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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

1,3-Cyclooctadione CAS:935-29-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed

1,3-Cyclooctadione CAS:935-29-5

Cas:935-29-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Bright Chemical Co., Ltd.

best seller Application:API

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,3-Cyclooctadione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chungking Joyinchem Co., Ltd.

Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

1,3-Cyclooctanedione Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai PotentPharm Science and Technology Co.,Ltd

1 good quality, better price and bettter service;2 Timely delivery;3 100% refunded if parcel is t delivered or poor quality.We will try to satisfy you upon receipt of your reply. I hope that we can become a long-term cooperative partner. Application:

1,3-Cyclooctanedione

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

935-29-5

Cas:935-29-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

1,7-bis(trimethylsiloxy)bicyclo[5.1.0]octane
80893-84-1

1,7-bis(trimethylsiloxy)bicyclo[5.1.0]octane

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With iron(III) chloride In N,N-dimethyl-formamide at 60℃; for 16h;73%
With iron(III) chloride In N,N-dimethyl-formamide at 60 - 70℃; for 3.25h;
With iron(III) chloride In N,N-dimethyl-formamide at 60℃;
9-oxabicyclo[6.1.0]nonan-2-one
57260-84-1

9-oxabicyclo[6.1.0]nonan-2-one

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); 1,2-bis-(diphenylphosphino)ethane In toluene at 140℃; for 96h;52%
With 4-(1-hydroxy-2-(methylamino)ethyl)-1,2-phenylene bis(2,2-dimethylpropanoate); tetrakis(triphenylphosphine) palladium(0) In toluene at 140℃; for 96h;52%
2-Hydroxy-2-methoxymethyl-cycloheptanone
78743-58-5

2-Hydroxy-2-methoxymethyl-cycloheptanone

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With potassium hydrogensulfate at 170 - 180℃; under 20 - 25 Torr;51%
(Z)-cyclooct-2-enone
23202-10-0

(Z)-cyclooct-2-enone

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With tert.-butylhydroperoxide; sodium tetrachloropalladate(II) In water; isopropyl alcohol at 50℃; Wacker-Tsuji oxidation; Inert atmosphere;37%
1-Trimethylsiloxy-bicyclo[5.1.0]octan
50338-48-2

1-Trimethylsiloxy-bicyclo[5.1.0]octan

A

3-hydroxycyclooctan-1-one
37996-43-3

3-hydroxycyclooctan-1-one

B

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With bis(acetylacetonate)oxovanadium; oxygen In ethanol Ambient temperature;A 31%
B 33%
With vanadyl acetylacetonate; oxygen In ethanol at 20℃; for 20h;A 31%
B 33%
cis-cyclooctane-1,3-diol
291273-22-8

cis-cyclooctane-1,3-diol

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With chromium(VI) oxide In acetone
1-Chlor-3-brom-cycloocten-(1)
6498-54-0

1-Chlor-3-brom-cycloocten-(1)

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multistep reaction;
1-Brom-cyclooct-1-en-3-on
6518-11-2

1-Brom-cyclooct-1-en-3-on

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
(i) Mor, (ii) aq. HCl; Multistep reaction;
1,2-Bis-(trimethylsiloxy)-cyclohepten-(1)
19719-90-5

1,2-Bis-(trimethylsiloxy)-cyclohepten-(1)

Bromoform
75-25-2

Bromoform

Et2Zn

Et2Zn

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
solvent: toluene, 0 grad C, 1 hr.; Yield given. Multistep reaction;
trans-cyclooctane-1,3-diol

trans-cyclooctane-1,3-diol

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With chromium(VI) oxide
1,4-dioxa-spiro[4.7]dodecan-7-one

1,4-dioxa-spiro[4.7]dodecan-7-one

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
With sulfuric acid In diethyl ether; chloroform
(Z)-1,4-dioxaspiro[4.7]dodec-6-ene
1728-26-3

