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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

N-[6-(4-Phenylbutoxy)hexyl]-benzenemethanamine

Cas:97664-55-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 97664-55-6 6-Benzylamino-1-(4'-phenylbutoxy)hexane Manufacturer

Cas:97664-55-6

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N-[6-(4-Phenylbutoxy)-hexyl]-benzenemethanamine

Cas:97664-55-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Kilogram

FOB Price: $2.0 / 10.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Henan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com

TIANFU-CHEM - 6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Gram

FOB Price: $1000.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top PurityCAS 97664-55-6 with fast shipping

Cas:97664-55-6

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane CAS:97664-55-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane CAS:97664-55-6

Cas:97664-55-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

N-[6-(4-Phenylbutoxy)hexyl]-benzenemethanamine

Cas:97664-55-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzenemethanamine, N-[6-(4-phenylbutoxy)hexyl]-

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

BENZENEMETHANAMINE,N-[6-(4-PHENYLBUTOXY)HEXYL]-

Cas:97664-55-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

N-[6-(4-Phenylbutoxy)hexyl]-benzenemethanamine

Cas:97664-55-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

6-Benzylamino-1-(4'-phenylbutoxy)hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Senova Technology Company Limited

Good price, high purity, mature production technology, in stock, accept custom synthesis per customer's requirements Storage:in stock Package:As per Customer‘ requirements Application:Pharmaceutical API

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:1 Gram

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

N-[6-(4-Phenylbutoxy)hexyl]-benzenemethanamine

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Benzenemethanamine,N-[6-(4-phenylbutoxy)hexyl]-

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Other

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Manufacturers

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Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

Benzenemethanamine,N-[6-(4-phenylbutoxy)hexyl]

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Nanjing HuaNuo Bio-Pharmacuetical Co.,Ltd

Independent research and development of impurities, familiar with the market and impurity characteristics; We can ship out on the same day if the products are in stock; Focus on impurity development of new products in the market; Expert in customizi

Salmeterol Impurity 3

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Benzenemethanamine, N-[6-(4-phenylbutoxy)hexyl]-

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as

6-Benzylamino-1-(4'-phenylbutoxy)hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

6-N-Benzylamino-1-(4'-phenylbutoxy)HexaneAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

6-N-Benzylamino-1-(4'-phenylbutoxy)Hexane

Cas:97664-55-6

Min.Order:0

Negotiable

Type:Other

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Synthetic route

6-bromohexyl 4-phenylbutyl ether
94749-73-2

6-bromohexyl 4-phenylbutyl ether

benzylamine
100-46-9

benzylamine

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Stage #1: benzylamine With triethylamine; potassium iodide In acetonitrile at 45℃;
Stage #2: 6-bromohexyl 4-phenylbutyl ether In acetonitrile
76%
With triethylamine; sodium iodide75%
With triethylamine; sodium iodide In dimethyl sulfoxide for 17h; Ambient temperature;70%
With caesium carbonate In N,N-dimethyl-formamide at 60 - 80℃; for 5h;38%
benzaldehyde
100-52-7

benzaldehyde

D 2543
97664-58-9

D 2543

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
With sodium tetrahydroborate; molecular sieve 2.) ethanol; Yield given. Multistep reaction;
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C
2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C
View Scheme
Multi-step reaction with 4 steps
1: 60 percent
2: NaN3 / dimethylformamide
3: lithium aluminum hydride
4: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol
View Scheme
Multi-step reaction with 2 steps
1: potassium hydroxide; tetrabutylammomium bromide / toluene / 10 h / 20 °C
2: triethylamine; potassium iodide / acetonitrile / 45 °C
View Scheme
4-phenyl-butan-1-ol
3360-41-6

4-phenyl-butan-1-ol

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C
2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C
View Scheme
Multi-step reaction with 2 steps
1: 81 percent / NaH / tetrahydrofuran / 7 h / Ambient temperature
2: 70 percent / Et3N, NaI / dimethylsulfoxide / 17 h / Ambient temperature
View Scheme
Multi-step reaction with 4 steps
1: 60 percent
2: NaN3 / dimethylformamide
3: lithium aluminum hydride
4: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol
View Scheme
Multi-step reaction with 2 steps
1: potassium hydroxide; tetrabutylammomium bromide / toluene / 10 h / 20 °C
2: triethylamine; potassium iodide / acetonitrile / 45 °C
View Scheme
Multi-step reaction with 3 steps
1.1: sodium hydroxide / 2 h / 60 °C
1.2: 4 h / 110 °C
2.1: triethylamine / toluene / 5 h / 5 - 10 °C
3.1: sodium hydroxide / toluene / 12 h / 110 °C
View Scheme
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

sodium-compound of (+-)-cyclopenten-(2)-yl-malonic acid diethyl ester

sodium-compound of (+-)-cyclopenten-(2)-yl-malonic acid diethyl ester

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 81 percent / NaH / tetrahydrofuran / 7 h / Ambient temperature
2: 70 percent / Et3N, NaI / dimethylsulfoxide / 17 h / Ambient temperature
View Scheme
6-bromohexyl 4-phenylbutyl ether
94749-73-2

