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inquiryN,N,2-trimethylquinolin-6-amine CAS:92-99-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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inquiryHigh quality 92-99-9 low price N,N,2-trimethylquinolin-6-amine immediately delivery Molecular Formula C12H14N2 Molar Mass 186.25 Density 1.0859 (rough estimate) Melting Point 101°C Bo
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inquiry4-amino-N,N-dimethylaniline
ethyl vinyl ether
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
With iodine In benzene at 80℃; for 2h; Green chemistry; | 83% |
trans-Crotonaldehyde
4-amino-N,N-dimethylaniline
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; for 1h; | 70% |
With hydrogenchloride In water; toluene Inert atmosphere; Reflux; | 62% |
In toluene at 20℃; | |
In toluene at 20℃; |
4-amino-N,N-dimethylaniline
crotonaldehyde
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
With hydrogenchloride In water | 70% |
With hydrogenchloride In water; toluene at 20℃; | 70% |
With hydrogenchloride In toluene Reflux; | 65% |
2-hydroxy-3-butene
4-amino-N,N-dimethylaniline
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
Stage #1: 4-amino-N,N-dimethylaniline With acetic anhydride In tetrahydrofuran Inert atmosphere; Stage #2: 2-hydroxy-3-butene With silver hexafluoroantimonate; [RhCl2(p-cymene)]2; copper(II) acetate monohydrate In tetrahydrofuran at 120℃; Inert atmosphere; Sealed tube; | 65% |
2-methylquinolin-6-amine
methyl iodide
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
Stage #1: 2-methylquinolin-6-amine With sodium hydride In N,N-dimethyl-formamide at 40℃; for 3h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 40℃; | 39% |
C15H19N3O2
A
6-(N,N-dimethylamino)-2-methylquinoline
B
7-Dimethylamino-2-methyl-benzo[d][1,3]diazepine-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In benzene Irradiation; | A 32% B 26% |
4-amino-N,N-dimethylaniline
paracetaldehyde
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
With hydrogenchloride |
2,4,6-Trimethyl-benzenesulfonate1-amino-6-dimethylamino-2-methyl-quinolinium;
6-(N,N-dimethylamino)-2-methylquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 20 percent / potassium carbonate / ethanol / 8 h / Ambient temperature 2: 32 percent / benzene / Irradiation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h / 25 °C / 750.08 - 2250.23 Torr / Inert atmosphere 2.1: acetic anhydride / tetrahydrofuran / Inert atmosphere 2.2: 120 °C / Inert atmosphere; Sealed tube View Scheme |
Conditions | Yield |
---|---|
Sealed tube; | 100% |
In ethanol at 79℃; for 12h; Sealed tube; | 25.06% |
6-(N,N-dimethylamino)-2-methylquinoline
mesitylenesulfonylhydroxylamine
2,4,6-Trimethyl-benzenesulfonate1-amino-6-dimethylamino-2-methyl-quinolinium;
Conditions | Yield |
---|---|
In dichloromethane for 1h; Ambient temperature; | 88% |
Conditions | Yield |
---|---|
With C52H49B9CuN2P2; oxygen; m-Toluic acid In methanol; acetonitrile for 35h; Photolysis; | 77% |
6-(N,N-dimethylamino)-2-methylquinoline
6-(dimethylamino)quinoline-2-carboxaldehyde
Conditions | Yield |
---|---|
With selenium(IV) oxide In 1,4-dioxane; water at 80℃; for 4h; | 58% |
With selenium(IV) oxide | 40% |
With selenium(IV) oxide In 1,4-dioxane; water at 80℃; for 4h; | 38% |
Conditions | Yield |
---|---|
In ethanol at 60℃; for 12h; | 43.72% |
6-(N,N-dimethylamino)-2-methylquinoline
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate In chloroform at 0℃; for 1h; Vilsmeier-Haack Formylation; Inert atmosphere; Stage #2: 6-(N,N-dimethylamino)-2-methylquinoline In chloroform for 16h; Vilsmeier-Haack Formylation; Reflux; Inert atmosphere; | 38.6% |
6-(N,N-dimethylamino)-2-methylquinoline
methyl p-toluene sulfonate
6-dimethylamino-1,2-dimethylquinolinium tosylate
Conditions | Yield |
---|---|
In chloroform for 14h; Solvent; Reflux; | 34% |
In chloroform for 12h; Heating / reflux; |
Conditions | Yield |
---|---|
In 1,2-dichloro-benzene at 120℃; for 12h; | 30.44% |
6-(N,N-dimethylamino)-2-methylquinoline
2,5-dimethyl-1-phenyl-1H-pyrrole-3-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 6-(N,N-dimethylamino)-2-methylquinoline; 2,5-dimethyl-1-phenyl-1H-pyrrole-3-carbaldehyde With zinc(II) chloride In N,N-dimethyl-formamide at 160℃; Stage #2: With sodium hydroxide; water In N,N-dimethyl-formamide | 2.1% |
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With ethanol |
6-(N,N-dimethylamino)-2-methylquinoline
3-(4-dimethylamino-phenyl)-propenal
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
at 140 - 150℃; |
Conditions | Yield |
---|---|
With ethanol |
6-(N,N-dimethylamino)-2-methylquinoline
4-dimethylamino-benzaldehyde
[2-(4-dimethylamino-trans-styryl)-[6]quinolyl]-dimethyl-amine
Conditions | Yield |
---|---|
With hydrogenchloride at 120℃; |
Conditions | Yield |
---|---|
at 140 - 150℃; |
6-(N,N-dimethylamino)-2-methylquinoline
7-Dimethylamino-2-methyl-benzo[d][1,3]diazepine-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 88 percent / CH2Cl2 / 1 h / Ambient temperature 2: 20 percent / potassium carbonate / ethanol / 8 h / Ambient temperature 3: 26 percent / benzene / Irradiation View Scheme |
6-(N,N-dimethylamino)-2-methylquinoline
C15H19N3O2
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 88 percent / CH2Cl2 / 1 h / Ambient temperature 2: 20 percent / potassium carbonate / ethanol / 8 h / Ambient temperature View Scheme |
6-(N,N-dimethylamino)-2-methylquinoline
(6-(dimethylamino)quinolin-2-yl)methanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: selenium(IV) oxide / water; 1,4-dioxane / 4 h / 80 °C 2: sodium tetrahydroborate / ethanol / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: selenium(IV) oxide / 1,4-dioxane; water / 3 h / 80 °C / Inert atmosphere 2: sodium tetrahydroborate; ethanol / 1 h / 0 - 20 °C / Inert atmosphere View Scheme |
6-(N,N-dimethylamino)-2-methylquinoline
(6-(dimethylamino)quinolin-2-yl)methyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: selenium(IV) oxide / water; 1,4-dioxane / 4 h / 80 °C 2: sodium tetrahydroborate / ethanol / 1 h / 20 °C 3: triethylamine; dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere; Darkness View Scheme |
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