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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Hexachloroacetone Manufacturer/High quality/Best price/In stock

Cas:116-16-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Hexachloroacetone with high purity

Cas:116-16-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Hexachloroacetone

Cas:116-16-5

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,1,1,3,3,3-Hexachloro-2-propanone

Cas:116-16-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Product Name: Hexachloroacetone Synonyms: hexachloro-aceton;Hexachloropropanone;Kureha HCA;Perchloro-2-propanone;HEXACHLORO-2-PROPANONE, WACKER QUALITY;HEXACHLOROACETONE, 99+%, REDISTILLED;HEXACHLOROACETONE 98% (GC);Hexachloroacetone,

116-16-5 Hexachloroacetone

Cas:116-16-5

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

2-Propanone,1,1,1,3,3,3-hexachloro-CAS NO.: 116-16-5

Cas:116-16-5

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Superiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail

LOW price 99% Hexachloroacetone CAS:116-16-5

Cas:116-16-5

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Triumph International Development Limilted

Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,DHL/TNT/FEdex/UPS/EMS Port:QI

Hexachloroacetone

Cas:116-16-5

Min.Order:10 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Hexachloroacetone

Cas:116-16-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Hexachloroacetone

Cas:116-16-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Hexachloroacetone

Cas:116-16-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

2-Propanone,1,1,1,3,3,3-hexachloro-

Cas:116-16-5

Min.Order:0

Negotiable

Type:Other

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Hangzhou Dingyan Chem Co., Ltd

Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. We could give you: 1.Best qualit

Hexachloroacetone

Cas:116-16-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Other

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GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Manufacturers

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

2-Propanone,1,1,1,3,3,3-hexachloro-

Cas:116-16-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

Hot selling products CAS 116-16-5 with fast delivery

Cas:116-16-5

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

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Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Other

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Hubei Langyou International Trading Co., Ltd

Hexachloroacetone Application:Hexachloroacetone

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Other

inquiry

Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

we produce and sell good chemicals around the world.Appearance:white power Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:SEA OR AIR Port:China Main Po

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

HexachloroacetoneAppearance:liquid Storage:Store below +30°C. Application:Reagent used for the polymerization of vinyl compounds and for the conversion of nucleoside-3′-phosphonates to the corresponding phosphates Transportation:By express (Door to d

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

Appearance:fine powder Storage:Tightly sealed in a clean, cool, dry area. Keep away from strong,direct light. Package:Packed In Paper-drums and plastic bag inside.N.W:25kg;G.W.:28KG, ID.35cm X H53cm, or depending on the customers' requirement Transp

Hexachloroacetone

Cas:116-16-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

Hexachloroacetone Basic information Product Name: Hexachloroacetone

116-16-5 C3Cl6O Hexachloroacetone

Cas:116-16-5

Min.Order:100 Gram

Negotiable

Type:Trading Company

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

2-Propanone,1,1,1,3,3,3-hexachloro-

Cas:116-16-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Harmonious Natural Bio-Technology Co., Ltd.

Before-Sale Service:---Any inquiries will be replied within 12 hours.---Golden Manufactory under?ISO/GMP?with?large stock.---Dedication to quality,We?have?strict?quality?control?system.?---OEM/ODM Available.---Sample is available for your evaluation

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Sigma Chemical Co., Ltd.

Qingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo

High Quality 1,1-Cyclobutanedicarboxylic acid

Cas:116-16-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

inquiry

Xiamen BaiFuchem Co.,Ltd

BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art

High Purity Hexachloroacetone

Cas:116-16-5

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

Hexachloroacetone

Cas:116-16-5

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole
73501-03-8

2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

4-methoxybenzonitrile
874-90-8

4-methoxybenzonitrile

C

dimethyl 3-(p-methoxyphenyl)isothiazole-4,5-dicarboxylate
59291-73-5

dimethyl 3-(p-methoxyphenyl)isothiazole-4,5-dicarboxylate

D

S

S

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene at 161℃; for 0.8h;A 99%
B 8%
C 88%
D n/a
acetone
67-64-1

acetone

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With chlorine; pyrographite at 150 - 160℃; for 7h; Temperature; Flow reactor; Industrial scale;98.4%
pentachloro-2-(trimethylsiloxy)propene
87651-34-1

pentachloro-2-(trimethylsiloxy)propene

A

chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

B

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With chlorine at 160℃;A 75%
B 51.8%
2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole
73501-03-8