6-bromohexyl 4-phenylbutyl ether

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaN3 / dimethylformamide
2: lithium aluminum hydride
3: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol
View Scheme
1-azido-6-(4-phenylbutoxy)hexane
168412-89-3

1-azido-6-(4-phenylbutoxy)hexane

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium aluminum hydride
2: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol
View Scheme
N-[6-(4-phenylbutoxy)hexyl] benzenemethanamine hydrochloride

N-[6-(4-phenylbutoxy)hexyl] benzenemethanamine hydrochloride

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
With sodium carbonate In dichloromethane; water at 25 - 30℃; for 0.5h; pH=~ 8;
6-(4-phenylbutyloxy)hexyl methanesulfonate
135235-81-3

6-(4-phenylbutyloxy)hexyl methanesulfonate

benzylamine
100-46-9

benzylamine

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
With sodium hydroxide In toluene at 110℃; for 12h;
1,6-hexanediol
629-11-8

1,6-hexanediol

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide / 2 h / 60 °C
1.2: 4 h / 110 °C
2.1: triethylamine / toluene / 5 h / 5 - 10 °C
3.1: sodium hydroxide / toluene / 12 h / 110 °C
View Scheme
6-(4-phenyl-butoxy)-hexan-1-ol
97664-53-4

6-(4-phenyl-butoxy)-hexan-1-ol

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / toluene / 5 h / 5 - 10 °C
2: sodium hydroxide / toluene / 12 h / 110 °C
View Scheme
3-carbomethoxy-4-hydroxy-α-bromoacetophenone
36256-45-8

3-carbomethoxy-4-hydroxy-α-bromoacetophenone

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

5-(2-{Benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-acetyl)-2-hydroxy-benzoic acid methyl ester
497063-91-9

5-(2-{Benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-acetyl)-2-hydroxy-benzoic acid methyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 60℃;100%
With triethylamine In acetonitrile at 20℃; for 0.666667h; Inert atmosphere;
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

D 2543
97664-58-9

D 2543

Conditions
ConditionsYield
With hydrogen; 5%-palladium/activated carbon In ethanol at 20℃; under 760.051 Torr;97.9%
3'-acetoxymethyl-4'-acetoxy-2-bromoacetophenone
24085-07-2

3'-acetoxymethyl-4'-acetoxy-2-bromoacetophenone

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

C36H45NO6

C36H45NO6

Conditions
ConditionsYield
With potassium carbonate In dichloromethane at 25℃; for 5h; Reagent/catalyst; Solvent;95%
With potassium carbonate at 20℃; for 4h;
(R)-2,2-dimethyl-6-(oxiran-2-yl)-4H-benzo[d][1,3]dioxine
1067185-91-4

(R)-2,2-dimethyl-6-(oxiran-2-yl)-4H-benzo[d][1,3]dioxine

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

(R)-2-(benzyl(6-(4-phenylbutoxy)hexyl)amino)-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanol
1067185-92-5

(R)-2-(benzyl(6-(4-phenylbutoxy)hexyl)amino)-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanol

Conditions
ConditionsYield
With triethylamine at 120℃; for 12h;83%
5-(2-bromoacetyl)-2-hydroxybenzaldehyde
115787-50-3

5-(2-bromoacetyl)-2-hydroxybenzaldehyde

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

2-hydroxy-5-<<<6,6-(4-phenylbutoxy)hexylbenzyl>amino>acetyl>benzaldehyde
163923-19-1

2-hydroxy-5-<<<6,6-(4-phenylbutoxy)hexylbenzyl>amino>acetyl>benzaldehyde

Conditions
ConditionsYield
In acetonitrile for 1h; Heating; other solvent;71%
With N-ethyl-N,N-diisopropylamine In butanone at 0 - 10℃; for 11.5h;
With N-ethyl-N,N-diisopropylamine In butanone at 0 - 10℃;
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

2-benzyloxy-5-(R)-oxiranylbenzoic acid methyl ester
94749-70-9

2-benzyloxy-5-(R)-oxiranylbenzoic acid methyl ester

2-Benzyloxy-5-((R)-2-{benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-1-hydroxy-ethyl)-benzoic acid methyl ester
160889-19-0