(Z)-1,4-dioxaspiro[4.7]dodec-6-ene

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 9-BBN / tetrahydrofuran / 48 h / 20 °C
1.2: 76 percent / NaOH; aq. H2O2 / tetrahydrofuran; ethanol / 1 h / Heating
2.1: oxalyl chloride; DMSO; Et3N / CHCl3 / 1 h / -78 - -10 °C
3.1: H2SO4 / diethyl ether; CHCl3
View Scheme
Multi-step reaction with 2 steps
1: pyridinium p-toluenesulfonate / water; acetone / Reflux; Inert atmosphere
2: tert.-butylhydroperoxide; sodium tetrachloropalladate(II) / water; isopropyl alcohol / 50 °C / Inert atmosphere
View Scheme
1,4-dioxaspiro[4,7]dodecan-7-ol
685109-33-5

1,4-dioxaspiro[4,7]dodecan-7-ol

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: oxalyl chloride; DMSO; Et3N / CHCl3 / 1 h / -78 - -10 °C
2: H2SO4 / diethyl ether; CHCl3
View Scheme
1,2-Bis-(trimethylsiloxy)-cyclohepten-(1)
19719-90-5

1,2-Bis-(trimethylsiloxy)-cyclohepten-(1)

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et2Zn / toluene / 2.25 h / Ambient temperature
2: FeCl3 / dimethylformamide / 3.25 h / 60 - 70 °C
View Scheme
Multi-step reaction with 2 steps
1: 97 percent / diethylzinc / toluene / 16 h / Ambient temperature
2: 73 percent / FeCl3 / dimethylformamide / 16 h / 60 °C
View Scheme
Multi-step reaction with 2 steps
1: 48 percent / Zn/Cu-(CH3)2CHI / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) room temperature, 2 h
2: 51 percent / potassium hydrogen sulfate / 170 - 180 °C / 20 - 25 Torr
View Scheme
Multi-step reaction with 2 steps
1: diethylzinc / toluene
2: iron(III) chloride / N,N-dimethyl-formamide / 60 °C
View Scheme
dimethyl 1,7-heptanedioate
1732-08-7

dimethyl 1,7-heptanedioate

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Na sand / toluene / Heating
2: Et2Zn / toluene / 2.25 h / Ambient temperature
3: FeCl3 / dimethylformamide / 3.25 h / 60 - 70 °C
View Scheme
diethyl pimelate
2050-20-6

diethyl pimelate

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 96 percent / Na / toluene / 96 h / Heating
2: 97 percent / diethylzinc / toluene / 16 h / Ambient temperature
3: 73 percent / FeCl3 / dimethylformamide / 16 h / 60 °C
View Scheme
Multi-step reaction with 2 steps
1: Na / toluene / 96 h
2: solvent: toluene, 0 grad C, 1 hr.
View Scheme
cis-Cyclooctyl-1,3-diacetat

cis-Cyclooctyl-1,3-diacetat

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether
2: CrO3 / acetone
View Scheme
(Z)-Cyclooctene
931-88-4, 931-87-3

(Z)-Cyclooctene

<(η5-C5H5)Fe(CO)2(CH2OSi(CH3)3)>

<(η5-C5H5)Fe(CO)2(CH2OSi(CH3)3)>

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: Br2 / CCl4
2: Mor / toluene / Heating
3: NBS, AIBN, CaCO3 / CCl4
4: acetic acid
5: KOH / methanol / Ambient temperature
6: NBS, Py / CCl4 / Heating
7: (i) Mor, (ii) aq. HCl
View Scheme
cycloactanone
502-49-8

cycloactanone

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: PCl3, benzene-1,2-diol / Heating
2: NBS, AIBN, CaCO3 / CCl4
View Scheme
Multi-step reaction with 5 steps
1: hydrogenchloride; bromine / ethanol; water / 72 h / 0 °C / Inert atmosphere
2: toluene-4-sulfonic acid / benzene / 24 h / Reflux; Inert atmosphere
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 160 °C / Inert atmosphere
4: pyridinium p-toluenesulfonate / water; acetone / Reflux; Inert atmosphere
5: tert.-butylhydroperoxide; sodium tetrachloropalladate(II) / water; isopropyl alcohol / 50 °C / Inert atmosphere
View Scheme
(E)-1-Bromo-cyclooctene
61815-42-7

