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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Tris(dimethylaminomethyl)phenol Manufacturer/High quality/Best price/In stock

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Biet Co., Ltd

Our advantage: 1. 24hours to reply your E-mail; 2. Customized pakage; 3. Adequate stocks; 4. The competitive price owing to low labor cost and low material cost; 5.Market information trend share with customers; 6. Suggestion for purchase decisi

Curing Agent DMP-30 CAS 90-72-2

Cas:90-72-2

Min.Order:1 Metric Ton

FOB Price: $2900.0

Type:Trading Company

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Aecochem Corp.

Xiamen Aeco Chemical Industrial Co., Ltd(same as Aecochem Corp.) Your Partner in China, a Professional chemical raw material supplier, our main products including the Epxoy Chemical ,Petro Chemical,Pharma Intermediate,Fine Chemicas and Life S

Supply high quality Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:200 Kilogram

Negotiable

Type:Manufacturers

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Luyunjia Chemistry Xiamen Limited

Specifications CAS No.: 90-72-2 Other Names: Tris(dimethylaminomethyl)phenol MF: C15H27N3O EINECS No.: 202-013-9 Place of Origin: Shanghai, China (Mainland) Grade Standard: Agriculture Grade, Electron Grade, Food Grade, Industrial Grade,

90-72-2 2,4,6-tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Tri-(dimethylaminomethy1)phenol DMP-30 supplier in China

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hefei TNJ chemical industry co.,ltd

Epoxy Resin LE-828 (to Russia market) 1.Bisphenol A Epoxy Resin 2.Bisphenol F Epoxy Resin 3.Epoxy Novolac Resin Appearance:transparent liquid Storage:Warehouse ventilation, away from open flame, high temperature, and antioxidant Package:180kg

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:3 Metric Ton

Negotiable

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dr

2,4,6-Tris(diMethylaMinoMethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2,4,6-tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service DMP-30 2,4,6-Tris(dimethylaminomethyl)phenol IN Stock Tris(dimethylaminomethyl)phenol CAS 90-72-2 90-72-2 CAS 90-72-2

DMP-30 2,4,6-Tris(dimethylaminomethyl)phenol IN Stock Tris(dimethylaminomethyl)phenol CAS 90-72-2

Cas:90-72-2

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Tris(dimethylaminomethyl)phenol Basic information Product Name: Tris(dimethylaminomethyl)phenol Synonyms: TRIS(DIMETHYLAMINOMETHYL)PHENOL;,’,’’-Tri(dimethylamino)mesito

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 90-72-2 with best quality

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Chemical Name 2,4,6-Tris(dimethylaminomethyl)phenol CAS No. 90-72-2 Molecular Formula C15H27N3O Molecular Weight 265.39400 PSA 29.95000

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Tris(dimethylaminomethyl)phenol 90-72-2

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Tris(dimethylaminomethyl)phenol CAS: 90-72-2 MF: C15H27N3O MW: 265.39 EINECS: 202-013-9 Tris(dimethylaminomethyl)phenol Structure Tris(dimethylaminomethyl)phenol Chemical Properties Melting point 316℃ Boiling point

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Tris(dimethylaminomethyl)phenol CAS:90-72-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga

Tris(dimethylaminomethyl)phenol CAS:90-72-2

Cas:90-72-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

Tris(dimethylaminomethyl)phenol CAS NO.90-72-2

Cas:90-72-2

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

Tris(dimethylaminomethyl)ph CAS 90-72-2enol

Cas:90-72-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Company information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big cust

Tris(dimethylaminomethyl)phenol CAS:90-72-2

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $7.0 / 10.0

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

Hangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting 2 4 6-Tris(dimethylaminomethyl)phenol ( DMP-30),CAS: 90-72-2 Please contact us by email freely. We are leading exporter in China. If you reall

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Tris (dimethylaminomethyl) phenol

Cas:90-72-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

tris(dimethylaminomethyl)phenol Synonyms:2,4,6-tris(dimethylaminomethyl)phenol; DMP-30

Cas:90-72-2

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Triumph International Development Limilted

Appearance:Pale yellow liquid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Air/

2,4,6-tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

TRIS-(DIMETHYLAMINOMETHYL) PHENOL (JD DMP-30)

Cas:90-72-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

TRIS(DIMETHYLAMINOMETHYL)PHENOL

Cas:90-72-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd

Tris(dimethylaminomethyl)phenol

Cas:90-72-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

triethylsiloxymethyl-N,N-dimethylamine
1353053-97-0

triethylsiloxymethyl-N,N-dimethylamine

2,6-bis-<(dimethyamino)methyl>phenol
15827-34-6

2,6-bis-<(dimethyamino)methyl>phenol

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Conditions
ConditionsYield
Sealed tube; Heating;90%
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

phenol
108-95-2

phenol

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Conditions
ConditionsYield
In water for 2.5h;80%
In water at 25 - 100℃; for 3h; Mannich reaction;80%
With water
Stage #1: formaldehyd; dimethyl amine In water at 60℃; under 3000.3 Torr; for 5h; Large scale;
Stage #2: phenol In water at 90℃; for 3.5h; Temperature; Large scale;
3-chloro-2,4,6-tris-dimethylaminomethyl-phenol; trihydrochloride
131253-33-3

