Product Name

  • Name

    2-Ethylhexylamine

  • EINECS 203-233-8
  • CAS No. 104-75-6
  • Article Data16
  • CAS DataBase
  • Density 0.7894 g/cm3
  • Solubility 2.5 g/L (20 ºC)
  • Melting Point -76 °C
  • Formula C8H19N
  • Boiling Point 167.3 °C at 760 mmHg
  • Molecular Weight 129.246
  • Flash Point 52.2 °C
  • Transport Information UN 2276 3/PG 3
  • Appearance colourless liquid
  • Safety 26-36/37/39-45-16
  • Risk Codes 10-21/22-23-34
  • Molecular Structure Molecular Structure of 104-75-6 (2-Ethylhexylamine)
  • Hazard Symbols ToxicT
  • Synonyms b-Ethylhexylamine;Hexylamine,2-ethyl- (6CI,8CI);1-Amino-2-ethylhexane;2-Ethyl-1-aminohexane;2-Ethyl-1-hexanamine;2-Ethyl-1-hexylamine;
  • PSA 26.02000
  • LogP 2.86180

Synthetic route

2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

Conditions
ConditionsYield
With sodium azide; triphenylphosphine In dichloromethane; N,N-dimethyl-formamide at 90℃; for 5h; Substitution; Mitsunobu reaction; Staudinger reaction;92%
With Ru(CO)ClH(oxydi-2,1-phenylene)bis(diphenylphosphine)(triphenylphosphine); ammonia In toluene at 170℃; for 48h; Autoclave; Glovebox; Inert atmosphere;77 %Spectr.
2-ethylhexenal
645-62-5

2-ethylhexenal

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

Conditions
ConditionsYield
With ammonia; hydrogen; nickel at 140℃;
2-ethyl-N-(2-ethylhexyl)-1-hexanamine
106-20-7

2-ethyl-N-(2-ethylhexyl)-1-hexanamine

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

Conditions
ConditionsYield
With 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); ammonia; water In tert-Amyl alcohol; tert-butyl methyl ether at 170℃; for 16h; pressure tube; Inert atmosphere;70 %Chromat.
2-ethyl-hexanal oxime
34612-83-4

2-ethyl-hexanal oxime

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

Conditions
ConditionsYield
Stage #1: 2-ethyl-hexanal oxime With hydrogenchloride; zinc In ethanol; water at 20℃; for 0.25h;
Stage #2: With ammonia; sodium hydroxide In ethanol; water at 20℃; for 0.25h;		5.513 g
d,l-2-ethylhexanal
123-05-7

d,l-2-ethylhexanal

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: hydroxylamine hydrochloride / ethanol / 0.67 h / 20 °C
2.1: hydrogenchloride; zinc / ethanol; water / 0.25 h / 20 °C
2.2: 0.25 h / 20 °C
View Scheme
2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

A

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

B

2-ethyl-N-(2-ethylhexyl)-1-hexanamine
106-20-7

2-ethyl-N-(2-ethylhexyl)-1-hexanamine

Conditions
ConditionsYield
With chlorocyclopentadienylbis(triphenylphosphine)ruthenium(II); urea; diphenylphosphinopropane In diethylene glycol dimethyl ether at 160℃; for 12h; Autoclave; Inert atmosphere;
maleic anhydride
108-31-6

maleic anhydride

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

N-(2-ethylhexyl)maleimide
48149-71-9

N-(2-ethylhexyl)maleimide

Conditions
ConditionsYield
Stage #1: maleic anhydride; 2-Ethylhexylamine In toluene at 80℃;
Stage #2: With 1,1,1,3,3,3-hexamethyl-disilazane; zinc dibromide In toluene at 80℃; for 2.5h;		100%
With chloroform Erwaermen des Reaktionsprodukts mit Natriumacetat und Acetanhydrid;
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

N-(2-ethyl-hexyl)-methanesulfonamide
362665-05-2

N-(2-ethyl-hexyl)-methanesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 1h;100%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

