Product Name

  • Name

    D-Lysine hydrochloride

  • EINECS 230-691-6
  • CAS No. 7274-88-6
  • Article Data2
  • CAS DataBase
  • Density
  • Solubility Soluble in water
  • Melting Point 266 °C (dec.)(lit.)
  • Formula C6H15ClN2O2
  • Boiling Point 311.5 °C at 760 mmHg
  • Molecular Weight 182.65
  • Flash Point 142.2 °C
  • Transport Information
  • Appearance white crystalline powder
  • Safety 24/25
  • Risk Codes
  • Molecular Structure Molecular Structure of 7274-88-6 (D-Lysine hydrochloride)
  • Hazard Symbols
  • Synonyms D-Lysine,monohydrochloride (9CI);Lysine, monohydrochloride, D- (8CI);NSC 206291;H-D-Lys-OH.HCl;H-D-Lys-OH·HCl;
  • PSA 89.34000
  • LogP 1.72990

Synthetic route

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

2,2-dimethoxy-propane
77-76-9

2,2-dimethoxy-propane

D-lysine methyl ester bis-hydrochloride

D-lysine methyl ester bis-hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol at 20℃; for 15h; Reflux;95%
4-phenylazobenzoyl chloride
104-24-5

4-phenylazobenzoyl chloride

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

bis-D-lysine

bis-D-lysine

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane64%
2,5-dioxopyrrolidin-1-yl 6-(((tert-butyldimethylsilyl)oxy)methyl)nicotinate
1277191-84-0

2,5-dioxopyrrolidin-1-yl 6-(((tert-butyldimethylsilyl)oxy)methyl)nicotinate

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
82911-69-1

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-6-(6-(((tert-butyldimethylsilyl)oxy)methyl)nicotinamido)hexanoic acid
1277191-85-1

(R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-6-(6-(((tert-butyldimethylsilyl)oxy)methyl)nicotinamido)hexanoic acid

Conditions
ConditionsYield
Stage #1: D-lysine hydrochloride With copper(ll) sulfate pentahydrate; sodium hydrogencarbonate In water for 2h; Reflux;
Stage #2: 2,5-dioxopyrrolidin-1-yl 6-(((tert-butyldimethylsilyl)oxy)methyl)nicotinate In N,N-dimethyl-formamide at 0 - 20℃; for 16h;
Stage #3: N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide Further stages;		62%
...Expand
palmitic acid N-succinimide ester
14464-31-4

palmitic acid N-succinimide ester

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Pam-DLys(Pam)-OH
870789-29-0

Pam-DLys(Pam)-OH

Conditions
ConditionsYield
Stage #1: palmitic acid N-succinimide ester; D-lysine hydrochloride With sodium carbonate In 1,4-dioxane at 20℃; for 48h;
Stage #2: With hydrogenchloride In 1,4-dioxane; water		61%
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

acryloyl chloride
814-68-6

acryloyl chloride

(R)-6-acrylamido-2-aminohexanoic acid

(R)-6-acrylamido-2-aminohexanoic acid

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium carbonate; sodium hydroxide In water at 0 - 20℃; for 4h; Inert atmosphere;45.3%
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-3-amino-azepan-2-one
28957-33-7

(R)-3-amino-azepan-2-one

Conditions
ConditionsYield
With hexamethyldisilazan In toluene for 168h; Heating / reflux;15%
Stage #1: D-lysine hydrochloride With thionyl chloride In methanol at -60 - 20℃; for 12h;
Stage #2: With sodium methylate In methanol for 4h; Reflux;
Multi-step reaction with 2 steps
1: hydrogenchloride / 3 h / Reflux
2: sodium methylate / methanol / 4 h / Reflux
View Scheme
tert-butyl fluoroformate
18595-34-1

tert-butyl fluoroformate

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Nε-(tert-butoxycarbonyl)-D-lysine
31202-69-4

