O2

Conditions

Conditions	Yield
With tin(IV) chloride In dichloromethane at -78 - -30℃;	74%

: 875-72-9
2-methylideneadamantane

: 461677-72-5
1-allyl-3-diazo-1,3-dihydro-2H-indol-2-one

: C22H25NO

Conditions

Conditions	Yield
dirhodium tetraacetate In dichloromethane at 20℃; for 0.2h;	72%

: 875-72-9
2-methylideneadamantane

: 1427281-56-8
4-[4-methoxy-4-(triethylsilylperoxy)cyclohexyl]phenyl acetate

: cis-adamantane-2-spiro-3′-8′-(4′-acetoxyphenyl)-1′,2′-dioxaspiro[4.5]-decane

Conditions

Conditions	Yield
With tin(IV) chloride In dichloromethane at -78 - -30℃;	70%

: 875-72-9
2-methylideneadamantane

: (PMePh2)2W(O)Cl2(CHCMe2Ph)

: sodium 1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-olate

: C31H27F18O3PW

Conditions

Conditions	Yield
Stage #1: (PMePh2)2W(O)Cl2(CHCMe2Ph); sodium 1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-olate In toluene at 20℃; for 0.5h; Inert atmosphere; Stage #2: 2-methylideneadamantane In toluene at 80℃; for 1h; Inert atmosphere; Sealed tube;	70%

...Expand

: 875-72-9
2-methylideneadamantane

: 504-02-9
1,3-cylohexanedione

: C17H22O2

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In methanol at 0℃;	69%

: 960121-27-1
4-phenyl-1,1-bis[(triethylsilyl)dioxy]cyclohexane

: 875-72-9
2-methylideneadamantane

: C23H30O2

Conditions

Conditions	Yield
With tin(IV) chloride In dichloromethane at -78 - -30℃;	68%

: 875-72-9
2-methylideneadamantane

: 126-81-8
dimedone

: C19H26O2

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In methanol at 0℃;	67%

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Olean-12-en-28-oicacid, 3-hydroxy-, 2-bromoethyl ester, (3b)- (9CI)

87576-10-1

Acetamide,2-(4-chlorophenoxy)-N-[2-(hexahydro-1H-azepin-1-yl)ethyl]-, hydrochloride (1:1)

87576-94-1

Methane,azido(trimethylsilyl)-

875781-15-0

3-Pyridinecarboxaldehyde,5-bromo-2-fluoro-

875781-17-2

1H-Pyrazolo[3,4-b]pyridine,5-bromo-

875781-18-3

1H-Pyrazolo[3,4-b]pyridine,5-bromo-3-iodo-

875781-43-4

5-Bromo-4,7-diazaindole

875781-44-5

5H-Pyrrolo[2,3-b]pyrazine,2-bromo-7-iodo-

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