2,9-bis(2-ethylhexyl)anthra[2,1,9-def:6,5,10-d',e',f']diisoquinoline-1,3,8,10(2H,9H)-tetraone
82531-03-1

2,9-bis(2-ethylhexyl)anthra[2,1,9-def:6,5,10-d',e',f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Conditions
ConditionsYield
With 1H-imidazole; zinc diacetate at 160℃; for 5h; Inert atmosphere;99%
With 1H-imidazole98%
In N,N-dimethyl-formamide for 8h; Inert atmosphere; Reflux;97%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-tert-butylphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-tert-butylphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

N-(2,6-diisopropylphenyl)-N′-(2-ethyl-1hexyl)-1,6-dichloro-7,12-di(4-tert-butylphenoxy)perylene-3,4,9,10-tetracarboxy bisimide

N-(2,6-diisopropylphenyl)-N′-(2-ethyl-1hexyl)-1,6-dichloro-7,12-di(4-tert-butylphenoxy)perylene-3,4,9,10-tetracarboxy bisimide

Conditions
ConditionsYield
In toluene for 16h; Reflux;99%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

diglycolyl chloride
21062-20-4

diglycolyl chloride

2,2’-oxybis(N-(2-ethylhexyl)acetamide)

2,2’-oxybis(N-(2-ethylhexyl)acetamide)

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 1h;99%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

N-butyl-N-(chloro(dibutylamino)methylene)butan-1-aminium chloride
81363-13-5

N-butyl-N-(chloro(dibutylamino)methylene)butan-1-aminium chloride

N,N,N',N'-tetra-(n-butyl)-N''-(2-ethylhexyl)guanidine
1283075-93-3

N,N,N',N'-tetra-(n-butyl)-N''-(2-ethylhexyl)guanidine

Conditions
ConditionsYield
With triethylamine In acetonitrile98%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

4-bromo-1,8-naphthalenedicarboxylic anhydride
81-86-7

4-bromo-1,8-naphthalenedicarboxylic anhydride

6-bromo-2-(2-ethylhexyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione
1193092-32-8

6-bromo-2-(2-ethylhexyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Conditions
ConditionsYield
In ethanol for 24h; Reflux;98%
In ethanol at 110℃; Inert atmosphere;95.01%
In ethanol for 4h; Reflux;85%
carbon disulfide
75-15-0

carbon disulfide

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

2-ethyl-1-hexyl isothiocyanate
21663-56-9

2-ethyl-1-hexyl isothiocyanate

Conditions
ConditionsYield
Stage #1: carbon disulfide; 2-Ethylhexylamine With potassium carbonate In water at 20℃; for 1h; Inert atmosphere;
Stage #2: With 1,3,5-trichloro-2,4,6-triazine In dichloromethane; water at 0℃; for 0.5h; Inert atmosphere;
Stage #3: With sodium hydroxide In dichloromethane; water pH=11; Inert atmosphere;		98%
With dicyclohexyl-carbodiimide In dichloromethane at -10 - 20℃; for 18h; Inert atmosphere;81%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

3-phenyl-1-(2-thioxobenzo[d]oxazol-3(2H)-yl)propan-1-one
312313-34-1

3-phenyl-1-(2-thioxobenzo[d]oxazol-3(2H)-yl)propan-1-one

N-(2-ethylhexyl)-3-phenylpropanamide
551910-81-7

N-(2-ethylhexyl)-3-phenylpropanamide

Conditions
ConditionsYield
With triethylamine; benzoic acid In 1-methyl-pyrrolidin-2-one at 20℃; for 1h;98%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

5-chloro-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde
87867-73-0

5-chloro-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde

5-((2-ethylhexyl)amino)-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde

5-((2-ethylhexyl)amino)-3-methyl-1-(pyridin-2-yl)-1H-pyrazole-4-carbaldehyde

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; chemoselective reaction;98%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

