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high purity Application:Drug intermediates Materials intermediates and active molecules
(S)-Malic acid
(E)-3-Ureido-but-2-enoic acid ethyl ester
A
2H-pyran-2-one-5-carboxylic acid
B
3-oxopropanoic acid
3-methoxy-2-propen-1-oic acid
3-oxopropanoic acid
Conditions | Yield |
---|---|
With sulfuric acid |
(S)-Malic acid
(E)-3-Ureido-but-2-enoic acid ethyl ester
phenol
A
3-oxopropanoic acid
B
coumarin
Conditions | Yield |
---|---|
analoge Reaktionen mit anderen ein- und mehrwertigen Phenolen; |
(E)-β-morpholino acrylonitrile
3-oxopropanoic acid
Conditions | Yield |
---|---|
With hydrogenchloride at 80℃; |
Conditions | Yield |
---|---|
With tetramethyl ammoniumhydroxide |
Conditions | Yield |
---|---|
With potassium bromate; thallium(III) sulfate; sulfuric acid In water; acetic acid at 40℃; for 60h; Rate constant; Mechanism; Thermodynamic data; other mineral acid; other metal ion; E(excit.), ΔH(excit.), ΔS(excit.), ΔG(excit.); |
L-Aspartic acid
chloroamine-T
A
3-oxopropanoic acid
B
toluene-4-sulfonamide
Conditions | Yield |
---|---|
With perchloric acid; sodium perchlorate; chloride In water at 39.9℃; Rate constant; Mechanism; Thermodynamic data; in absence or presence of methanol, add of PTS, variation of ionic strength; ΔH(excit.), -ΔS(excit.), ΔG(excit.); |
Conditions | Yield |
---|---|
With perchloric acid; N-bromoacetamide In water at 29.9℃; for 12h; Rate constant; Kinetics; Thermodynamic data; mechanism, ΔF (exit), ΔH (exit), ΔS (exit); | |
With manganese(II) sulfate; manganese(III) sulfate; sulfuric acid; sodium perchlorate; sodium sulfate In water at 29.9℃; Rate constant; Thermodynamic data; Mechanism; var. of reagents, conc., ratio, ionic strength, pH, additives, dielectric const. of solvent, Ea, ΔH(excit.), ΔS(excit.), ΔG(excit.); | |
With perchloric acid; ammonium cerium(IV) nitrate; nitric acid In water at 35℃; Rate constant; Mechanism; var. ratio; | |
With perchloric acid; N-bromoacetamide In water at 29.9℃; for 12h; | |
With potassium permanganate; sulfuric acid at 39.85℃; Kinetics; Further Variations:; Temperatures; conc. of H2SO4; Deamination; decarboxylation; |
Conditions | Yield |
---|---|
With manganese(III) pyrophosphate; sulfuric acid In water at 35℃; for 72h; Rate constant; Mechanism; Thermodynamic data; further reagents - Mn(2+), H2SO4; | |
With potassium bromate; hydrogenchloride; water Rate constant; Thermodynamic data; kobs vs. substrate concentration at 35 deg C and vs. HCl concentration at 40 deg C; ΔH(excit), ΔS(excit) (temp.-range 30-45 deg C); | |
With sodium hydroxide; sodium hypochlorite In water var. pH values; other hydroxyacids; | |
With perchloric acid; mercury(II) diacetate; acetic acid In water at 313℃; Kinetics; Temperature; Concentration; |
sodium sulbactam
A
3-oxopropanoic acid
B
2-amino-3-methyl-3-sulfinobutanoic acid
Conditions | Yield |
---|---|
With borate buffer at 65℃; for 1.5h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 30℃; Mechanism; Thermodynamic data; activation energy, ΔG(excit.); |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver nitrate In water at 33℃; Rate constant; Thermodynamic data; Mechanism; ΔE(activ.); ΔH(activ.); ΔS(activ.); presence of allyl acetate.; | |
With [2,2]bipyridinyl; perchloric acid; ammonium cerium(IV) nitrate; silver(I) In water at 50℃; Kinetics; Rate constant; Mechanism; var. of conc., pH, ionic strength, temp., without bipyridyl; | |
With sulfuric acid; manganese(III) ion at 40℃; Kinetics; Temperature; |
Conditions | Yield |
---|---|
With chloroamine-T; hypochloric acid In water at 30℃; Kinetics; Mechanism; var. pH, var. temp.; |
Conditions | Yield |
---|---|
With ruthenium trichloride; perchloric acid; bromate salt; sulfuric acid; mercury(II) diacetate In water at 19.9 - 39.9℃; Rate constant; |
Conditions | Yield |
---|---|
