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inquiryProduct description: Product name 4-(Methylamino)benzoic acid CAS number 10541-83-0 Assay ≥99% Appearance White powder Capacity 200mt/year Application Pharmaceutical/pesticid
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inquiry4-(Methylamino)benzoic acid CAS:10541-83-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryp-N,N-dimethylaminobenzoic acid
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
Stage #1: p-N,N-dimethylaminobenzoic acid With 1,4-diaza-bicyclo[2.2.2]octane; rose bengal; acetic acid In acetonitrile at 20℃; for 2h; Flow reactor; Irradiation; Stage #2: With sulfuric acid In methanol; water at 20℃; for 12h; | 96% |
Conditions | Yield |
---|---|
With copper In water at 100℃; for 12h; Ullmann reaction; | 93.3% |
4-(benzotriazol-1-ylmethyl-amino)-benzoic acid
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran for 0.333333h; Heating; | 91% |
4-amino-benzoic acid
dimethyl sulfate
A
N-methyl-p-aminobenzoic acid
B
methyl 4-(N-methyl)aminobenzoate
C
4-methoxycarbonyl aniline
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran for 2h; Methylation; esterification; Heating; | A 10 % Spectr. B 5 % Spectr. C 76% |
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water Heating / reflux; | 74% |
With hydrogenchloride at 90 - 92℃; for 4.5h; | 64.2% |
4-amino-benzoic acid
carbonic acid dimethyl ester
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With sodium-exchanged Y-zeolite at 130℃; for 9h; | A 74% B n/a |
4-amino-benzoic acid
carbonic acid dimethyl ester
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
NaY-faujasite at 130℃; for 9h; | 74% |
Conditions | Yield |
---|---|
With copper In water at 100℃; for 48h; Ullmann reaction; | 56.4% |
4-bromo-N-methylaniline
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With n-butyllithium; diethyl ether anschliessend Behandeln mit Kohlendioxid; |
4-amino-benzoic acid
dimethyl sulfate
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With aqueous alkali |
Conditions | Yield |
---|---|
With methanol; potassium hydroxide | |
With potassium hydroxide | |
With methanol; potassium hydroxide |
4-amino-benzoic acid
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; formaldehyd; zinc |
N-methylaniline
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With magnesium; methyl iodide at 190 - 200℃; im Kohlendioxydstrom und Zersetzung der Magnesiumverbindung mit Salmiak; |
Dimethyl-p-toluidine
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
in der tierischen Organismus; |
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With water at 25℃; Rate constant; Mechanism; |
4-[N-methyl-N-(trifluoroacetyl)amino]benzoic acid
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With 1-benzyl-1-aza-18-crown-6; barium thiocyanate; tetramethyl-ammonium; ethylate In ethanol at 25℃; Rate constant; other aza<18>crown-6 compound; also without Ba(SCN)2; inhibition with 4-MeCON(Me)C6H4COOH or 4-MeNHC6H4COOH; |
methanol
4-amino-benzoic acid
methyl iodide
N-methyl-p-aminobenzoic acid
4-amino-benzoic acid
dimethyl sulfate
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
diethyl ether
carbon dioxide
N-methylaniline
methyl iodide
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
hydrogenchloride
methyl N-methyl-N-nitroso-4-aminobenzoate
N-methyl-p-aminobenzoic acid
hydrogenchloride
ethyl 4-N-methyl-N-nitrosoaminobenzoate
N-methyl-p-aminobenzoic acid
sulfuric acid
4-(acetyl-methyl-amino)-isophthalic acid
N-methyl-p-aminobenzoic acid
4-amino-benzoic acid
2-(2-Methoxyethoxy)ethyl methyl carbonate
A
N-methyl-p-aminobenzoic acid
B
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With NaY faujasite In diethylene glycol dimethyl ether at 135℃; for 10h; Kinetics; |
ethyl p-acetamidobenzoate
A