C15H13ClN4O4S

C15H13ClN4O4S

C23H31N5O4S

C23H31N5O4S

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane at 25℃; for 1.25h;98%
With triethylamine In chloroform at 20℃; for 0.166667h; Cooling with ice;28.4 g
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-methoxyphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-methoxyphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-methoxyphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

N-(2,6-diisopropylphenyl)-1,6-dichloro-7,12-di-(4-methoxyphenoxy)perylene-3,4,9,10-tetracarboxy monoimide monoanhydride

Conditions
ConditionsYield
In toluene for 16h; Reflux;98%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-Chloro-N-(2-ethyl-hexyl)-acetamide
32461-85-1

2-Chloro-N-(2-ethyl-hexyl)-acetamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane for 0.25h;97%
With TEA In dichloromethane at 20℃; for 3h;
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

2,3-diacetyl succinic acid dimethyl ester
74536-45-1

2,3-diacetyl succinic acid dimethyl ester

1-(2-Ethyl-hexyl)-2,5-dimethyl-1H-pyrrole-3,4-dicarboxylic acid dimethyl ester
181262-97-5

1-(2-Ethyl-hexyl)-2,5-dimethyl-1H-pyrrole-3,4-dicarboxylic acid dimethyl ester

Conditions
ConditionsYield
With acetic acid for 24h; Ambient temperature;97%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

epichlorohydrin
106-89-8

epichlorohydrin

3,3'-(2-ethylhexylazanediyl)bis(1-chloropropan-2-ol)

3,3'-(2-ethylhexylazanediyl)bis(1-chloropropan-2-ol)

Conditions
ConditionsYield
In methanol at 20℃; for 12h;97%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

2,3,4,2',3',4',6'-hepta-O-benzoyl-6-O-trifluoromethylsulfonyl-α,α-trehalose

2,3,4,2',3',4',6'-hepta-O-benzoyl-6-O-trifluoromethylsulfonyl-α,α-trehalose

2,3,4,2',3',4',6'-hepta-O-benzoyl-6-O-deoxy-6-[(2-ethylhexyl)amino]-α,α-trehalose

2,3,4,2',3',4',6'-hepta-O-benzoyl-6-O-deoxy-6-[(2-ethylhexyl)amino]-α,α-trehalose

Conditions
ConditionsYield
In dichloromethane at 20℃; for 20h;96%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

isatoic anhydride
118-48-9

isatoic anhydride

N-(2-ethylhexyl)-2-aminobenzamide
556062-39-6

N-(2-ethylhexyl)-2-aminobenzamide

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide; toluene96%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

1H,3H-thieno[3,4-c]furan-1,3-dione
6007-85-8

1H,3H-thieno[3,4-c]furan-1,3-dione

5-(2-ethylhexyl)-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione
1231160-82-9

5-(2-ethylhexyl)-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Conditions
ConditionsYield
Stage #1: 2-Ethylhexylamine; 1H,3H-thieno[3,4-c]furan-1,3-dione In toluene at 140℃; for 24h; Inert atmosphere;
Stage #2: With thionyl chloride at 140℃; for 3h; Inert atmosphere;		96%
In acetic acid Inert atmosphere; Reflux; Schlenk technique;
Stage #1: 2-Ethylhexylamine; 1H,3H-thieno[3,4-c]furan-1,3-dione In toluene at 140℃; for 24h;
Stage #2: With thionyl chloride for 3h; Reflux;		6.20 g
Stage #1: 2-Ethylhexylamine; 1H,3H-thieno[3,4-c]furan-1,3-dione In toluene Reflux;
Stage #2: With thionyl chloride for 4h; Reflux;
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

[silver(I)(acetonitrile)](bis(trifluoromethanesulfonyl)imide)
1334406-90-4, 1357467-59-4

[silver(I)(acetonitrile)](bis(trifluoromethanesulfonyl)imide)