2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

ethyl 3-(p-methoxyphenyl)isothiazole-4-carboxylate
76162-57-7

ethyl 3-(p-methoxyphenyl)isothiazole-4-carboxylate

C

ethyl 3-(p-methoxyphenyl)isothiazole-5-carboxylate
76162-58-8

ethyl 3-(p-methoxyphenyl)isothiazole-5-carboxylate

D

4-methoxybenzonitrile
874-90-8

4-methoxybenzonitrile

E

S

S

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene at 161℃; for 1h;A n/a
B 47%
C 35%
D 16%
E n/a
acetone
67-64-1

acetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

pentachloroacetone
1768-31-6

pentachloroacetone

Conditions
ConditionsYield
With N-benzyl-N,N,N-triethylammonium chloride; chlorine at 40 - 70℃;A 8%
B 43%
With chlorine an der Sonne;
With acetic acid beim Chlorieren anfangs in Gegenwart von wenig HCl bei Raumtemperatur, spaeter in Gegenwart von Natriumacetat bei Siedetemperatur;
chloroacetone
78-95-5

chloroacetone

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With chlorine at 50 - 100℃;
glycerol
56-81-5

glycerol

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With iodine; chlorine
citric acid
77-92-9

citric acid

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With water; chlorine im Sonnenlicht;
2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole
73501-03-8

2,2-bis(trichloromethyl)-5-(p-methoxyphenyl)-1,3,4-oxathiazole

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

4-methoxybenzonitrile
874-90-8

4-methoxybenzonitrile

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene for 1h; Heating; other oxathiazoles also thermolised, also in the presence of dipolarophiles;A 99 % Chromat.
B 98 % Chromat.
chlorine
7782-50-5

chlorine

chloroacetone
78-95-5

chloroacetone

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
at 50 - 100℃;
water
7732-18-5

water

chlorine
7782-50-5

chlorine

citric acid
77-92-9

citric acid

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
im Sonnenlicht;
hydrogenchloride
7647-01-0

hydrogenchloride

chlorine
7782-50-5

chlorine

acetic acid
64-19-7

acetic acid

acetone
67-64-1

acetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

pentachloroacetone
1768-31-6

pentachloroacetone

Conditions
ConditionsYield
at 20℃; Zusatz von Natriumacetat bei Siedetemperatur;
chlorine
7782-50-5

chlorine

acetic acid
64-19-7

acetic acid

chloroacetone
78-95-5

chloroacetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

pentachloroacetone
1768-31-6

pentachloroacetone

C

decachloro-hexane-2,5-dione
855912-10-6

decachloro-hexane-2,5-dione

Conditions
ConditionsYield
at 160℃; unter Belichtung;
iodine
7553-56-2

iodine

chlorine
7782-50-5

chlorine

glycerol
56-81-5

glycerol

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

trichlorolactic acid

trichlorolactic acid

C

glycerol chlorohydrin

glycerol chlorohydrin

D

glycerol dichlorohydrin

glycerol dichlorohydrin

Conditions
ConditionsYield
Produkt5:Oxalsaeure;
1,1-Dichloroacetone
513-88-2

1,1-Dichloroacetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

1,1,1-trichloroacetone
918-00-3

1,1,1-trichloroacetone

C

pentachloroacetone
1768-31-6

pentachloroacetone

Conditions
ConditionsYield
With pyridine; chlorine at 70 - 80℃; for 4h;
1,1,3-trichloroacetone
921-03-9

1,1,3-trichloroacetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

pentachloroacetone
1768-31-6

pentachloroacetone

Conditions
ConditionsYield
With pyridine; chlorine at 70 - 80℃;
1,1,1-trichloroacetone
918-00-3

1,1,1-trichloroacetone

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Conditions
ConditionsYield
With pyridine; chlorine at 120 - 125℃;
chloroacetone
78-95-5

chloroacetone

A

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

B

1,1,1-trichloroacetone
918-00-3

1,1,1-trichloroacetone

C

pentachloroacetone
1768-31-6

pentachloroacetone

Conditions
ConditionsYield
With pyridine; chlorine at 70 - 80℃; for 7.75h;
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