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / 60percent aq. NaOH, benzyltriethylammonium chloride / benzene / 5 h / 40 °C 2: 64.2 percent / aq. HCl / 4.5 h / 90 - 92 °C View Scheme |
O2-{2,4-dinitro-5-((4-N-methylamino)benzoyloxy-phenyl)}-1-(N,N-dimethylamino)-diazen-1-ium 1,2-diolate
A
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With water In aq. phosphate buffer; dimethyl sulfoxide at 25℃; pH=7.4; Kinetics; Temperature; |
GLUTATHIONE
O2-{2,4-dinitro-5-((4-N-methylamino)benzoyloxy-phenyl)}-1-(N,N-dimethylamino)-diazen-1-ium 1,2-diolate
A
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
In aq. phosphate buffer; dimethyl sulfoxide at 37℃; for 0.5h; pH=7.4; Kinetics; |
GLUTATHIONE
O2-{2,4-dinitro-5-((4-N-methylamino)benzoyloxy-phenyl)}-1-(N,N-dimethylamino)-diazen-1-ium 1,2-diolate
A
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
With glutathione S-transferase P1 In aq. phosphate buffer; dimethyl sulfoxide at 37℃; for 0.0166667h; pH=7.4; Enzymatic reaction; |
methanol
N-methyl-p-aminobenzoic acid
methyl 4-(N-methyl)aminobenzoate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid for 72h; Heating; | 100% |
With toluene-4-sulfonic acid for 18h; Reflux; | 100% |
With toluene-4-sulfonic acid for 18h; Reflux; | 100% |
2-amino-4-(morpholin-4-yl)-6-(1-bromomethyl)-1,3,5-triazine
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 12h; | 99% |
2-amino-4-(4-phenylpiperazin-1-yl)-6-(1-bromomethyl)-1,3,5-triazine
N-methyl-p-aminobenzoic acid
4-({[2-amino-4-(4-phenylpiperazin-1-yl)-1,3,5-triazin-6-yl]methyl}methylamino)benzoic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 12h; | 97% |
N-methyl-p-aminobenzoic acid
4-(formyl-methyl-amino)-benzoic acid
Conditions | Yield |
---|---|
In formic acid; water | 97% |
N-methyl-p-aminobenzoic acid
1,2-diamino-benzene
N-(4-(1H-benzoimidazol-2-yl)-phenyl)-N-methyl-amine
Conditions | Yield |
---|---|
With polyphosphoric acid at 210℃; for 4h; | 96% |
Stage #1: N-methyl-p-aminobenzoic acid; 1,2-diamino-benzene at 200 - 210℃; for 4h; Stage #2: With water at 20 - 80℃; |
N-methyl-p-aminobenzoic acid
Propargylamine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; | 95.6% |
N-methyl-p-aminobenzoic acid
3-chloro-4-(methylamino)benzoic acid
Conditions | Yield |
---|---|
With tert-butylhypochlorite In acetic acid | 94.5% |
N-methyl-p-aminobenzoic acid
3-Bromo-4-ethylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: N-methyl-p-aminobenzoic acid With pyridine In dichloromethane at 20℃; for 1h; Stage #2: With bromine In dichloromethane at -20℃; for 5h; Reagent/catalyst; Solvent; | 94% |
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 25℃; Inert atmosphere; | 93% |
N-methyl-p-aminobenzoic acid
2-((2,4-difluorobenzyl)(pyridin-2-yl)amino)ethanol
Conditions | Yield |
---|---|
Stage #1: N-methyl-p-aminobenzoic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 0.05h; Stage #2: 2-((2,4-difluorobenzyl)(pyridin-2-yl)amino)ethanol In dichloromethane at 25℃; | 92% |
N-methyl-p-aminobenzoic acid
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 92% |
N-methyl-p-aminobenzoic acid
benzyl chloroformate
4-<<(benzyloxy)carbonyl>methylamino>benzoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran at 0 - 25℃; for 18h; | 91.13% |
With sodium hydroxide In 1,4-dioxane; water at 0 - 5℃; for 0.5h; | 86% |
With sodium hydrogencarbonate In tetrahydrofuran at 0 - 21℃; for 2h; | 78% |
N-methyl-p-aminobenzoic acid
4,5-dimethoxyanthranilamide
4,5-Dimethoxy-2-(4-methylamino-benzoylamino)-benzamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 50h; | 91% |
N-methyl-p-aminobenzoic acid
2,4-diamino-6-(hydroxymethyl)pteridine hydrochloride
4-[(2,4-diaminopteridin-6-ylmethyl)methylamino]benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,4-diamino-6-(hydroxymethyl)pteridine hydrochloride In water at 20 - 80℃; for 0.0833333h; Stage #2: With dibromotriphenylphosphorane In N,N-dimethyl acetamide at 20℃; for 20h; Stage #3: N-methyl-p-aminobenzoic acid With N-ethyl-N,N-diisopropylamine at 20℃; for 72h; | 90% |