[Ag(2-EtHexAm)2][Tf2N]

[Ag(2-EtHexAm)2][Tf2N]

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h;96%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

3-methoxy-4-bromo-1,8-naphthalic anhydride

3-methoxy-4-bromo-1,8-naphthalic anhydride

N-(2-ethylhexyl)-3-methoxy-4-bromo-1,8-naphthalimide

N-(2-ethylhexyl)-3-methoxy-4-bromo-1,8-naphthalimide

Conditions
ConditionsYield
In ethanol for 4h; Reflux; Inert atmosphere;96%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

25,27-bis[(3-isothiocyanatopropyl)oxy]calix[4]arene-crown-6
252357-81-6

25,27-bis[(3-isothiocyanatopropyl)oxy]calix[4]arene-crown-6

25,27-bis[(3-(N'-(2-ethylhexyl)thioureido)propyl)oxy]calix[4]arene-crown-6

25,27-bis[(3-(N'-(2-ethylhexyl)thioureido)propyl)oxy]calix[4]arene-crown-6

Conditions
ConditionsYield
In dichloromethane at 20℃; for 10h; Addition;95%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

D,L-lactide
95-96-5

D,L-lactide

N-(2-ethyl-hexyl)-lactamide
100535-55-5

N-(2-ethyl-hexyl)-lactamide

Conditions
ConditionsYield
at 20℃; under 760.051 Torr; for 96h;95%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

N-(2-ethylhexyl)-4-methylbenzenesulfonamide

N-(2-ethylhexyl)-4-methylbenzenesulfonamide

Conditions
ConditionsYield
With pyridine at 0 - 20℃;95%
With triethylamine In dichloromethane at 0 - 20℃;
With triethylamine In dichloromethane at 0 - 25℃;
methanol
67-56-1

methanol

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

1,3-bis(2-ethylhexyl)urea

1,3-bis(2-ethylhexyl)urea

Conditions
ConditionsYield
With Ru-MACHO-BH In toluene at 140℃; for 24h; Autoclave; Inert atmosphere;95%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

(1R,2R,6S,7S)-4-oxa-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione
2746-19-2

(1R,2R,6S,7S)-4-oxa-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione

exo-N-2-ethylhexylnorbornene dicarboximide

exo-N-2-ethylhexylnorbornene dicarboximide

Conditions
ConditionsYield
In toluene at 115℃; for 17h;95%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

4-nitrophenyl azide
1516-60-5

4-nitrophenyl azide

1-(2-ethylhexyl)-5-methyl-1,2,3-triazole

1-(2-ethylhexyl)-5-methyl-1,2,3-triazole

Conditions
ConditionsYield
With acetic acid In toluene at 55℃; for 18h;95%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

cis-1,2,3,6-tetrahydrophthalic anhydride
935-79-5

cis-1,2,3,6-tetrahydrophthalic anhydride

2-(2-ethylhexyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

2-(2-ethylhexyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 24h; Molecular sieve; Reflux;94.9%
pyridine-4-carbaldehyde
872-85-5

pyridine-4-carbaldehyde

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

C14H22N2

C14H22N2

Conditions
ConditionsYield
With toluene-4-sulfonic acid In ethanol at 80℃; for 8h;94.5%
With toluene-4-sulfonic acid In ethanol for 8h; Reflux;94.5%
With toluene-4-sulfonic acid In ethanol at 80℃; for 8h;94.5%
2,2'-dithiodibenzoic acid dichloride
19602-82-5

2,2'-dithiodibenzoic acid dichloride

2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

2,2'-dithiobis
88848-47-9

2,2'-dithiobis

Conditions
ConditionsYield
In 1,4-dioxane for 2h; Ambient temperature;94.1%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

N,N,N′,N′-tetraethylchloroformamidinium chloride
70976-93-1

N,N,N′,N′-tetraethylchloroformamidinium chloride

N''-(2-ethylhexyl)-N,N,N',N'-tetraethylguanidine
1283075-91-1

N''-(2-ethylhexyl)-N,N,N',N'-tetraethylguanidine

Conditions
ConditionsYield
With triethylamine In acetonitrile94%

2-Ethylhexylamine Consensus Reports

Reported in EPA TSCA Inventory.

