Conditions | Yield |
---|---|
Stage #1: stearamide With titanium(IV) isopropylate In toluene at 20 - 100℃; Stage #2: With hydrogenchloride In diethyl ether; toluene | 90% |
Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride In water; butan-1-ol at 60℃; | |
With hydrogenchloride In methanol; water |
Conditions | Yield |
---|---|
Stage #1: stearonitrile With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); {[(phenylphosphinediyl)bis(2,1-phenylene)]bis(methylene)}bis(di-tert-butylphosphine); hydrogen In isopropyl alcohol at 50℃; under 11251.1 Torr; for 17h; Inert atmosphere; Autoclave; Stage #2: With hydrogenchloride In methanol; water at 20℃; for 0.5h; |
octadecylamine hydrochloride
1-(4-dodecyloxyphenyl)-3-octadecylamino-2-propen-1-one
Conditions | Yield |
---|---|
In ethanol for 0.0833333h; Heating; | 95% |
octadecylamine hydrochloride
Conditions | Yield |
---|---|
In ethanol; water byproducts: NaCl; dissolving of C18H37NH3Cl in EtOH:H2O (1:5) mixt. with stirring at 50°C; dissolving of Na4Ge4S10 in H2O, filtration, addn. of filtrate tosoln. of C18H37NH3Cl, pptn., stirring at 60°C for 2 h; cooling, filtration, washing with EtOH:H2O mixt. and finally with ether,drying under vac. at room temp. overnight; elem. anal.; | 90% |
sodium tetrahydroborate
octadecylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogen In Triethylene glycol dimethyl ether at 150 - 180℃; for 2h; | 71% |
4-oxo-2,2,6,6-tetramethylpiperidin-oxyl
octadecylamine hydrochloride
C27H55N2O
Conditions | Yield |
---|---|
With sodium cyanoborohydride In methanol | 68% |
octadecylamine hydrochloride
Conditions | Yield |
---|---|
With N,N'-dicyclohexylcarbodiimide In acetonitrile byproducts: DCU, H2, (C4H9)4NCl; refluxed; | 53% |
formaldehyd
octadecylamine hydrochloride
5',6',7',8'-tetrahydro-1'H-spiro[cyclohexane-1,2'-quinazolin]-4'(3'H)-one
Conditions | Yield |
---|---|
Stage #1: formaldehyd; octadecylamine hydrochloride; 5',6',7',8'-tetrahydro-1'H-spiro[cyclohexane-1,2'-quinazolin]-4'(3'H)-one In methanol; water Mannich Aminomethylation; Reflux; Stage #2: With ammonium hydroxide | 46% |
octadecylamine hydrochloride
Conditions | Yield |
---|---|
With N,N'-cyclohexylcarbodiimide In acetonitrile byproducts: N,N'-dicyclohexylurea; soln. of (Bu4N)4(α-Mo8O26), DCC and alkylamine hydrochloride in MeCN heated at 40°C for 120 h; soln. filtered, filtrate allowed to evap., residue recrystd. with acetone; elem. anal.; | 40% |
Conditions | Yield |
---|---|
With formaldehyd |
furfural
octadecylamine hydrochloride
1-aminooctadecane
3-hydroxy-1-octadecyl-pyridinium; chloride
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With chlorobenzene | |
With xylene | |
With toluene | |
With chlorobenzene |
Conditions | Yield |
---|---|
With formic acid |
Conditions | Yield |
---|---|
With toluene Erhitzen; | |
With triethylamine In chloroform |
octadecylamine hydrochloride
N-Cyanoguanidine
1-octadecyl-biguanide
Conditions | Yield |
---|---|
at 120 - 150℃; |
octadecylamine hydrochloride
trichloromethyl chloroformate
octadecyl isocyanate
Conditions | Yield |
---|---|
With toluene anfangs bei 60-70grad,zuletzt bei Siedetemperatur; |
formaldehyd
octadecylamine hydrochloride
benzoyl chloride
isobutyraldehyde
3-(Benzoyl-octadecyl-amino)-2,2-dimethyl-propionaldehydd
Conditions | Yield |
---|---|
(i) aq. iPrOH, (ii) /BRN= 471389/, Et3N, CHCl3; Multistep reaction; |