Nε-(tert-butoxycarbonyl)-D-lysine

Conditions
ConditionsYield
(i) CuCO3*Cu(OH)2, (ii) aq. NaOH, NaHCO3, dioxane; Multistep reaction;
2,2-dimethylpropanoic anhydride
1538-75-6

2,2-dimethylpropanoic anhydride

2-methyl-1-nitroisourea
57538-27-9

2-methyl-1-nitroisourea

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Nα-tert-butoxycarbonyl-NG-nitro-D-homoarginine
132718-70-8

Nα-tert-butoxycarbonyl-NG-nitro-D-homoarginine

Conditions
ConditionsYield
Yield given. Multistep reaction;
...Expand
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

benzyl chloroformate
501-53-1

benzyl chloroformate

(R)-2-amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid
34404-32-5, 1155-64-2, 32302-83-3

(R)-2-amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid

Conditions
ConditionsYield
With copper (II) carbonate hydroxide; sodium hydroxide 1.) H2O, reflux, 2.5 h, 2.) RT, overnight; Yield given. Multistep reaction;
acetic anhydride
108-24-7

acetic anhydride

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Nε-acetyl-lysine
51621-57-9

Nε-acetyl-lysine

Conditions
ConditionsYield
With TEA 1.) H2O, reflux, 30 min, 2.) H2O, MeOH, a) 0 deg C, 1.5 h, b) RT, 1 h; Yield given. Multistep reaction;
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

benzaldehyde
100-52-7

benzaldehyde

Nε-benzylidene-D-lysine

Nε-benzylidene-D-lysine

Conditions
ConditionsYield
With lithium hydroxide at 0℃;
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Nα-carbobenzoxy-D-lysine
70671-54-4

Nα-carbobenzoxy-D-lysine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-3-Benzyloxycarbonylamino-7-hydroxy-heptanoic acid methyl ester

(R)-3-Benzyloxycarbonylamino-7-hydroxy-heptanoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Acetic acid (R)-5-benzyloxycarbonylamino-7-diazo-6-oxo-heptyl ester

Acetic acid (R)-5-benzyloxycarbonylamino-7-diazo-6-oxo-heptyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-6-Acetoxy-2-benzyloxycarbonylamino-hexanoic acid

(R)-6-Acetoxy-2-benzyloxycarbonylamino-hexanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-7-Acetoxy-3-benzyloxycarbonylamino-heptanoic acid methyl ester

(R)-7-Acetoxy-3-benzyloxycarbonylamino-heptanoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(S)-2-[((2R,3R)-3-Benzyloxycarbonylamino-7-hydroxy-2-methyl-heptanoyl)-methyl-amino]-3-methyl-butyric acid methyl ester

(S)-2-[((2R,3R)-3-Benzyloxycarbonylamino-7-hydroxy-2-methyl-heptanoyl)-methyl-amino]-3-methyl-butyric acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 11 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
10.1: iPr2NEt; 1-hydroxy-7-azabenzotriazole; 2-bromo-1-ethylpyridinium tetrafluoroborate / CH2Cl2 / -25 - 20 °C
11.1: TFA / CH2Cl2 / 0 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-3-Benzyloxycarbonylamino-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid methyl ester

(R)-3-Benzyloxycarbonylamino-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid methyl ester
790302-28-2

(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid

(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoic acid

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(S)-2-{[(2R,3R)-3-((S)-2-tert-Butoxycarbonylamino-3-methyl-butyrylamino)-2-methyl-7-oxo-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester

(S)-2-{[(2R,3R)-3-((S)-2-tert-Butoxycarbonylamino-3-methyl-butyrylamino)-2-methyl-7-oxo-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 14 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
10.1: iPr2NEt; 1-hydroxy-7-azabenzotriazole; 2-bromo-1-ethylpyridinium tetrafluoroborate / CH2Cl2 / -25 - 20 °C
11.1: TFA / CH2Cl2 / 0 °C
12.1: aq. HCl; H2 / Pd/C / methanol / 20 °C
13.1: HOBt; EDCI; N-methylmorpholine / CH2Cl2 / 0 - 20 °C
14.1: DMSO; oxalyl chloride; iPr2NEt / CH2Cl2 / -78 - -55 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(S)-2-[((2R,3R)-3-Amino-7-hydroxy-2-methyl-heptanoyl)-methyl-amino]-3-methyl-butyric acid methyl ester; hydrochloride

(S)-2-[((2R,3R)-3-Amino-7-hydroxy-2-methyl-heptanoyl)-methyl-amino]-3-methyl-butyric acid methyl ester; hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 12 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
10.1: iPr2NEt; 1-hydroxy-7-azabenzotriazole; 2-bromo-1-ethylpyridinium tetrafluoroborate / CH2Cl2 / -25 - 20 °C
11.1: TFA / CH2Cl2 / 0 °C
12.1: aq. HCl; H2 / Pd/C / methanol / 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(S)-2-{[(2R,3R)-3-((S)-2-tert-Butoxycarbonylamino-3-methyl-butyrylamino)-7-hydroxy-2-methyl-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester
790302-31-7

(S)-2-{[(2R,3R)-3-((S)-2-tert-Butoxycarbonylamino-3-methyl-butyrylamino)-7-hydroxy-2-methyl-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 13 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
10.1: iPr2NEt; 1-hydroxy-7-azabenzotriazole; 2-bromo-1-ethylpyridinium tetrafluoroborate / CH2Cl2 / -25 - 20 °C
11.1: TFA / CH2Cl2 / 0 °C
12.1: aq. HCl; H2 / Pd/C / methanol / 20 °C
13.1: HOBt; EDCI; N-methylmorpholine / CH2Cl2 / 0 - 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(S)-2-{[(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester
790302-29-3

(S)-2-{[(2R,3R)-3-Benzyloxycarbonylamino-2-methyl-7-(2-trimethylsilanyl-ethoxymethoxy)-heptanoyl]-methyl-amino}-3-methyl-butyric acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 10 steps
1.1: aq. LiOH / 0 °C
2.1: aq. NaOH / ethanol / 0.33 h / -10 - 20 °C
2.2: HCl / ethanol / 0.17 h / 50 °C
3.1: NaNO2; AcOH / 6 h / 40 °C
4.1: Et3N; isobutyl chloroformate / tetrahydrofuran / 1 h / -25 - -10 °C
4.2: tetrahydrofuran; diethyl ether / -10 - 20 °C
5.1: PhCO2Ag; Et3N / -25 - 20 °C
6.1: K2CO3 / methanol / 6 h / 0 °C
7.1: iPr2NEt / CH2Cl2 / 5 h / 20 °C
8.1: LDA; LiCl / tetrahydrofuran / -78 °C
9.1: LiOH*H2O / tetrahydrofuran; methanol; H2O / 0 - 20 °C
10.1: iPr2NEt; 1-hydroxy-7-azabenzotriazole; 2-bromo-1-ethylpyridinium tetrafluoroborate / CH2Cl2 / -25 - 20 °C
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-6-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoic acid
55878-47-2

(R)-6-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) basic copper carbonate, 2.) NaOH / 1.) H2O, reflux, 2.5 h, 2.) RT, overnight
2: 91 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Boc-D-Lys-OH
106719-44-2

Boc-D-Lys-OH

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) basic copper carbonate, 2.) NaOH / 1.) H2O, reflux, 2.5 h, 2.) RT, overnight
2: 91 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature
3: H2 / 5percent Pd/C / methanol; H2O / 24 h / 2585.7 Torr
View Scheme
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