2-Benzyloxy-5-((R)-2-{benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-1-hydroxy-ethyl)-benzoic acid methyl ester

Conditions
ConditionsYield
In tetrahydrofuran Heating;60%
Bromoacetaldehyde diethyl acetal
2032-35-1

Bromoacetaldehyde diethyl acetal

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

N-benzyl-N-diethyloxyethyl-6-(4-phenylbutoxy)hexylamine

N-benzyl-N-diethyloxyethyl-6-(4-phenylbutoxy)hexylamine

Conditions
ConditionsYield
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 80℃; for 22h;51%
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

2-Benzyloxy-5-(S)-oxiranyl-benzoic acid methyl ester

2-Benzyloxy-5-(S)-oxiranyl-benzoic acid methyl ester

2-Benzyloxy-5-((S)-2-{benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-1-hydroxy-ethyl)-benzoic acid methyl ester

2-Benzyloxy-5-((S)-2-{benzyl-[6-(4-phenyl-butoxy)-hexyl]-amino}-1-hydroxy-ethyl)-benzoic acid methyl ester

Conditions
ConditionsYield
In tetrahydrofuran Heating;
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

methyl 4-([1-13C]-α-bromoacetyl)salicylate
261381-22-0

methyl 4-([1-13C]-α-bromoacetyl)salicylate

C32(13)CH41NO5
261381-23-1

C32(13)CH41NO5

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran for 5h; Alkylation; Heating;
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 60℃;
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

C24(13)CH34(2)H3NO4

C24(13)CH34(2)H3NO4

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: i-Pr2EtN / tetrahydrofuran / 60 °C
2: LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
3: H2 / 10 percent Pd/C / ethanol / 4 h / 760 Torr
View Scheme
Multi-step reaction with 3 steps
1: diisopropylethylamine / tetrahydrofuran / 5 h / Heating
2: 146 mg / LiAlD4 / diethyl ether / 2.5 h / Heating
3: 71 percent / H2 / Pd/C / ethanol / 3 h / 20 °C / 760 Torr
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

C31(13)CH40(2)H3NO4
1025930-27-1

C31(13)CH40(2)H3NO4

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: i-Pr2EtN / tetrahydrofuran / 60 °C
2: LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: diisopropylethylamine / tetrahydrofuran / 5 h / Heating
2: 146 mg / LiAlD4 / diethyl ether / 2.5 h / Heating
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

C25H34(2)H3NO4

C25H34(2)H3NO4

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C
2: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
3: 77 percent / H2 / 10 percent Pd/C / ethanol / 4 h / 760 Torr
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

C32H40(2)H3NO4
497063-93-1

C32H40(2)H3NO4

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C
2: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

salmeterol
89365-50-4

salmeterol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 71 percent / acetonitrile / 1 h / Heating; other solvent
2: NaBH4 / methanol / 36 h / Ambient temperature
3: 0.21 g / H2 / Pd/C / methanol / 10 h
View Scheme
Multi-step reaction with 3 steps
1: hydrogenchloride / 10 h / Cooling with ice
2: sodium tetrahydroborate / 8 h / 20 °C
3: palladium 10% on activated carbon / ethanol / 36 h / 45 °C
View Scheme
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / butanone / 0 - 10 °C
2: methanol; sodium tetrahydroborate / 8 h / -5 - 30 °C / Inert atmosphere
3: palladium on carbon; hydrogen / methanol / 1.17 h / 25 °C / 413.73 - 517.16 Torr
View Scheme
Multi-step reaction with 4 steps
1: triethylamine / acetonitrile / 0.67 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere
3: palladium 10% on activated carbon / methanol / 2 h / Inert atmosphere
4: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C / Inert atmosphere
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

4-hydroxy-1-[[[6-(4-phenylbutoxy)hexyl](phenylmethyl)amino]methyl]-1,3-benzenedimethanol
934842-69-0

4-hydroxy-1-[[[6-(4-phenylbutoxy)hexyl](phenylmethyl)amino]methyl]-1,3-benzenedimethanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 71 percent / acetonitrile / 1 h / Heating; other solvent
2: NaBH4 / methanol / 36 h / Ambient temperature
View Scheme
Multi-step reaction with 2 steps
1: hydrogenchloride / 10 h / Cooling with ice
2: sodium tetrahydroborate / 8 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / butanone / 0 - 10 °C
2: methanol; sodium tetrahydroborate / 8 h / -5 - 30 °C / Inert atmosphere
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