3-chloro-2,4,6-tris-dimethylaminomethyl-phenol; trihydrochloride

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Conditions
ConditionsYield
With water; platinum Hydrogenation;
formaldehyd
50-00-0

formaldehyd

dimethyl amine
124-40-3

dimethyl amine

4-hydroxy-benzoic acid
99-96-7

4-hydroxy-benzoic acid

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Conditions
ConditionsYield
With water
formaldehyd
50-00-0

formaldehyd

water
7732-18-5

water

dimethyl amine
124-40-3

dimethyl amine

phenol
108-95-2

phenol

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Conditions
ConditionsYield
at 90 - 95℃;
bis(diethylamino)dihydrosilane
27804-64-4

bis(diethylamino)dihydrosilane

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dihydrosilane

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dihydrosilane

Conditions
ConditionsYield
In chloroform at 20℃; for 0.25h;96%
lead(II) bis(trimethylsilyl)amide
55147-59-6, 65455-92-7

lead(II) bis(trimethylsilyl)amide

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris(dimethylaminomethyl)phenoxy]-plumbylene

bis[2,4,6-tris(dimethylaminomethyl)phenoxy]-plumbylene

Conditions
ConditionsYield
In pentane N2 or Ar-atmosphere; stirring (room temp., 2 h); evapn. (reduced pressure), recrystn. (pentane, -30°C); elem. anal.;96%
In benzene byproducts: HN(SiMe3)2; 2 equiv. ligand;
bis[bis(trimethylsilyl)amino]germanium(II)
59863-12-6

bis[bis(trimethylsilyl)amino]germanium(II)

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]germanium(II)

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]germanium(II)

Conditions
ConditionsYield
In pentane N2 or Ar-atmosphere; stirring (room temp., 2 h); evapn. (vac.), extg. (pentane), pptn. (-30°C, 48 h), filtering, drying (vac.); elem. anal.;96%
In benzene byproducts: HN(SiMe3)2; 2 equiv. ligand;
In benzene byproducts: (Me3Si)2NH; N2 or Ar-atmosphere, 20°C;
bis(bis(trimethylsilyl)amido)tin(II)
55147-78-9

bis(bis(trimethylsilyl)amido)tin(II)

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris(dimethylaminomethyl)phenoxy]-stannylene
524960-14-3

bis[2,4,6-tris(dimethylaminomethyl)phenoxy]-stannylene

Conditions
ConditionsYield
In pentane N2 or Ar-atmosphere; stirring (room temp., 2 h); concg. (vac.), filtering, drying (vac.); elem. anal.;96%
In benzene byproducts: HN(SiMe3)2; 2 equiv. ligand;
In benzene byproducts: (Me3Si)2NH; N2 or Ar-atmosphere, 20°C;
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis(dimethylamino)bis(trimethylsilyl)silane

bis(dimethylamino)bis(trimethylsilyl)silane

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]bis(trimethylsilyl)silane
394739-08-3

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]bis(trimethylsilyl)silane

Conditions
ConditionsYield
In toluene for 2h; Heating;95%
N,N-Dimethyltrimethylsilylamine
2083-91-2

N,N-Dimethyltrimethylsilylamine

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[2,4,6-tris((dimethylamino)methyl)phenoxy]trimethylsilane
161787-77-5

[2,4,6-tris((dimethylamino)methyl)phenoxy]trimethylsilane

Conditions
ConditionsYield
In pentane94%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[2,4,6-tris(((dimethylamino)methyl)phenoxy)phenyl]silane

[2,4,6-tris(((dimethylamino)methyl)phenoxy)phenyl]silane

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

Conditions
ConditionsYield
In pentane at 20℃; for 3h;94%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

C51H83N9O3Si

C51H83N9O3Si

Conditions
ConditionsYield
In pentane at 20℃;94%
tri(dimethylamino)silane
15112-89-7

tri(dimethylamino)silane

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

tris[2,4,6-tris((dimethylamino)methyl)phenoxy]hydrosilane

tris[2,4,6-tris((dimethylamino)methyl)phenoxy]hydrosilane

Conditions
ConditionsYield
With ammonium sulfate at 110℃; for 48h;92%
bis(diethylamino)dimethylsilane
4669-59-4

bis(diethylamino)dimethylsilane

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dimethylsilane
394739-06-1

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dimethylsilane

Conditions
ConditionsYield
In pentane for 2h; Heating;91%
bis(bis(trimethylsilyl)amido)tin(II)
55147-78-9

bis(bis(trimethylsilyl)amido)tin(II)