Nα-tert-butyloxycarbonyl-Nε-nicotinoyl-D-lysine
122546-52-5

Nα-tert-butyloxycarbonyl-Nε-nicotinoyl-D-lysine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 1.) basic copper carbonate, 2.) NaOH / 1.) H2O, reflux, 2.5 h, 2.) RT, overnight
2: 91 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature
3: H2 / 5percent Pd/C / methanol; H2O / 24 h / 2585.7 Torr
4: dimethylformamide / 120 h / Ambient temperature
View Scheme
(9H-fluoren-9-yl)methyl azidoformate
28920-44-7

(9H-fluoren-9-yl)methyl azidoformate

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

N,N'-bis-(9-fluorenylmethyloxycarbonyl)-D-lysine
75932-02-4

N,N'-bis-(9-fluorenylmethyloxycarbonyl)-D-lysine

Conditions
ConditionsYield
In hexane; water; sodium carbonate; acetone
benzyl bromide
100-39-0

benzyl bromide

D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

(R)-benzyl 2,6-bis(dibenzylamino)hexanoate

(R)-benzyl 2,6-bis(dibenzylamino)hexanoate

Conditions
ConditionsYield
Stage #1: benzyl bromide; D-lysine hydrochloride With potassium carbonate In ethanol at 60℃; for 96h;
Stage #2: In ethanol
D-lysine hydrochloride
7274-88-6

D-lysine hydrochloride

C26H30F6N2O5

C26H30F6N2O5

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / water / 20 - 30 °C
1.2: 120 °C / 36228.6 Torr / Autoclave; Sealed tube
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane-d2 / 2 h / 20 °C
View Scheme

D-Lysine, hydrochloride (1:1) Chemical Properties

Product Name: D-Lysine hydrochloride (CAS NO.7274-88-6)

Molecular Formula: C6H15ClN2O2
Molecular Weight: 182.648500 g/mol
Appearance: brown power
Melting Point: 266 °C (dec.)(lit.)
Solubility: soluble
Alpha: -21 °(c=8, 6N HCl)
Storage temp.: Store at RT.
BRN: 4356907
Flash Point: 142.2 °C 
Enthalpy of Vaporization: 60.75 kJ/mol 
Boiling Point: 311.5 °C at 760 mmHg 
Vapour Pressure: 0.000123 mmHg at 25°C 
H-Bond Donor: 4
H-Bond Acceptor: 4
Structure Descriptors of D-Lysine hydrochloride (CAS NO.7274-88-6):
  IUPAC Name: 2,6-diaminohexanoic acid hydrochloride
  Canonical SMILES: C(CCN)CC(C(=O)O)N.Cl
  InChI: InChI=1S/C6H14N2O2.ClH/c7-4-2-1-3-5(8)6(9)10;/h5H,1-4,7-8H2,(H,9,10);1H 
  InChIKey: BVHLGVCQOALMSV-UHFFFAOYSA-N
Categories: Lysine [Lys, K]; Amino Acids and Derivatives; alpha-Amino Acids; Amino Acids; Biochemistry; Amino hydrochloride

D-Lysine, hydrochloride (1:1) Uses

 D-Lysine hydrochloride (CAS NO.7274-88-6) is a kind of hormones which is used to adjust endocrine.

D-Lysine, hydrochloride (1:1) Toxicity Data With Reference

1.    

ipr-rat LD50:4750 mg/kg ABBIA4 64,319,56

D-Lysine, hydrochloride (1:1) Consensus Reports

Reported in EPA TSCA Inventory.

D-Lysine, hydrochloride (1:1) Safety Profile

Safety Information of D-Lysine hydrochloride (CAS NO.7274-88-6):
Safety Statements:24/25
24/25:Avoid contact with skin and eyes  
WGK Germany:3
RTECS:OL5632500
F:21
When heated to decomposition it emits very toxic fumes of HCl and NOx.

D-Lysine, hydrochloride (1:1) Specification

 D-Lysine hydrochloride , its CAS NO. is 7274-88-6, the synonyms are D-Lysine, monohydrochloride ; Lysine, hydrochloride, D- ; Lysine, monohydrochloride, D- .

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