Stage #1: 2,4-diamino-6-(hydroxymethyl)pteridine hydrochloride With dibromotriphenylphosphorane In N,N-dimethyl acetamide at 20℃; for 24h; Inert atmosphere; Stage #2: N-methyl-p-aminobenzoic acid With N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 20 - 60℃; for 72h; | 56% |
Stage #1: 2,4-diamino-6-(hydroxymethyl)pteridine hydrochloride With bromine; triphenylphosphine In ISOPROPYLAMIDE at 0 - 20℃; for 20h; Stage #2: N-methyl-p-aminobenzoic acid With N-ethyl-N,N-diisopropylamine In ISOPROPYLAMIDE at 60 - 70℃; for 24h; Stage #3: With hydrogenchloride; sodium hydroxide more than 3 stages; |
N-methyl-p-aminobenzoic acid
N-methyl-1,2-phenylenediamine
N-(4-(1-methyl-1H-benzoimidazol-2-yl)-phenyl)-N-methyl-amine
Conditions | Yield |
---|---|
With polyphosphoric acid at 200℃; for 3h; | 90% |
Stage #1: N-methyl-p-aminobenzoic acid; N-methyl-1,2-phenylenediamine at 200 - 210℃; for 4h; Stage #2: With water at 20 - 80℃; |
N-methyl-p-aminobenzoic acid
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With sodium hydroxide | 89% |
N-methyl-p-aminobenzoic acid
benzyl chloroformate
4-(((benzyloxy)carbonyl)amino)benzoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran; water at 0 - 21℃; for 4h; | 89% |
propylamine
N-methyl-p-aminobenzoic acid
4-(N-methylamino)-N-propylbenzamide
Conditions | Yield |
---|---|
With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane at 20℃; for 17h; | 87% |
di-tert-butyl dicarbonate
N-methyl-p-aminobenzoic acid
4-((tert-butoxycarbonyl)(methyl)amino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: di-tert-butyl dicarbonate; N-methyl-p-aminobenzoic acid With sodium hydroxide In 1,4-dioxane; water at 20℃; for 48h; Stage #2: With hydrogenchloride In water Cooling with ice bath; | 87% |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran for 48h; Reflux; | 69% |
With triethylamine In 1,4-dioxane; water | |
With triethylamine In tetrahydrofuran at 20℃; for 24h; | 0.54 g |
With triethylamine In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 0.54 g |
N-methyl-p-aminobenzoic acid
trifluoroacetic anhydride
A
4-[N-methyl-N-(trifluoroacetyl)amino]benzoic acid
B
p-benzoic anhydride
Conditions | Yield |
---|---|
In chloroform at 20℃; for 3h; | A 84% B 80 mg |
N-methyl-p-aminobenzoic acid
(4-(methylamino)phenyl)methanol
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 0 - 25℃; for 6h; | 84% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 24h; | 65% |
Multi-step reaction with 2 steps 1: acetyl chloride / 20 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: acetyl chloride / 20 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 °C View Scheme |
N-methyl-p-aminobenzoic acid
4-(N-acetyl-N-methylamino)benzoic acid
Conditions | Yield |
---|---|
With acetic anhydride In pyridine | 84% |
With acetic anhydride In pyridine | 84% |
With acetic anhydride In pyridine | 84% |
With acetic anhydride In pyridine | 84% |
N-methyl-p-aminobenzoic acid
benzotriazol-1-ol
4-(methylamino)benzoic acid benzotriazol-1-yl ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran; dichloromethane at 20℃; | 84% |
carbon dioxide
N-methyl-p-aminobenzoic acid
p-N,N-dimethylaminobenzoic acid
Conditions | Yield |
---|---|
With phenylsilane In N,N-dimethyl acetamide at 60℃; for 4h; Reagent/catalyst; Sealed tube; | 84% |
Conditions | Yield |
---|---|
With polyphosphoric acid at 205℃; for 4h; | 83% |
Stage #1: N-methyl-p-aminobenzoic acid; 2-amino-phenol at 205℃; for 4h; Stage #2: With water at 20 - 80℃; | 83% |
N-methyl-p-aminobenzoic acid
2,3-dichloro-5,6-dicyanopyrazine
4-[(3-chloro-5,6-dicyanopyrazin-2-yl)methylamino]benzoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran for 12h; Reflux; | 83% |
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