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inquiry6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane CAS:97664-55-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry6-N-Benzylamino-1-(4'-phenylbutoxy)HexaneAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
6-bromohexyl 4-phenylbutyl ether
benzylamine
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Stage #1: benzylamine With triethylamine; potassium iodide In acetonitrile at 45℃; Stage #2: 6-bromohexyl 4-phenylbutyl ether In acetonitrile | 76% |
With triethylamine; sodium iodide | 75% |
With triethylamine; sodium iodide In dimethyl sulfoxide for 17h; Ambient temperature; | 70% |
With caesium carbonate In N,N-dimethyl-formamide at 60 - 80℃; for 5h; | 38% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; molecular sieve 2.) ethanol; Yield given. Multistep reaction; |
1 ,6-dibromohexane
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C 2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C View Scheme | |
Multi-step reaction with 4 steps 1: 60 percent 2: NaN3 / dimethylformamide 3: lithium aluminum hydride 4: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; tetrabutylammomium bromide / toluene / 10 h / 20 °C 2: triethylamine; potassium iodide / acetonitrile / 45 °C View Scheme |
4-phenyl-butan-1-ol
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C 2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: 81 percent / NaH / tetrahydrofuran / 7 h / Ambient temperature 2: 70 percent / Et3N, NaI / dimethylsulfoxide / 17 h / Ambient temperature View Scheme | |
Multi-step reaction with 4 steps 1: 60 percent 2: NaN3 / dimethylformamide 3: lithium aluminum hydride 4: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; tetrabutylammomium bromide / toluene / 10 h / 20 °C 2: triethylamine; potassium iodide / acetonitrile / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / 2 h / 60 °C 1.2: 4 h / 110 °C 2.1: triethylamine / toluene / 5 h / 5 - 10 °C 3.1: sodium hydroxide / toluene / 12 h / 110 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 81 percent / NaH / tetrahydrofuran / 7 h / Ambient temperature 2: 70 percent / Et3N, NaI / dimethylsulfoxide / 17 h / Ambient temperature View Scheme |
6-bromohexyl 4-phenylbutyl ether
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaN3 / dimethylformamide 2: lithium aluminum hydride 3: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme |
1-azido-6-(4-phenylbutoxy)hexane
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium aluminum hydride 2: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With sodium carbonate In dichloromethane; water at 25 - 30℃; for 0.5h; pH=~ 8; |
6-(4-phenylbutyloxy)hexyl methanesulfonate
benzylamine
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With sodium hydroxide In toluene at 110℃; for 12h; |
1,6-hexanediol
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide / 2 h / 60 °C 1.2: 4 h / 110 °C 2.1: triethylamine / toluene / 5 h / 5 - 10 °C 3.1: sodium hydroxide / toluene / 12 h / 110 °C View Scheme |
6-(4-phenyl-butoxy)-hexan-1-ol
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / toluene / 5 h / 5 - 10 °C 2: sodium hydroxide / toluene / 12 h / 110 °C View Scheme |
3-carbomethoxy-4-hydroxy-α-bromoacetophenone
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
5-(2-{Benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-acetyl)-2-hydroxy-benzoic acid methyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 60℃; | 100% |
With triethylamine In acetonitrile at 20℃; for 0.666667h; Inert atmosphere; |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
D 2543
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In ethanol at 20℃; under 760.051 Torr; | 97.9% |
3'-acetoxymethyl-4'-acetoxy-2-bromoacetophenone
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane at 25℃; for 5h; Reagent/catalyst; Solvent; | 95% |
With potassium carbonate at 20℃; for 4h; |
(R)-2,2-dimethyl-6-(oxiran-2-yl)-4H-benzo[d][1,3]dioxine
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
(R)-2-(benzyl(6-(4-phenylbutoxy)hexyl)amino)-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanol
Conditions | Yield |
---|---|
With triethylamine at 120℃; for 12h; | 83% |
5-(2-bromoacetyl)-2-hydroxybenzaldehyde
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
2-hydroxy-5-<<<6,6-(4-phenylbutoxy)hexylbenzyl>amino>acetyl>benzaldehyde
Conditions | Yield |
---|---|
In acetonitrile for 1h; Heating; other solvent; | 71% |
With N-ethyl-N,N-diisopropylamine In butanone at 0 - 10℃; for 11.5h; | |
With N-ethyl-N,N-diisopropylamine In butanone at 0 - 10℃; |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
2-benzyloxy-5-(R)-oxiranylbenzoic acid methyl ester
2-Benzyloxy-5-((R)-2-{benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-1-hydroxy-ethyl)-benzoic acid methyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran Heating; | 60% |
Bromoacetaldehyde diethyl acetal
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 80℃; for 22h; | 51% |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