1,1,1,3,3,3-hexachloro-propan-2-ol
6188-63-2

1,1,1,3,3,3-hexachloro-propan-2-ol

Conditions
ConditionsYield
With N,N'-hexamethylenebis(1-benzyl-3-carbamoyl-1,4-dihydropyridine) In dichloromethane at 25℃; Rate constant; other reagents, solvents;100%
With N,N'-hexamethylenebis(1-benzyl-3-carbamoyl-1,4-dihydropyridine) In dichloromethane at 25℃; Kinetics; var. of reagent, solvent;100%
With 1,2-dimethyl-1,4-dihydropyridine; zinc(II) iodide In cyclohexane at 20℃; for 24h;100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

Triphenylmethylamin
5824-40-8

Triphenylmethylamin

trityl isocyanate
4737-21-7

trityl isocyanate

Conditions
ConditionsYield
With triethylamine In dichloromethane for 2h; Ambient temperature;100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

isopropylamine
75-31-0

isopropylamine

A

chloroform
67-66-3

chloroform

B

N-Isopropyl-2,2,2-trichloroacetamide
23144-67-4

N-Isopropyl-2,2,2-trichloroacetamide

Conditions
ConditionsYield
In hexaneA n/a
B 100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-butylamine
109-73-9

N-butylamine

A

chloroform
67-66-3

chloroform

B

trichloro-acetic acid butylamide
31464-96-7

trichloro-acetic acid butylamide

Conditions
ConditionsYield
In hexaneA n/a
B 100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

(1R,9R,12S)-12-Hydroxymethyl-1,5-dimethyl-8-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),4-dien-12-ol

(1R,9R,12S)-12-Hydroxymethyl-1,5-dimethyl-8-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),4-dien-12-ol

C15H18O4

C15H18O4

Conditions
ConditionsYield
With triethylamine In dichloromethane for 1h; Ambient temperature;100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

2-amino-5-iodobenzoic acid
5326-47-6

2-amino-5-iodobenzoic acid

5-iodoisatoic anhydride
116027-10-2

5-iodoisatoic anhydride

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane; water at 20℃; for 0.166667h;100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

tributyltin methoxide
1067-52-3

tributyltin methoxide

tributyl-trichloromethyl-stannane
5764-62-5

tributyl-trichloromethyl-stannane

Conditions
ConditionsYield
byproducts: CCl3COOCH3; 1:1.1; 33°C / 7 d and 55°C / 4 h;100%
byproducts: Cl3CCOOCH3; 55°C, 4 h;;
byproducts: Cl3CCOOCH3; 55°C, 4 h;;
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

tributyltin methoxide
1067-52-3

tributyltin methoxide

1.1.1.3.3.3-Hexachlor-2-methoxy-2--propan
14630-19-4

1.1.1.3.3.3-Hexachlor-2-methoxy-2--propan

Conditions
ConditionsYield
In tetrachloromethane 1:1;100%
In neat (no solvent) addn. of tributyltin alkoxide to ketone (1:1 mole ratio) at 33°C; proved by NMR;100%
In neat (no solvent) addn. of tributyltin alkoxide to ketone (1:1 mole ratio) at 33°C; proved by NMR;100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-Trimethylstannyldiphenylmethylenamin
34982-42-8

N-Trimethylstannyldiphenylmethylenamin

(C4H9)3SnOC(CCl3)2NC(C6H5)2
34982-57-5

(C4H9)3SnOC(CCl3)2NC(C6H5)2

Conditions
ConditionsYield
100%
100%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-ethyl-N-(3-nitropyridine-2-yl)-1H-pyrrol-1-amine
332379-50-7

N-ethyl-N-(3-nitropyridine-2-yl)-1H-pyrrol-1-amine

N,N'-bis[[N-ethyl-N-(pyrrol-1-yl)]-2-amino-pyridin-3-yl]urea[1,2-b][1,2,5]benzotriazepin-11-one
332379-61-0

N,N'-bis[[N-ethyl-N-(pyrrol-1-yl)]-2-amino-pyridin-3-yl]urea[1,2-b][1,2,5]benzotriazepin-11-one

Conditions
ConditionsYield
In dichloromethane at 20℃; for 4h;99%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

2,2,3,3-tetrafluoropropanol
76-37-9

2,2,3,3-tetrafluoropropanol

A

chloroform
67-66-3

chloroform

B

bis(2,2,3,3-tetrafluoropropyl) carbonate
1422-70-4

bis(2,2,3,3-tetrafluoropropyl) carbonate

Conditions
ConditionsYield
With potassium fluoride; zirconium(IV) oxide at 140℃; for 10h; Product distribution / selectivity; pressure tight reactor;A 99%
B 99%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