(E)-1-Bromo-cyclooctene

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: NBS, AIBN, CaCO3 / CCl4
2: acetic acid
3: KOH / methanol / Ambient temperature
4: NBS, Py / CCl4 / Heating
5: (i) Mor, (ii) aq. HCl
View Scheme
1,2-dibromocyclooctane
29974-69-4

1,2-dibromocyclooctane

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: Mor / toluene / Heating
2: NBS, AIBN, CaCO3 / CCl4
3: acetic acid
4: KOH / methanol / Ambient temperature
5: NBS, Py / CCl4 / Heating
6: (i) Mor, (ii) aq. HCl
View Scheme
(E)-1-Chloro-cyclooctene
86428-68-4

(E)-1-Chloro-cyclooctene

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NBS, AIBN, CaCO3 / CCl4
View Scheme
1-Brom-3-hydroxy-cycloocten-(1)
6518-10-1

1-Brom-3-hydroxy-cycloocten-(1)

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NBS, Py / CCl4 / Heating
2: (i) Mor, (ii) aq. HCl
View Scheme
1,3-Dibrom-cycloocten-(1)
6518-05-4

1,3-Dibrom-cycloocten-(1)

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid
2: KOH / methanol / Ambient temperature
3: NBS, Py / CCl4 / Heating
4: (i) Mor, (ii) aq. HCl
View Scheme
1-Brom-3-acetoxy-cycloocten-(1)
6518-09-8

1-Brom-3-acetoxy-cycloocten-(1)

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: KOH / methanol / Ambient temperature
2: NBS, Py / CCl4 / Heating
3: (i) Mor, (ii) aq. HCl
View Scheme
2-bromocyclooctan-1-one
39261-18-2

2-bromocyclooctan-1-one

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / benzene / 24 h / Reflux; Inert atmosphere
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 160 °C / Inert atmosphere
3: pyridinium p-toluenesulfonate / water; acetone / Reflux; Inert atmosphere
4: tert.-butylhydroperoxide; sodium tetrachloropalladate(II) / water; isopropyl alcohol / 50 °C / Inert atmosphere
View Scheme
2-Brom-1-cyclooctanon-ethylenacetal
73274-50-7

2-Brom-1-cyclooctanon-ethylenacetal

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 160 °C / Inert atmosphere
2: pyridinium p-toluenesulfonate / water; acetone / Reflux; Inert atmosphere
3: tert.-butylhydroperoxide; sodium tetrachloropalladate(II) / water; isopropyl alcohol / 50 °C / Inert atmosphere
View Scheme
Isopropenyl acetate
108-22-5

Isopropenyl acetate

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

1,3-diacetoxy-1,3-cyclooctadiene
138196-40-4

1,3-diacetoxy-1,3-cyclooctadiene

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 90℃;99%
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

methyl iodide
74-88-4

methyl iodide

2,2-dimethylcyclooctane-1,3-dione
55277-52-6

2,2-dimethylcyclooctane-1,3-dione

Conditions
ConditionsYield
With potassium carbonate In acetone Ambient temperature;97%
With potassium carbonate In N,N-dimethyl-formamide; acetone for 30h; Heating;97%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

1,3-bis-(trimethylsilyloxy)-1,3-cyclooctadiene

1,3-bis-(trimethylsilyloxy)-1,3-cyclooctadiene

Conditions
ConditionsYield
Stage #1: 1,3-cyclooctanedione With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at 0℃; deprotonation;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran at 0℃; silylation; Further stages.;
76%
With N,N,N,N,N,N-hexamethylphosphoric triamide; diisopropylamine; lithium diisopropyl amide In tetrahydrofuran; hexane at 0℃; for 3h;76%
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