In tetrahydrofuran Heating; |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
methyl 4-([1-13C]-α-bromoacetyl)salicylate
C32(13)CH41NO5
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran for 5h; Alkylation; Heating; | |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 60℃; |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: i-Pr2EtN / tetrahydrofuran / 60 °C 2: LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C 3: H2 / 10 percent Pd/C / ethanol / 4 h / 760 Torr View Scheme | |
Multi-step reaction with 3 steps 1: diisopropylethylamine / tetrahydrofuran / 5 h / Heating 2: 146 mg / LiAlD4 / diethyl ether / 2.5 h / Heating 3: 71 percent / H2 / Pd/C / ethanol / 3 h / 20 °C / 760 Torr View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
C31(13)CH40(2)H3NO4
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: i-Pr2EtN / tetrahydrofuran / 60 °C 2: LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: diisopropylethylamine / tetrahydrofuran / 5 h / Heating 2: 146 mg / LiAlD4 / diethyl ether / 2.5 h / Heating View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C 2: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C 3: 77 percent / H2 / 10 percent Pd/C / ethanol / 4 h / 760 Torr View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
C32H40(2)H3NO4
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C 2: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
salmeterol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 71 percent / acetonitrile / 1 h / Heating; other solvent 2: NaBH4 / methanol / 36 h / Ambient temperature 3: 0.21 g / H2 / Pd/C / methanol / 10 h View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride / 10 h / Cooling with ice 2: sodium tetrahydroborate / 8 h / 20 °C 3: palladium 10% on activated carbon / ethanol / 36 h / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1: N-ethyl-N,N-diisopropylamine / butanone / 0 - 10 °C 2: methanol; sodium tetrahydroborate / 8 h / -5 - 30 °C / Inert atmosphere 3: palladium on carbon; hydrogen / methanol / 1.17 h / 25 °C / 413.73 - 517.16 Torr View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / acetonitrile / 0.67 h / 20 °C / Inert atmosphere 2: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere 3: palladium 10% on activated carbon / methanol / 2 h / Inert atmosphere 4: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C / Inert atmosphere View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
4-hydroxy-1-[[[6-(4-phenylbutoxy)hexyl](phenylmethyl)amino]methyl]-1,3-benzenedimethanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 71 percent / acetonitrile / 1 h / Heating; other solvent 2: NaBH4 / methanol / 36 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride / 10 h / Cooling with ice 2: sodium tetrahydroborate / 8 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine / butanone / 0 - 10 °C 2: methanol; sodium tetrahydroborate / 8 h / -5 - 30 °C / Inert atmosphere View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrahydrofuran / Heating 2: 1.) LiAlH4; 2.) H2 / 2.) Pd-C / 1.) THF View Scheme |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60 percent / tetrahydrofuran / Heating 2: 1.) LiAlH4; 2.) H2 / 2.) Pd-C / 1.) THF View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / dichloromethane / 5 h / 25 °C 2: sulfuric acid / ethanol / 25 °C 3: (R)-diphenylprolinol; borane-THF / toluene / Inert atmosphere 4: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 45 °C View Scheme |
8-(benzyloxy)-5-[(1R)-2-bromo-1-(tetrahydro-2H-pyran-2-yloxy)ethyl]quinolin-2(1H)-one
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 120℃; for 4h; |
5-benzyloxy-8-(2,2-dihydroxyacetyl)-4H-benzo[1,4]oxazin-3-one
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
B
5-(benzyloxy)-8-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-2H-1,4-benzoxazin-3 (4H)-one
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-8-(2,2-dihydroxyacetyl)-4H-benzo[1,4]oxazin-3-one; N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine With acetic acid In dichloromethane for 4h; Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 72h; Stage #3: With sodium tetrahydroborate In methanol; dichloromethane for 2h; |
4-(benzyloxy)-7-{(1R)-2-bromo-1-[tetrahydro-2H-pyran-2-yloxy]ethyl}-1,3-benzothiazol-2(3H)-one
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine at 120℃; for 18h; |
benzyl 7-(bromoacetyl)-2-oxo-2,3-dihydro-1,3-benzothiazol-4-yl carbonate
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
7-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-4-hydroxy-1,3-benzothiazol-2(3H)-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 40℃; for 2h; Acidic aqueous solution; |
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
Conditions | Yield |
---|---|
With hydrogenchloride for 10h; Cooling with ice; | |
Multi-step reaction with 2 steps 1: potassium carbonate / dichloromethane / 5 h / 25 °C 2: sulfuric acid / ethanol / 25 °C View Scheme |
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