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]tin(II)
211423-73-3, 175855-63-7

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]tin(II)

Conditions
ConditionsYield
In pentane inert atmosphere; dropwise addn. of ligand to equimolar amt. of Sn-compd., stirring (room temp., 2 h); solvent removal (vac.), dissoln. in pentane, crystn. (-30°C); elem. anal.;91%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

lithium 2,4,6-tris((dimethylamino)methyl)phenoxide

lithium 2,4,6-tris((dimethylamino)methyl)phenoxide

Conditions
ConditionsYield
With n-butyllithium In diethyl ether at 20℃; for 2h;90%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dihydrosilane

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dihydrosilane

tris[2,4,6-tris((dimethylamino)methyl)phenoxy]hydrosilane

tris[2,4,6-tris((dimethylamino)methyl)phenoxy]hydrosilane

Conditions
ConditionsYield
In chloroform at 20℃; for 24h;90%
bis[bis(trimethylsilyl)amino]germanium(II)
59863-12-6

bis[bis(trimethylsilyl)amino]germanium(II)

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]germanium(II)
211423-72-2

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]germanium(II)

Conditions
ConditionsYield
In pentane inert atmosphere; dropwise addn. of ligand to equimolar amt. of Ge-compd., stirring (room temp., 2 h); solvent removal (vac.), dissoln. in pentane, crystn. (-30°C);89%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

(dimethylamino)tris(trimethylsilyl)silane

(dimethylamino)tris(trimethylsilyl)silane

[2,4,6-tris((dimethylamino)methyl)phenoxy]tris(trimethylsilyl)silane

[2,4,6-tris((dimethylamino)methyl)phenoxy]tris(trimethylsilyl)silane

Conditions
ConditionsYield
In pentane for 2h; Heating;83%
lead(II) bis(trimethylsilyl)amide
55147-59-6, 65455-92-7

lead(II) bis(trimethylsilyl)amide

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]lead(II)
211423-74-4

[bis(trimethylsilyl)amino][2,4,6-tris(dimethylaminomethyl)phenoxy]lead(II)

Conditions
ConditionsYield
In pentane inert atmosphere; dropwise addn. of ligand to Pb-compd., stirring (room temp., 2 h); solvent removal (vac.), dissoln. in pentane, crystn. (-30°C); elem. anal.;82%
germanium(II) chloride dioxane

germanium(II) chloride dioxane

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

tris(dimesitylgermylenecarbodiimide)
202127-98-8

tris(dimesitylgermylenecarbodiimide)

Conditions
ConditionsYield
In tetrahydrofuran byproducts: LiCl; N2-atmosphere; stirring (room temp.); C6H6 addn., filtering, evapn.;78%
triphenylphosphine
603-35-0

triphenylphosphine

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

silver(l) oxide
20667-12-3

silver(l) oxide

[2,4,6-tris(dimethylaminomethyl)phenolato]bis(triphenylphosphine)silver(I)
616880-27-4

[2,4,6-tris(dimethylaminomethyl)phenolato]bis(triphenylphosphine)silver(I)

Conditions
ConditionsYield
In toluene Ag2O, PPh3, and 2,4,6-tris(dimethylaminomethyl)phenol in toluene were stirred overnight at room temp.; react. mixt. was filtered, filtrate was left to stand at room temp., ppt. was filtered, washed with toluene and dried in vacuo; elem. anal.;66%
3-nitrobenzene-1,2-dicarbonitrile
51762-67-5

3-nitrobenzene-1,2-dicarbonitrile

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

3-[2,4,6-tris-(N,N-dimethylaminomethyl)phenoxy]phthalonitrile

3-[2,4,6-tris-(N,N-dimethylaminomethyl)phenoxy]phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 0 - 60℃; Inert atmosphere;64%
With potassium carbonate In dimethyl sulfoxide at 20 - 60℃; Inert atmosphere;64%
With potassium carbonate In N,N-dimethyl-formamide at 45℃; for 24h; Inert atmosphere;
With potassium carbonate In N,N-dimethyl-formamide at 45℃; for 24h; Inert atmosphere;
trimethylaluminum
75-24-1

trimethylaluminum

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[Me2AlOC6H2(CH2NMe2)3-2,4,6](AlMe3)2

