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Cas:97-07-4
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Cas:97-07-4
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Type:Lab/Research institutions
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Cas:97-07-4
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Cas:97-07-4
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
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Cas:97-07-4
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inquiryProduct name: 2-Nitro-4-Methylsulfonylchlorobenzene CAS No.:97-07-4 Molecule Formula:C7H6ClNO4S Molecule Weight:235.64 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:97-07-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:97-07-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:97-07-4
Min.Order:1 Metric Ton
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Cas:97-07-4
Min.Order:100 Gram
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Type:Manufacturers
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Cas:97-07-4
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:97-07-4
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Cas:97-07-4
Min.Order:0
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Cas:97-07-4
Min.Order:1 Kilogram
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Cas:97-07-4
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Cas:97-07-4
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Cas:97-07-4
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inquiryOur mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 25℃; for 2h; | 99.7% |
(nitration); |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium sulfite; sodium hydrogencarbonate / water / 4 h / 75 °C 1.2: 15 h / 105 - 107 °C 2.1: sulfuric acid; nitric acid / 2 h / 25 °C View Scheme |
1-chloro-4-methanesulfonyl-2-nitrobenzene
C12H13NO8S
Conditions | Yield |
---|---|
Stage #1: malonic acid dimethyl ester With potassium tert-butylate In tert-butyl alcohol Stage #2: 1-chloro-4-methanesulfonyl-2-nitrobenzene In tert-butyl alcohol at 20℃; for 15h; Heating / reflux; | 100% |
Conditions | Yield |
---|---|
In ethanol at 40 - 80℃; for 0.5h; | 99% |
With sodium hydroxide |
Conditions | Yield |
---|---|
With sodium hydroxide In dimethyl sulfoxide at 60℃; for 1h; | 96% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
3-Amino-1,2-propanediol
4-(β,γ-dihydroxypropylamino-3-nitro)phenyl methyl sulfone
Conditions | Yield |
---|---|
In dimethyl sulfoxide | 95% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
2-fluorothiophenol
2-(2-fluorophenylthio)-5-(methylsulfonyl)nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 4h; | 95% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
N-(2-cyanoethyl)-N-methylamine
3-[(4-Methanesulfonyl-2-nitro-phenyl)-methyl-amino]-propionitrile
Conditions | Yield |
---|---|
In butan-1-ol at 118℃; for 2h; | 91% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; hydrogen In water; toluene at 160℃; under 30003 Torr; for 36h; Autoclave; | 84% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
(3-chlorophenyl)(pyridin-2-yl)methanamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 130℃; for 0.5h; Sealed tube; Microwave irradiation; | 83% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
5-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one
2,2-dimethyl-5-[4-(methylsulfonyl)-2-nitrophenoxy]-4H-1,3-benzodioxin-4-one
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 7h; | 80% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
N,N-dimethylethylenediamine
4-(β-dimethylaminoethyl)amino-3-nitrophenyl methyl sulfone
Conditions | Yield |
---|---|
In dimethyl sulfoxide; ethyl acetate | 78% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; hydrogen In water; toluene at 160℃; under 30003 Torr; for 36h; Autoclave; | 73% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
2-fluorothiophenol
A
4-(ethylthio)-3-nitrophenyl methyl sulfone
B
2-(2-fluorophenylthio)-5-(methylsulfonyl)nitrobenzene
C
3,4-bis(2-fluorophenylthio)phenyl methyl sulfone
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 3.5h; | A 4.96% B 63% C 8.03 g D 1.50 g |
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 3.5h; | A 4.96 g B 63% C 8.03 g D 1.50 g |
1-chloro-4-methanesulfonyl-2-nitrobenzene
3-ethylamino propionitrile
A
3-nitro-4-ethylaminophenyl methyl sulfone
B
2-nitro-4-methylsulfonyl-N-ethyl-N-β-cyanoethylaniline
Conditions | Yield |
---|---|
In methanol for 42h; Heating; | A 43% B 56% |
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 100℃; for 16h; | 34% |
1-chloro-4-methanesulfonyl-2-nitrobenzene
3,4-dihydroxythiophene-2,5-dicarboxylic acid diethyl ester
Conditions | Yield |
---|---|
With potassium carbonate; lithium bromide In N,N-dimethyl acetamide at 200℃; for 1h; Microwave irradiation; Sealed tube; Inert atmosphere; | 20.9% |
Conditions | Yield |
---|---|
With ethanol; sodium carbonate |
1-chloro-4-methanesulfonyl-2-nitrobenzene
sodium methansulfinate
Conditions | Yield |
---|---|
With ethanol |
1-chloro-4-methanesulfonyl-2-nitrobenzene
sodium methylate
4-methanesulfonyl-1-methoxy-2-nitro-benzene
Conditions | Yield |
---|---|
With methanol |
1-chloro-4-methanesulfonyl-2-nitrobenzene
1-ethoxy-4-methanesulfonyl-2-nitro-benzene
1-chloro-4-methanesulfonyl-2-nitrobenzene
1-fluoro-4-methanesulfonyl-2-nitrobenzene
Conditions | Yield |
---|---|
With potassium fluoride at 180℃; |
1-chloro-4-methanesulfonyl-2-nitrobenzene
bis-(4-methanesulfonyl-2-nitro-phenyl)-sulfide
Conditions | Yield |
---|---|
With alkali sulfide |
1-chloro-4-methanesulfonyl-2-nitrobenzene
4-methoxy-aniline
(4-methanesulfonyl-2-nitro-phenyl)-(4-methoxy-phenyl)-amine
Conditions | Yield |
---|---|
With ethanol |
1-chloro-4-methanesulfonyl-2-nitrobenzene
aniline
(4-methanesulfonyl-2-nitro-phenyl)-phenyl-amine
Conditions | Yield |
---|---|
With ethanol |
carbon disulfide
1-chloro-4-methanesulfonyl-2-nitrobenzene
2-chloro-5-methanesulfonyl-benzothiazole
Conditions | Yield |
---|---|
(i) Na2S3, (ii) /BRN= 1098293/, (iii) SO2Cl2; Multistep reaction; |
1-chloro-4-methanesulfonyl-2-nitrobenzene
1-(4-(methylsulfonyl)-2-nitrophenyl)piperidine
Conditions | Yield |
---|---|
With /BRN= 102438/ In dimethyl sulfoxide at 45℃; Rate constant; |
1-chloro-4-methanesulfonyl-2-nitrobenzene
N-(2-cyanoethyl)-N-methylamine
A
methyl 4-methyl-amino-3-nitrophenyl sulfone
B
3-[(4-Methanesulfonyl-2-nitro-phenyl)-methyl-amino]-propionitrile
Conditions | Yield |
---|---|
In butan-1-ol at 118℃; for 40h; |
1-chloro-4-methanesulfonyl-2-nitrobenzene
3-diethylaminopropionitrile
A
hydrochloride of 3-diethylaminopropionitrile
B
N,N-diethyl-4-(methylsulfonyl)-2-nitroaniline
C
acrylonitrile
Conditions | Yield |
---|---|
In i-Amyl alcohol |
Conditions | Yield |
---|---|
In ethanol for 18h; Ambient temperature; |
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