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inquiry2-methyl-2-phenoxypropanoic acid Application:2-methyl-2-phenoxypropanoic acid
ethyl 2-methyl-2-phenoxypropanoate
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide In ethanol at 26℃; for 0.5h; | 94.1% |
With water; sodium hydroxide In ethanol at 26℃; for 0.5h; | 94.1% |
With potassium hydroxide | |
Stage #1: ethyl 2-methyl-2-phenoxypropanoate With methanol; lithium hydroxide; water In tetrahydrofuran at 20℃; Stage #2: With hydrogenchloride In tetrahydrofuran; water pH=2; | |
Stage #1: ethyl 2-methyl-2-phenoxypropanoate With water; lithium hydroxide In methanol for 3h; Reflux; Stage #2: With hydrogenchloride In water pH=2; |
Conditions | Yield |
---|---|
Stage #1: C12H15IO2 With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Stage #2: With potassium hydroxide; water In methanol at 50℃; for 12h; | A 83% B 8.3% |
A
2,2-dimethylbenzofuran-3(2H)-one
B
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-iodophenoxy)-2-methylpropanoate With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Stage #2: With potassium hydroxide In methanol; water at 50℃; for 12h; Inert atmosphere; | A 83% B 8% |
Conditions | Yield |
---|---|
Stage #1: phenol With sodium hydroxide In butanone at 50℃; for 2h; Stage #2: 2-bromo-2-methylpropionic acid In butanone at 50℃; for 12h; | 81% |
Multistep reaction.; |
1,1,1-trichloro-2-methyl-2-propanol
phenol
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
With sodium hydroxide In acetone at 0 - 20℃; for 4h; | 38% |
Conditions | Yield |
---|---|
With potassium permanganate; sodium carbonate |
tetrachloromethane
acetone
1,1,1-trichloro-2-methyl-2-propanol
phenol
2-methyl-2-phenoxypropionic acid
tetrachloromethane
chloroform
acetone
phenol
2-methyl-2-phenoxypropionic acid
tetrachloromethane
2-methyllactic acid
acetone
phenol
2-methyl-2-phenoxypropionic acid
tetrachloromethane
acetone
phenol
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With sodium hydroxide | |
With potassium hydroxide | |
Stage #1: acetone; phenol With sodium hydroxide at 20℃; for 0.5h; Reflux; Stage #2: chloroform In acetone for 3.5h; Reflux; Stage #3: With hydrogenchloride; water |
Conditions | Yield |
---|---|
With sodium hydroxide; acetone |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 160 °C 2: aqueous KOH-solution View Scheme |
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; methanol; water | |
With potassium hydroxide In 1,4-dioxane; methanol; water |
ethyl 2-methyl-2-phenoxypropanoate
A
2,2-dimethylbenzofuran-3(2H)-one
B
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water for 12h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: caesium carbonate / acetonitrile / 16 h / 25 °C / Reflux 2: sodium hydroxide; water / ethanol / 0.5 h / 26 °C View Scheme | |
Multi-step reaction with 2 steps 1: caesium carbonate / acetonitrile / 16 h / 25 °C / Reflux 2: sodium hydroxide; water / ethanol / 0.5 h / 26 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide In chloroform for 3h; Heating; | 1.34 g |
Conditions | Yield |
---|---|
In ethanol; water reflux (4 h), solvent evapn.; elem. anal.; | 99.9% |
2-methyl-2-phenoxypropionic acid
benzylamine
N-Benzyl-2-methyl-2-phenoxy-propionamide
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane | 94% |
Conditions | Yield |
---|---|
With tert-Amyl alcohol; t-Boc-L-valine; oxygen; palladium diacetate; potassium hydrogencarbonate at 90℃; for 24h; Schlenk technique; | 91% |
methanol
7-amino-2,4-dimethyl-1,8-naphthyridine
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
for 0.25h; | 89.04% |
Conditions | Yield |
---|---|
In methanol | 88.51% |
[2,2]bipyridinyl
2-methyl-2-phenoxypropionic acid
zinc(II) acetate dihydrate
Conditions | Yield |
---|---|
Stage #1: 2-methyl-2-phenoxypropionic acid; zinc(II) acetate dihydrate In methanol at 60℃; for 0.333333h; Stage #2: [2,2]bipyridinyl In methanol at 60℃; for 0.1h; | 77.93% |
2-methyl-2-phenoxypropionic acid
hexamethylenetetramine
cadmium(II) acetate dihydrate
Conditions | Yield |
---|---|
Stage #1: 2-methyl-2-phenoxypropionic acid; hexamethylenetetramine; cadmium(II) acetate dihydrate In methanol; ethanol at 20℃; for 2h; Stage #2: With ammonia In methanol; ethanol | 77.49% |
Conditions | Yield |
---|---|
Stage #1: cadmium(II) chloride dihydrate; 2-methyl-2-phenoxypropionic acid; water at 60℃; for 0.333333h; Stage #2: [2,2]bipyridinyl at 60℃; for 0.1h; | 72.4% |
3-(3,4-diossimetilenefenil)-4-ammino-5-mercapto-4H-1,2,4-triazolo
2-methyl-2-phenoxypropionic acid
3-Benzo[1,3]dioxol-5-yl-6-(1-methyl-1-phenoxy-ethyl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
Conditions | Yield |
---|---|
With trichlorophosphate Heating; | 68% |
Conditions | Yield |
---|---|
With sodium hydroxide In water; acetone | 60% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 58.3% |
2-methyl-2-phenoxypropionic acid
Conditions | Yield |
---|---|
Stage #1: 2-methyl-2-phenoxypropionic acid With 1-chloro-1-(dimethylamino)-2-methyl-1-propene In dichloromethane at 20℃; for 0.166667h; Stage #2: (1S,3S)-isopropyl 3-((6-(5-(aminomethyl)-1-methyl-1H-1,2,3-triazol-4-yl)-2-methylpyridin-3-yl)oxy)cyclohexane-1-carboxylate With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 1h; Stage #3: With lithium hydroxide monohydrate In tetrahydrofuran; methanol; water at 20℃; | 47% |
2-methyl-2-phenoxypropionic acid
1,4-dimethyl but-2-enedioate
Conditions | Yield |
---|---|
With potassium phosphate; PrPPTNO; water In acetonitrile at 25 - 32℃; for 16h; Inert atmosphere; Schlenk technique; Darkness; UV-irradiation; | 26% |
formic acid
2-methyl-2-phenoxypropionic acid
1-amino-3-(3,4-dihydroisoquinoline-2(1H)-yl)propan-2-ol
Conditions | Yield |
---|---|
Stage #1: 2-methyl-2-phenoxypropionic acid; 1-amino-3-(3,4-dihydroisoquinoline-2(1H)-yl)propan-2-ol With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 24℃; for 16h; Stage #2: formic acid | 8% |
ethanol
2-methyl-2-phenoxypropionic acid
ethyl 2-methyl-2-phenoxypropanoate
Conditions | Yield |
---|---|
With hydrogenchloride |
2-methyl-2-phenoxypropionic acid
2-methyl-2-phenoxy-propionyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride | |
With thionyl chloride | |
With thionyl chloride |
2-methyl-2-phenoxypropionic acid
2-Methyl-2-(2-nitrophenoxy)propanoic Acid
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
bei der Destillation; |
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