2,2,2-trifluoroethanol
75-89-8

2,2,2-trifluoroethanol

A

chloroform
67-66-3

chloroform

B

bis(2,2,2-trifluoroethyl) carbonate
1513-87-7

bis(2,2,2-trifluoroethyl) carbonate

Conditions
ConditionsYield
With potassium fluoride; zirconium(IV) oxide at 140℃; for 10h; pressure tight reactor;A 99%
B 99%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-benzyl-2-(phenylethynyl)-4-(trifluoromethyl)aniline

N-benzyl-2-(phenylethynyl)-4-(trifluoromethyl)aniline

benzyl[2-(phenylethynyl)-4-(trifluoromethyl)phenyl]carbamic chloride

benzyl[2-(phenylethynyl)-4-(trifluoromethyl)phenyl]carbamic chloride

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexachloro-propan-2-one With pyridine In dichloromethane at -78℃; Inert atmosphere;
Stage #2: N-benzyl-2-(phenylethynyl)-4-(trifluoromethyl)aniline In dichloromethane at -78 - 20℃; Inert atmosphere;
99%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

3,3,3-Trichloro-2-trichloromethyl-2-trimethylsilanyloxy-propionitrile

3,3,3-Trichloro-2-trichloromethyl-2-trimethylsilanyloxy-propionitrile

Conditions
ConditionsYield
aluminium trichloride at 40 - 50℃; for 1h;98%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-benzyl-5-methyl-2-(phenylethynyl)aniline
1380395-17-4

N-benzyl-5-methyl-2-(phenylethynyl)aniline

benzyl[5-methyl-2-(phenylethynyl)phenyl]carbamic chloride

benzyl[5-methyl-2-(phenylethynyl)phenyl]carbamic chloride

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexachloro-propan-2-one With pyridine In dichloromethane at -78℃; Inert atmosphere;
Stage #2: N-benzyl-5-methyl-2-(phenylethynyl)aniline In dichloromethane at -78 - 20℃; Inert atmosphere;
98%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

1-amino-2-propene
107-11-9

1-amino-2-propene

A

chloroform
67-66-3

chloroform

B

2,2,2-trichloro-N-(2-propenyl)acetamide
39089-56-0

2,2,2-trichloro-N-(2-propenyl)acetamide

Conditions
ConditionsYield
In hexane for 0.5h;A n/a
B 97%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

(1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]-1-[pentyl]methyl}amine
694526-76-6

(1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]-1-[pentyl]methyl}amine

(4S,5R,1'R)-4-chloromethyl-1-(4-methoxyphenyl)-5-phenyl-3-(1'-phenylethyl)imidazolidin-2-one

(4S,5R,1'R)-4-chloromethyl-1-(4-methoxyphenyl)-5-phenyl-3-(1'-phenylethyl)imidazolidin-2-one

Conditions
ConditionsYield
Stage #1: (1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]-1-[pentyl]methyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -78℃; for 2h;
97%
Stage #1: (1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]-1-[pentyl]methyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -10℃; for 2h;
97%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

2,2,3,3-tetrafluoropropanol
76-37-9

2,2,3,3-tetrafluoropropanol

bis(2,2,3,3-tetrafluoropropyl) carbonate
1422-70-4

bis(2,2,3,3-tetrafluoropropyl) carbonate

Conditions
ConditionsYield
Stage #1: 2,2,3,3-tetrafluoropropanol With Tetraethylene glycol dimethyl ether; potassium carbonate at 10 - 30℃;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one at 30 - 70℃; Reagent/catalyst;
97%
With potassium fluoride at 100℃; for 10h;100 g
methanol
67-56-1

methanol

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

Conditions
ConditionsYield
Stage #1: methanol With Tetraethylene glycol dimethyl ether; potassium carbonate at 10 - 30℃;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one at 30 - 75℃; Reagent/catalyst;
97%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

methyl 3-(benzylamino)-4-(phenylethynyl)benzoate

methyl 3-(benzylamino)-4-(phenylethynyl)benzoate

methyl 3-[benzyl(chlorocarbonyl)amino]-4-(phenylethynyl)benzoate

methyl 3-[benzyl(chlorocarbonyl)amino]-4-(phenylethynyl)benzoate

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexachloro-propan-2-one With pyridine In dichloromethane at -78℃; Inert atmosphere;
Stage #2: methyl 3-(benzylamino)-4-(phenylethynyl)benzoate In dichloromethane at -78 - 20℃; Inert atmosphere;
97%
potassium cyanide

