1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:135-67-1
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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:135-67-1
Min.Order:1 Gram
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:135-67-1
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:135-67-1
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inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 3.Safe a
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inquiryProduct Name: Phenoxazine CAS: 135-67-1 MF: C12H9NO MW: 183.21 EINECS: 205-210-8 Mol File: 135-67-1.mol Phenoxazine Structure Phenoxazine Chemical Properties Melting point 156-159 °C (lit.) Boiling point 316.88°C (
PhenoxazineCAS: 135-67-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:135-67-1
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Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
superior quality Appearance:green gray powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:135-67-1
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryPhenoxazineAppearance:White fine powder Storage:Kept in a cool,dry and ventilated place Package:according to customers' requirements Application:Meets the requirements Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or C
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Product name: Phenoxazine CAS No.:135-67-1 Molecule Formula:C12H9NO Molecule Weight:183.21 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPECIFIC
Cas:135-67-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
We're in good position to supply OLED intermediates . In the past 25 years, we have won technical support from several well-known universities and institutes. We have developed many chemicals together. It makes us capable of developing Cust
Conditions | Yield |
---|---|
With sodium methylate Inert atmosphere; | 98% |
Stage #1: 1-(10H-phenoxazin-10-yl)ethan-1-one With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 24h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction; | 69% |
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube; | 63% |
With sulfuric acid | |
Multi-step reaction with 2 steps 1: potassium hydroxide; triethyl borane / tetrahydrofuran / 24 h / 25 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: sodium hydroxide; water / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
phenoxazine
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 155℃; for 0.25h; Microwave irradiation; chemoselective reaction; | 90% |
N -(2-(2-chlorophenoxy)phenyl)acetamide
phenoxazine
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 155℃; for 0.25h; Microwave irradiation; chemoselective reaction; | 85% |
N-(2-(2-bromophenoxy)phenyl)acetamide
phenoxazine
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 155℃; for 0.25h; Temperature; Solvent; Reagent/catalyst; Microwave irradiation; chemoselective reaction; | 83% |
Multi-step reaction with 2 steps 1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 100 °C / Microwave irradiation 2: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 155 °C / Microwave irradiation View Scheme |
N-(2-(2-iodophenoxy)phenyl)acetamide
phenoxazine
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 155℃; for 0.25h; Microwave irradiation; chemoselective reaction; | 74% |
Multi-step reaction with 2 steps 1: potassium carbonate; N,N`-dimethylethylenediamine / toluene / 24 h / 135 °C / Inert atmosphere 2: sodium methylate / Inert atmosphere View Scheme |
phenoxazine
Conditions | Yield |
---|---|
With zinc | 73% |
phenoxazine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis in 0.2M KClO4 with mercury pool working electrode, Ag/0.1M AgNO3 reference electrode, Pt counter electrode, potential -1.90 V; | 73% |
phenoxazine
Conditions | Yield |
---|---|
at 200 - 250℃; under 1 Torr; for 1h; | 48% |
N-(2-(2-bromophenoxy)phenyl)acetamide
A
1-(10H-phenoxazin-10-yl)ethan-1-one
B
phenoxazine
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 155℃; for 0.25h; Reagent/catalyst; Temperature; Microwave irradiation; | A 27% B 48% |
10-(α-methylbenzyl)phenoxazine
methyl iodide
A
phenoxazine
B
4-methyl-N-(α-phenylethyl)phenoxazine
C
4,6-dimethyl-N-(α-phenylethyl)phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium Product distribution; other 10-alkylphenoxazines, other electrophiles, various ratios of reagents, regiospecifity of lithiation; | A 2% B 40% C 5.5% |
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With hydrogenchloride at 240℃; Condensation; | A 8% B 39% |
Benzohydroxamic acid
A
N-phenyl benzoyl amide
B
phenoxazine
C
4-amino-phenol
D
aniline
E
2-amino-phenol
F
benzil
Conditions | Yield |
---|---|
at 240℃; for 0.5h; Product distribution; Mechanism; | A 11% B 4% C n/a D 32% E n/a F 2% |
Conditions | Yield |
---|---|
With calcium oxide at 560℃; | 18% |
cis-10-(1-Propenyl)phenoxazine
A
phenoxazine
B
1-ethyl-2-methyl-1H-pyrido[3,2,1-k,l]phenoxazine
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In ethyl acetate at 60℃; for 1.66667h; | A n/a B 13.5% |
Conditions | Yield |
---|---|
at 260℃; im mit Kohlendioxyd gefuellten Rohr und Behandeln des Reaktionsprodukts mit Alkohol und verd. Salzsaeure; | |
With 2-aminophenol hydrochloride at 220 - 230℃; | |
at 270℃; |
Conditions | Yield |
---|---|
at 200 - 240℃; | |
at 200 - 240℃; |
Conditions | Yield |
---|---|
With iodine at 270℃; | |
With hydrogenchloride |
10-Methyl-10H-phenoxazine
phenoxazine
Conditions | Yield |
---|---|
With Pyridine hydrobromide at 200℃; for 0.666667h; |
Conditions | Yield |
---|---|