With hydrogenchloride; N-chloronicotinamide; sodium perchlorate In acetic acid at 39.85℃; for 12h; Kinetics; Further Variations:; Temperatures; concentration of amino acid; concentration of reagents; Oxidation; |
3-oxopropanoic acid
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
die Produkte zerfallen weiter in Acetaldehyd,Kohlendioxyd,Kohlenoxyd und Wasser; |
(S)-Malic acid
sulfuric acid
phenol
A
3-oxopropanoic acid
B
coumarin
Conditions | Yield |
---|---|
analoge Reaktionen mit anderen ein- und mehrwertigen Phenolen; |
Conditions | Yield |
---|---|
With mercury(II) diacetate; N-bromoacetamide In acetic acid at 30℃; Kinetics; Mechanism; Thermodynamic data; other temperatures, E(act.), ΔH(excit.), ΔS(excit.), ΔG(excit.); various solvent concentrations, effect of added salts; |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; perchloric acid; mercury(II) diacetate; palladium dichloride at 35℃; Rate constant; Kinetics; Mechanism; energy data: ΔE(a), ΔH(excit.), ΔS(excit.), ΔG(excit.); various NBS, PdCl2 and HClO4 concentrations; also in the presence of var. amounts of NaCl; other hydroxyacids; |
Conditions | Yield |
---|---|
With potassium peroxydiphosphate; sulfuric acid; ruthenium trichloride at 39.9℃; Kinetics; Mechanism; Thermodynamic data; ΔH(excit.), ΔS(excit.), other temperatures; |
Conditions | Yield |
---|---|
With sodium hydroxide; bromamine T In water at 20℃; Thermodynamic data; Kinetics; Mechanism; Ea, ΔH(excit.), ΔS(excit.), ΔG(excit.), solvent isotopic effect; |
ethanol
S-benzyl thiosuccinic acid
A
4-butanolide
B
3-oxopropanoic acid
(S)-Malic acid
sulfuric acid
A
2H-pyran-2-one-5-carboxylic acid
B
3-oxopropanoic acid
Conditions | Yield |
---|---|
With perchloric acid; sodium dodecyl-sulfate; chloroamine-T at 35℃; Kinetics; Further Variations:; Temperatures; Reagents; |
Conditions | Yield |
---|---|
With oxone In acetate buffer at 35℃; for 48h; pH=4.2; Kinetics; Further Variations:; pH-values; Temperatures; | |
With oxone In acetate buffer at 20.84℃; pH=4.2; Activation energy; Further Variations:; Temperatures; | |
With α-ketoglutarate Enzyme kinetics; |
2-oxo-propionic acid
3-amino propanoic acid
A
L-alanin
B
3-oxopropanoic acid
Conditions | Yield |
---|---|
With pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 In aq. phosphate buffer at 37℃; for 0.0833333h; pH=7.4; Enzymatic reaction; enantioselective reaction; |
(2R)-aspartic acid
pyridoxal hydrochloride
A
3-oxopropanoic acid
B
pyridoxamine
Conditions | Yield |
---|---|
In ethanol; water for 0.5h; Kinetics; |
Conditions | Yield |
---|---|
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 93% |
3-oxopropanoic acid
methyl 3-bromophenethylcarbamate
Conditions | Yield |
---|---|
With sulfuric acid In tetrahydrofuran Reflux; | 91.3% |
pyrid-2-ylhydrazine
3-oxopropanoic acid
5-hydroxy-1-(2-pyridyl)-1H-pyrazole
Conditions | Yield |
---|---|
In ethanol at 0 - 100℃; for 72h; | 90% |
3-oxopropanoic acid
3-trifluoromethyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazine
Conditions | Yield |
---|---|
Stage #1: 3-oxopropanoic acid With thionyl chloride; sulfuric acid In dichloromethane; N,N-dimethyl-formamide for 6h; Heating; Stage #2: 3-trifluoromethyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazine With triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 2h; Solvent; Temperature; Reagent/catalyst; | 75.3% |
Conditions | Yield |
---|---|
Stage #1: 3-oxopropanoic acid; 4-acetyl-benzoic acid In acetic acid at 110℃; for 20h; Stage #2: methylhydrazine With ammonia In water for 5h; pH=9; Heating / reflux; Stage #3: With hydrogenchloride pH=1 - 2; | 33% |
Conditions | Yield |
---|---|
Hydrierung des Reaktionsprodukts an Platin in Wasser oder Essigsaeure; |
3-oxopropanoic acid
N-(4-{[(aminoiminomethyl)amino]sulfonyl}phenyl)acetamide
N-acetyl-sulfanilic acid-(6-oxo-1,6-dihydro-pyrimidin-2-ylamide)
3-oxopropanoic acid
1-amino-4-({[amino(imino)methyl]amino}sulfonyl)benzene
sulfanilic acid-(6-oxo-1,6-dihydro-pyrimidin-2-ylamide)
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