[Me2AlOC6H2(CH2NMe2)3-2,4,6](AlMe3)2

Conditions
ConditionsYield
In toluene byproducts: CH4; all manipulations under dry O2-free N2 atm.; soln. of org. compd. added dropwise to cooled (-10°C) soln. of Me3Al with vigorous stirring,react. mixt. stirred for 12 h at room temp.; solvent removed in vac., residue recrystd. from hexane/toluene (1/3); elem. anal.;62%
phenylsilanyl trifluoromethanesulfonate
127808-36-0

phenylsilanyl trifluoromethanesulfonate

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

A

[2,4,6-tris(((dimethylamino)methyl)phenoxy)phenyl]silane

[2,4,6-tris(((dimethylamino)methyl)phenoxy)phenyl]silane

B

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

bis[(2,4,6-tris((dimethylamino)methyl)phenoxy)phenyl]silane

Conditions
ConditionsYield
With triethylamine In toluene at 20℃; for 3h;A 60%
B n/a
cadmium bis(trimethylsilyl)amide

cadmium bis(trimethylsilyl)amide

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

[Cd(μ-2,4,6-tris(dimethylamino-methylphenolate)(bis(trimethylsilyl)amide)]2
847906-04-1

[Cd(μ-2,4,6-tris(dimethylamino-methylphenolate)(bis(trimethylsilyl)amide)]2

Conditions
ConditionsYield
In toluene under inert atm. alcohol was slowly added to Cd complex in toluene, stirred for 12 h, pyridine was added, mixt. was warmed until clear; elem. anal.;59.4%
tris(bis(trimethylsilyl)amido)praseodymium(III)

tris(bis(trimethylsilyl)amido)praseodymium(III)

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

A

Pr(3+)*3((CH3)2NCH2)3C6H2O(1-)=[Pr(((CH3)2NCH2)3C6H2O)3]

Pr(3+)*3((CH3)2NCH2)3C6H2O(1-)=[Pr(((CH3)2NCH2)3C6H2O)3]

Pr(((CH3)2NCH2)3C6H2O)3(H2O)2

Pr(((CH3)2NCH2)3C6H2O)3(H2O)2

Conditions
ConditionsYield
In hexane 25°C; filtn., crystn. of second product after solvent redn.; elem. anal.;A 59%
B 23%
trimethylaluminum
75-24-1

trimethylaluminum

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

Me2AlOC6H2(CH2NMe2)3-2,4,6

Me2AlOC6H2(CH2NMe2)3-2,4,6

Conditions
ConditionsYield
In toluene byproducts: CH4; all manipulations under dry O2-free N2 atm.; soln. of org. compd. added dropwise to cooled (-10°C) soln. of Me3Al with vigorous stirring,react. mixt. stirred for 12 h at room temp.; solvent removed in vac., residue washed with hexane, sublimed in vac.; elem. anal.;55%
4-Nitrophthalonitrile
31643-49-9

4-Nitrophthalonitrile

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

4-(2,4,6-tris((dimethylamino)methyl)phenoxy)phthalonitrile

4-(2,4,6-tris((dimethylamino)methyl)phenoxy)phthalonitrile

Conditions
ConditionsYield
Stage #1: 2,4,6-tris(dimethylaminomethyl)phenol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1h;
Stage #2: 4-Nitrophthalonitrile In N,N-dimethyl-formamide at 20℃; for 10.25h;
50.8%
With potassium carbonate In N,N-dimethyl-formamide
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

phthalocyanine silicon(IV) dichloride
19333-10-9

phthalocyanine silicon(IV) dichloride

bis(2,4,6-tris(N,N-dimethylaminomethyl)phenoxy)[phtalocyaninato]silicon
1415224-02-0

bis(2,4,6-tris(N,N-dimethylaminomethyl)phenoxy)[phtalocyaninato]silicon

Conditions
ConditionsYield
With sodium hydride In toluene for 6h; Inert atmosphere; Reflux;35.6%
phenylsilane
694-53-1

phenylsilane

2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

C51H83N9O3Si

C51H83N9O3Si

Conditions
ConditionsYield
31%
2,4,6-tris(dimethylaminomethyl)phenol
90-72-2

2,4,6-tris(dimethylaminomethyl)phenol

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dichlorosilane

bis[2,4,6-tris((dimethylamino)methyl)phenoxy]dichlorosilane

Conditions
ConditionsYield
With bis(N,N-dimethylamino)dichlorosilane In toluene at 110℃; for 6h; slow distillation;23%
Multi-step reaction with 2 steps
1: 91 percent / pentane / 2 h / Heating
2: 80 percent / SiCl4 / 80 °C
View Scheme
Multi-step reaction with 3 steps
1: 90 percent / nBuLi / diethyl ether / 2 h / 20 °C
2: 28 percent / diethyl ether / 48 h / 20 °C
3: 80 percent / SiCl4 / 80 °C
View Scheme
Multi-step reaction with 2 steps
1: 90 percent / nBuLi / diethyl ether / 2 h / 20 °C
2: 23 percent / SiCl4 / diethyl ether / 48 h / 20 °C
View Scheme

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