Conditions | Yield |
---|---|
In water Heating; |
octadecylamine hydrochloride
4-amino-3,6-disulfo-1,8-naphthaldehyde anhydride dipotassium salt
Conditions | Yield |
---|---|
In water Heating; pH 5, Li(1+)/H(1+) acetate buffer; |
octadecylamine hydrochloride
NBD chloride
4-n-Octadecylamino-7-nitrobenz-2,1,3-oxadiazol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In methanol; water Heating; |
octadecylamine hydrochloride
Conditions | Yield |
---|---|
With water at 100℃; vom pH 8-9; |
methanol
carbon dioxide
octadecylamine hydrochloride
n-octadecylcarbamate methyl ester
Conditions | Yield |
---|---|
In water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorobenzene 2: ammonia View Scheme |
Conditions | Yield |
---|---|
In neat (no solvent) twice recrystd. and vac. dried; | |
recrystd. twice, dried in vac.; |
copper diacetate
octadecylamine hydrochloride
salicylaldehyde
{Cu(C6H4(O)CHN(CH2)17CH3)2}
Conditions | Yield |
---|---|
In ethanol | |
In ethanol |
octadecylamine hydrochloride
Conditions | Yield |
---|---|
In not given recrystd. twice, vac. dried; |
Conditions | Yield |
---|---|
In water; butan-1-ol at 60 - 100℃; |
Empirical Formula: C18H40ClN
Molecular Weight: 305.9699 g/mol
EINECS: 217-410-2
Flash Point: 154.1 °C
Melting point: 157-160 °C
Storage tempreture: 2-8 °C
Appearance: White powder
Enthalpy of Vaporization: 59.33 kJ/mol
Boiling Point: 348.9 °C at 760 mmHg
Vapour Pressure: 4.88E-05 mmHg at 25 °C
Structure of Octadecylamine hydrochloride (CAS NO.1838-08-0):
IUPAC Name of Octadecylamine hydrochloride (CAS NO.1838-08-0): Octadecylazanium chloride
Product Categories: Alkylamine Salts & Quarternary ;Cationic Surfactants;Functional Materials
1. | unr-mus LDLo:200 mg/kg | ATMPA2 Annals of Tropical Medicine and Parasitology. 32 (1938),177. |
Octadecylamine hydrochloride (CAS NO.1838-08-0) hasn't been listed as a carcinogen by NTP, IARC, ACGIH, or CA Prop 65. You can see actual entry in RTECS for complete information.
Reported in EPA TSCA Inventory.
Poison by an unspecified route. When heated to decomposition it emits very toxic fumes of NOx and HCl. See also OCTADECYLAMINE.
Safety Statements: 24/25
R24:Toxic in contact with skin.
R25 :Toxic if swallowed.
Octadecylamine hydrochloride ,its cas register number is 1838-08-0. It also can be called Octadecan-1-aminium chloride ; 1-Octadecanamine, hydrochloride ;and 1-Octadecanamine, hydrochloride (1:1) . It is hazardous,so the first aid measures and others should be known. Such as: When on the skin: first,should flush skin with plenty of water immediately for at least 15 minutes while removing contaminated clothing. Secondly,Get medical aid. Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Then get medical aid soon. While ,it's Inhaled: Remove from exposure and move to fresh air immediately.Give artificial respiration while not breathing. When breathing is difficult, give oxygen. And as soon as to get medical aid. Then you have the ingesting of the product : If victim is conscious and alert, give 2-4 cupfuls of milk or water. Get medical aid immediately.
In addition, Octadecylamine hydrochloride (CAS NO.1838-08-0) can stable under normal temperatures and pressures, and you must not take it with strong oxidants. And also prevent it to broken down into hazardous decomposition products: irritating and toxic fumes and gases.
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