potassium cyanide

sodium cyanide
773837-37-9

sodium cyanide

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

16-methylene-4-androstene-3,17-dione
80108-48-1

16-methylene-4-androstene-3,17-dione

C22H29NO

C22H29NO

Conditions
ConditionsYield
With potassium carbonate; sodium hydroxide In water; acetone at 36℃; for 22h;96.05%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

ethanolamine
141-43-5

ethanolamine

A

chloroform
67-66-3

chloroform

B

2,2,2-trichloro-N-(2-hydroxyethyl)acetamide
35234-31-2

2,2,2-trichloro-N-(2-hydroxyethyl)acetamide

Conditions
ConditionsYield
In hexane for 0.5h;A n/a
B 96%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

(1S,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine
867171-99-1

(1S,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine

(4S,5S,1'R)-5-n-butyl-4-chloromethyl-1-(4-methoxyphenyl)-3-(1'-phenylethyl)imidazolidin-2-one

(4S,5S,1'R)-5-n-butyl-4-chloromethyl-1-(4-methoxyphenyl)-3-(1'-phenylethyl)imidazolidin-2-one

Conditions
ConditionsYield
Stage #1: (1S,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -78℃; for 2h;
96%
Stage #1: (1S,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -10℃; for 2h;
83%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

(1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine
694526-75-5

(1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine

(4S,5R,1'R)-5-n-butyl-4-chloromethyl-1-(4-methoxyphenyl)-3-(1'-phenylethyl)imidazolidin-2-one

(4S,5R,1'R)-5-n-butyl-4-chloromethyl-1-(4-methoxyphenyl)-3-(1'-phenylethyl)imidazolidin-2-one

Conditions
ConditionsYield
Stage #1: (1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -78℃; for 2h;
96%
Stage #1: (1R,2'R,1''R)-(4-methoxyphenyl){1-[1'-(1''-phenylethyl)aziridin-2'-yl]pentyl}amine With sodium hydride In tetrahydrofuran at -10℃; for 1h;
Stage #2: 1,1,1,3,3,3-hexachloro-propan-2-one In tetrahydrofuran at -10℃; for 2h;
96%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-benzyl-4-methyl-2-(phenylethynyl)phenylamine
1380395-15-2

N-benzyl-4-methyl-2-(phenylethynyl)phenylamine

benzyl[4-methyl-2-(phenylethynyl)phenyl]carbamic chloride

benzyl[4-methyl-2-(phenylethynyl)phenyl]carbamic chloride

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexachloro-propan-2-one With pyridine In dichloromethane at -78℃; Inert atmosphere;
Stage #2: N-benzyl-4-methyl-2-(phenylethynyl)phenylamine In dichloromethane at -78 - 20℃; Inert atmosphere;
96%
1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

N-benzyl-2-((4-(trifluoromethyl)phenyl)ethynyl)aniline
1616706-99-0

N-benzyl-2-((4-(trifluoromethyl)phenyl)ethynyl)aniline

ethyl 4-({2-[benzyl(chlorocarbonyl)amino]phenyl}ethynyl)benzoate

ethyl 4-({2-[benzyl(chlorocarbonyl)amino]phenyl}ethynyl)benzoate

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexachloro-propan-2-one With pyridine In dichloromethane at -78℃; Inert atmosphere;
Stage #2: N-benzyl-2-((4-(trifluoromethyl)phenyl)ethynyl)aniline In dichloromethane at -78 - 20℃; Inert atmosphere;
96%
sodium cyanide
773837-37-9

sodium cyanide

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

16-methylene-4-androstene-3,17-dione
80108-48-1

16-methylene-4-androstene-3,17-dione

2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

C22H29NO

C22H29NO

Conditions
ConditionsYield
With sodium carbonate; sodium hydroxide In ethanol; water at 40℃; for 22h;95.77%
potassium cyanide

potassium cyanide

1,1,1,3,3,3-hexachloro-propan-2-one
116-16-5

1,1,1,3,3,3-hexachloro-propan-2-one

16-methylene-4-androstene-3,17-dione
80108-48-1

16-methylene-4-androstene-3,17-dione

2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

C22H29NO

C22H29NO

Conditions
ConditionsYield
With potassium carbonate In water; isopropyl alcohol at 32℃; for 22h;95.72%

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