(S)-Salmeterol

(S)-Salmeterol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran / Heating
2: 1.) LiAlH4; 2.) H2 / 2.) Pd-C / 1.) THF
View Scheme
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

(R)-(-)-salmeterol

(R)-(-)-salmeterol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 60 percent / tetrahydrofuran / Heating
2: 1.) LiAlH4; 2.) H2 / 2.) Pd-C / 1.) THF
View Scheme
Multi-step reaction with 4 steps
1: potassium carbonate / dichloromethane / 5 h / 25 °C
2: sulfuric acid / ethanol / 25 °C
3: (R)-diphenylprolinol; borane-THF / toluene / Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 45 °C
View Scheme
8-(benzyloxy)-5-[(1R)-2-bromo-1-(tetrahydro-2H-pyran-2-yloxy)ethyl]quinolin-2(1H)-one
662111-14-0

8-(benzyloxy)-5-[(1R)-2-bromo-1-(tetrahydro-2H-pyran-2-yloxy)ethyl]quinolin-2(1H)-one

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

8-(benzyloxy)-5-[(1R)-2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-(tetrahydro-2H-pyran-2-yloxy)ethyl]quinolin-2(1H)-one

8-(benzyloxy)-5-[(1R)-2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-(tetrahydro-2H-pyran-2-yloxy)ethyl]quinolin-2(1H)-one

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine at 120℃; for 4h;
5-benzyloxy-8-(2,2-dihydroxyacetyl)-4H-benzo[1,4]oxazin-3-one
662111-25-3

5-benzyloxy-8-(2,2-dihydroxyacetyl)-4H-benzo[1,4]oxazin-3-one

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

A

5-(benzyloxy)-8-(2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-hydroxyethyl)-2H-1,4-benzoxazin-3(4H)-one

5-(benzyloxy)-8-(2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-hydroxyethyl)-2H-1,4-benzoxazin-3(4H)-one

B

5-(benzyloxy)-8-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-2H-1,4-benzoxazin-3 (4H)-one
662111-26-4

5-(benzyloxy)-8-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-2H-1,4-benzoxazin-3 (4H)-one

Conditions
ConditionsYield
Stage #1: 5-benzyloxy-8-(2,2-dihydroxyacetyl)-4H-benzo[1,4]oxazin-3-one; N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine With acetic acid In dichloromethane for 4h;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 72h;
Stage #3: With sodium tetrahydroborate In methanol; dichloromethane for 2h;
4-(benzyloxy)-7-{(1R)-2-bromo-1-[tetrahydro-2H-pyran-2-yloxy]ethyl}-1,3-benzothiazol-2(3H)-one
662111-37-7

4-(benzyloxy)-7-{(1R)-2-bromo-1-[tetrahydro-2H-pyran-2-yloxy]ethyl}-1,3-benzothiazol-2(3H)-one

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

4-(benzyloxy)-7-{(1R)-2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-[tetrahydro-2H-pyran-2-yloxy]ethyl}-1.3-benzothiazol-2(3H)-one

4-(benzyloxy)-7-{(1R)-2-{benzyl[6-(4-phenylbutoxy)hexyl]amino}-1-[tetrahydro-2H-pyran-2-yloxy]ethyl}-1.3-benzothiazol-2(3H)-one

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine at 120℃; for 18h;
benzyl 7-(bromoacetyl)-2-oxo-2,3-dihydro-1,3-benzothiazol-4-yl carbonate
662111-43-5

benzyl 7-(bromoacetyl)-2-oxo-2,3-dihydro-1,3-benzothiazol-4-yl carbonate

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

7-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-4-hydroxy-1,3-benzothiazol-2(3H)-one
662111-44-6

7-({benzyl[6-(4-phenylbutoxy)hexyl]amino}acetyl)-4-hydroxy-1,3-benzothiazol-2(3H)-one

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 40℃; for 2h; Acidic aqueous solution;
N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine
97664-55-6

N-[6-(4-phenylbutoxy)hexyl]benzenemethanamine

4-hydroxy-α'-[[[6-(4-phenylbutoxy)hexyl]benzylamino]methyl]-1,3-benzenedirmethanol

4-hydroxy-α'-[[[6-(4-phenylbutoxy)hexyl]benzylamino]methyl]-1,3-benzenedirmethanol

Conditions
ConditionsYield
With hydrogenchloride for 10h; Cooling with ice;
Multi-step reaction with 2 steps
1: potassium carbonate / dichloromethane / 5 h / 25 °C
2: sulfuric acid / ethanol / 25 °C
View Scheme

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