2,2-difluoro-1,3-cyclooctanedione
1047997-32-9

2,2-difluoro-1,3-cyclooctanedione

Conditions
ConditionsYield
With caesium carbonate; Selectfluor In acetonitrile at 0 - 20℃; Inert atmosphere;73%
Stage #1: 1,3-cyclooctanedione With caesium carbonate In acetonitrile at 0℃; for 0.25h; Inert atmosphere;
Stage #2: With Selectfluor In acetonitrile at 0 - 20℃; for 6.25h;
69%
Stage #1: 1,3-cyclooctanedione With caesium carbonate In acetonitrile at 20℃; for 0.5h; Inert atmosphere;
Stage #2: With Selectfluor In acetonitrile at 20℃; for 1.5h; Cooling with ice; Inert atmosphere;
31.1%
Ketene
463-51-4

Ketene

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

A

Acetic acid (E)-3-oxo-cyclooct-1-enyl ester
109853-13-6

Acetic acid (E)-3-oxo-cyclooct-1-enyl ester

B

1,3-diacetoxy-1,3-cyclooctadiene
138196-40-4

1,3-diacetoxy-1,3-cyclooctadiene

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 125℃; for 10h;A 8%
B 57%
all-trans-Retinal
116-31-4

all-trans-Retinal

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

retinylidene-1,3-cyclooctanedione

retinylidene-1,3-cyclooctanedione

Conditions
ConditionsYield
With piperidine; acetic acid In toluene Ambient temperature;56%
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

benzylamine
100-46-9

benzylamine

N1,N7-dibenzylheptanediamide

N1,N7-dibenzylheptanediamide

Conditions
ConditionsYield
With iodine; tetrabutylammoniun azide; 4-pyrrolidin-1-ylpyridine In tetrahydrofuran at 20℃; for 12h;51%
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

ethylene dibromide
106-93-4

ethylene dibromide

A

spiro[2.7]decane-4,10-dione

spiro[2.7]decane-4,10-dione

B

3-(2-bromoethoxy)cyclooct-2-en-1-one

3-(2-bromoethoxy)cyclooct-2-en-1-one

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 30℃; for 11.1667h;A 24%
B 14%
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

<2,2,4,4,8,8-D6>-Cyclo-octan-1,3-dion
31465-58-4

<2,2,4,4,8,8-D6>-Cyclo-octan-1,3-dion

Conditions
ConditionsYield
With water-d2
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

4-chloro-aniline
106-47-8

4-chloro-aniline

2-(p-Chlor-phenylhydrazono)-cyclooctandion-(1,3)
6518-12-3

2-(p-Chlor-phenylhydrazono)-cyclooctandion-(1,3)

Conditions
ConditionsYield
(i) NaNO2, aq. H2SO4, (ii) /BRN= 2354368/, NaOAc; Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

4-nitro-aniline
100-01-6

4-nitro-aniline

2-(p-Nitro-phenylhydrazono)-cyclooctandion-(1,3)

2-(p-Nitro-phenylhydrazono)-cyclooctandion-(1,3)

Conditions
ConditionsYield
(i) NaNO2, aq. HCl, (ii) /BRN= 2354368/, NaOAc; Multistep reaction;
3-phenylbut-3-en-1-yl 4-methylbenzenesulfonate
16728-06-6

3-phenylbut-3-en-1-yl 4-methylbenzenesulfonate

1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

3-<(3-phenyl-3-butenyl)oxy>-2-cycloocten-1-one
109183-23-5

3-<(3-phenyl-3-butenyl)oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium hexamethylsilazane 1.) DME, toluene; 0 deg. C , 30 min. 2.) DME, toluene; 60 deg. C ,16h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

but-3-enyl 4-methylbenzenesulfonate
778-29-0

but-3-enyl 4-methylbenzenesulfonate

3-(3-butenyloxy)-2-cycloocten-1-one
108162-99-8

3-(3-butenyloxy)-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 2.) DME, 60 degC, 16 h; Yield given. Multistep reaction;
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