2-Ethylhexylamine Standards and Recommendations

DOT Classification:  8; Label: Corrosive

2-Ethylhexylamine Specification

The CAS registry number of 2-Ethyl hexylamine is 104-75-6. Its EINECS registry number is 203-233-8. The IUPAC name is 2-ethylhexan-1-amine. In addition, the molecular formula is C8H19N and the molecular weight is 129.24. It is also called 1-amino-2-ethylhexane. What's more, it is a kind of colourless liquid and belongs to the classes of Industrial/Fine Chemicals; Butoctamide; Amines; C8; Nitrogen Compounds. It should be stored in sealed container, and put them in a cool and dry place. 

Physical properties about this chemical are: (1)ACD/LogP: 2.87; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -0.23; (4)ACD/LogD (pH 7.4): -0.04; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 1; (8)ACD/KOC (pH 7.4): 1.08; (9)#H bond acceptors: 1; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 6; (12)Polar Surface Area: 3.24 Å2; (13)Index of Refraction: 1.43; (14)Molar Refractivity: 42.6 cm3; (15)Molar Volume: 164.6 cm3; (16)Polarizability: 16.89 ×10-24cm3; (17)Surface Tension: 27.4 dyne/cm; (18)Density: 0.784 g/cm3; (19)Flash Point: 52.2 °C; (20)Enthalpy of Vaporization: 40.38 kJ/mol; (21)Boiling Point: 167.3 °C at 760 mmHg; (22)Vapour Pressure: 1.71 mmHg at 25°C.

Preparation of 2-Ethyl hexylamine: it can be prepared by 2-ethyl-hexan-1-ol. This reaction is a kind of substitution//mitsunobu reaction. It will need reagents sodium azide and Ph3P, and solvents CH2Cl2 and dimethylformamide. The reaction time is 5 hours at reaction temperature of 90 °C. The yield is about 92%.

2-Ethyl hexylamine can be prepared by 2-ethyl-hexan-1-ol

Uses of 2-Ethyl hexylamine: it is used as raw materials for medicine, dyes, pesticides, sulfide accelerators, antioxidants, the flotation agents, emulsifiers, etc. In addition, it can be used to get 2-ethyl-hexanenitrile. This reaction will need reagent O2, catalyst RuHAP and solvent toluene. The reaction time is 24 hours at reaction temperature of 110 °C. The yield is about 99%.

2-Ethyl hexylamine can be used to get 2-ethyl-hexanenitrile

When you are using this chemical, please be cautious about it as the following:
This chemical is flammable and can cause burns. And it is harmful by inhalation, in contact with skin and if swallowed. During using it, wear suitable protective clothing, gloves and eye/face protection. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. And in case of accident or if you feel unwell, seek medical advice immediately (show label where possible). What's more, you should keep away from sources of ignition and no smoking.

You can still convert the following datas into molecular structure:
(1)SMILES: NCC(CC)CCCC
(2)InChI: InChI=1/C8H19N/c1-3-5-6-8(4-2)7-9/h8H,3-7,9H2,1-2H3
(3)InChIKey: LTHNHFOGQMKPOV-UHFFFAOYAF

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rabbit LD50 skin 600uL/kg (0.6mL/kg)   Union Carbide Data Sheet. Vol. 2/20/1963,
rat LCLo inhalation 125ppm/4H (125ppm)   Journal of Industrial Hygiene and Toxicology. Vol. 31, Pg. 343, 1949.
rat LD50 oral 450mg/kg (450mg/kg)   Union Carbide Data Sheet. Vol. 2/20/1963,

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