4-methylpent-3-enyl 4-methylbenzenesulfonate
783-86-8

4-methylpent-3-enyl 4-methylbenzenesulfonate

3-<(4-methyl-3-pentenyl)oxy>-2-cycloocten-1-one
108163-02-6

3-<(4-methyl-3-pentenyl)oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 60 degC, 16 h; Yield given. Multistep reaction;
With potassium hexamethylsilazane 1.) DME, toluene; 0 deg. C , 30 min. 2.) DME, toluene; 60 deg. C ,16h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

4-phenyl-3-butenyl para-toluenesulfonate
93652-37-0, 7515-44-8

4-phenyl-3-butenyl para-toluenesulfonate

3-<((E)-4-phenyl-3-butenyl)oxy>-2-cycloocten-1-one
108176-31-4, 109183-21-3

3-<((E)-4-phenyl-3-butenyl)oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 60 deg C, 16 h; Yield given. Multistep reaction;
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

(±)-2-methylbut-3-en-1-yl 4-methylbenzenesulfonate
71394-00-8

(±)-2-methylbut-3-en-1-yl 4-methylbenzenesulfonate

3-<(2-methyl-3-butenyl)oxy>-2-cycloocten-1-one
109183-18-8

3-<(2-methyl-3-butenyl)oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

(E)-hexa-3,5-dien-1-yl 4-methylbenzenesulfonate
36206-73-2

(E)-hexa-3,5-dien-1-yl 4-methylbenzenesulfonate

3-<(E)-3,5-hexadienyloxy>-2-cycloocten-1-one
108163-00-4, 109183-19-9

3-<(E)-3,5-hexadienyloxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 2.) DME, 60 deg C, 16 h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

triethyloxonium fluoroborate
368-39-8

triethyloxonium fluoroborate

3-(ethoxy)-2-cycloocten-1-one
109183-16-6

3-(ethoxy)-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 1.) DME, 60 min, 2.) DME,CH2Cl2, 30 min; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Toluene-4-sulfonic acid (E)-5-trimethylsilanyl-pent-3-enyl ester
108162-98-7

Toluene-4-sulfonic acid (E)-5-trimethylsilanyl-pent-3-enyl ester

3-<<(E)-5-(trimethylsilyl)-3-pentenyl>oxy>-2-cycloocten-1-one
108163-03-7, 109183-26-8, 109183-27-9

3-<<(E)-5-(trimethylsilyl)-3-pentenyl>oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

(Z)-hexa-3,5-dienyl p-toluenesulfonate
87463-28-3

(Z)-hexa-3,5-dienyl p-toluenesulfonate

3-<(E)-3,5-hexadienyloxy>-2-cycloocten-1-one
108163-00-4, 109183-19-9

3-<(E)-3,5-hexadienyloxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

Toluene-4-sulfonic acid (E)-2-methyl-hexa-3,5-dienyl ester
109183-42-8

Toluene-4-sulfonic acid (E)-2-methyl-hexa-3,5-dienyl ester

3-<((E)-2-methyl-3,5-hexadienyl)oxy>-2-cycloocten-1-one
109183-28-0

3-<((E)-2-methyl-3,5-hexadienyl)oxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With tert-butoxide 1.) DME, -10 deg. C, 40 min. 2.) DME, 60 deg. C, 24h; Yield given. Multistep reaction;
1,3-cyclooctanedione
935-29-5

1,3-cyclooctanedione

3-heptenyl toluenesulfonate
100566-38-9

3-heptenyl toluenesulfonate

3-<(E)-3-heptenyloxy>-2-cycloocten-1-one
108163-01-5, 109183-20-2

3-<(E)-3-heptenyloxy>-2-cycloocten-1-one

Conditions
ConditionsYield
With potassium tert-butylate 60 deg C, 16 h; Yield given. Multistep reaction;
With potassium hexamethylsilazane 1.) DME, toluene; 0 deg. C , 30 min. 2.) DME, toluene; 60 deg. C ,16h; Yield given. Multistep reaction;

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