With sulfuric acid; copper In ethanol Heating; |
diazomethane
carbon dioxide
10-(tert-butyldimethylsilyl)-phenoxazine
A
phenoxazine
B
methyl phenoxazine-4-carboxylate
C
10-(tert-Butyl-dimethyl-silanyl)-10H-phenoxazine-4-carboxylic acid methyl ester
D
dimethyl 10-(tert-butyldimethylsilyl)-phenoxazine-4,6-dicarboxylate
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
diazomethane
carbon dioxide
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
methyl phenoxazine-4-carboxylate
C
methyl N-(α-phenylethyl)phenoxazine-4-carboxylate
D
dimethyl 10-(α-methylbenzyl)phenoxazine-4,6-dicarboxylate
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
chloro-trimethyl-silane
10-(tert-butyldimethylsilyl)-phenoxazine
A
phenoxazine
B
10-(tert-Butyl-dimethyl-silanyl)-4-trimethylsilanyl-10H-phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
chloro-trimethyl-silane
10-(tert-butyldimethylsilyl)-phenoxazine
A
phenoxazine
B
10-(tert-Butyl-dimethyl-silanyl)-4,6-bis-trimethylsilanyl-10H-phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
chloro-trimethyl-silane
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
10-(1-Phenyl-ethyl)-4-trimethylsilanyl-10H-phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
chloro-trimethyl-silane
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
10-(1-Phenyl-ethyl)-4-trimethylsilanyl-10H-phenoxazine
C
4,6-bis(trimethylsilyl)-10-(α-methylbenzyl)phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
Dimethyldisulphide
10-(tert-butyldimethylsilyl)-phenoxazine
A
phenoxazine
B
10-(tert-Butyl-dimethyl-silanyl)-4-methylsulfanyl-10H-phenoxazine
C
10-(tert-Butyl-dimethyl-silanyl)-4,6-bis-methylsulfanyl-10H-phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
Dimethyldisulphide
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
4-(methylthio)phenoxazine
C
4,6-bis(methylthio)phenoxazine
D
4,6-dimethylthio-N-(α-phenylethyl)phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
Dimethyldisulphide
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
4-(methylthio)-10-(α-methylbenzyl)phenoxazine
C
4,6-dimethylthio-N-(α-phenylethyl)phenoxazine
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
carbon dioxide
10-(tert-butyldimethylsilyl)-phenoxazine
A
phenoxazine
B
10H-phenoxazine-4-carboxylic acid
C
10-(tert-Butyl-dimethyl-silanyl)-10H-phenoxazine-4-carboxylic acid
D
10-(tert-butyldimethylsilyl)-phenoxazine-4,6-dicarboxylic acid
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Multistep reaction; | |
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) 0 deg C, 1 h; Multistep reaction; |
carbon dioxide
10-(α-methylbenzyl)phenoxazine
A
phenoxazine
B
10-(1-Phenyl-ethyl)-10H-phenoxazine-4-carboxylic acid
C
10-(α-methylbenzyl)phenoxazine-4,6-dicarboxylic acid
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Multistep reaction; | |
With n-butyllithium 1.) THF, hexane, 0 deg C, 3 h, 2.) -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With triethylsilane; trifluoroacetic acid In dichloromethane at 20℃; for 24h; Inert atmosphere; chemoselective reaction; | 99% |
phenoxazine
2-phenyl-4,6-bis(p-bromophenyl)pyrimidine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In N,N-dimethyl-formamide at 130℃; for 48h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With Aliquat 336; sodium hydroxide In water Heating; | 98% |
phenoxazine
2,4,6-tris(4-bromophenyl)-1,3,5-triazine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In toluene for 24h; Reflux; | 97% |
Stage #1: phenoxazine; 2,4,6-tris(4-bromophenyl)-1,3,5-triazine With potassium carbonate In toluene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With tri-tert-butyl phosphine; palladium diacetate In toluene for 24h; Inert atmosphere; Reflux; | 96.5% |
phenoxazine
4,6-bis(4-bromophenyl)-2-methylpyrimidine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In N,N-dimethyl-formamide at 130℃; for 48h; Inert atmosphere; | 97% |
phenoxazine
7-bromo-2,3-diphenyl-5-azaquinoxaline
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 48h; | 97% |
With tri-tert-butylphosphonium tetrafluoroborate; palladium diacetate; sodium t-butanolate In toluene Inert atmosphere; Reflux; | 97% |
Conditions | Yield |
---|---|
Stage #1: phenoxazine With tetraethylammonium bromide; potassium hydroxide In acetone at 50℃; for 1.5h; Inert atmosphere; Stage #2: 3-bromomethylheptane In acetone at 60℃; Inert atmosphere; | 97% |
With potassium hydroxide |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 48h; | 97% |
Conditions | Yield |
---|---|
With sodium ethanolate In N,N-dimethyl-formamide at 70 - 150℃; for 48h; | 97% |
With sodium hydride In hexane; N,N-dimethyl-formamide; mineral oil for 10h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With potassium phosphate In N,N-dimethyl-formamide for 16h; Reflux; Inert atmosphere; | 97% |
With potassium carbonate In N,N-dimethyl-formamide at 0.14℃; for 48h; | 31.9% |
Conditions | Yield |
---|---|
With cetyltrimethylammonim bromide; sodium hydroxide In acetone Reflux; | 96% |
phenoxazine
1,3-bis-(4-bromobenzoyl)benzene
1,3-bis{4-(10H-phenoxazine-10-yl)benzoyl}benzene
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); potassium carbonate In toluene at 120℃; for 24h; Buchwald-Hartwig Coupling; | 96% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate In acetonitrile at 20℃; for 12h; Irradiation; | 96% |
With ammonium peroxydisulfate; 2,4,6-triphenylpyrylium tetrafluoroborate In dichloromethane at 20℃; Irradiation; | 92% |
phenoxazine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In toluene for 22h; Buchwald-Hartwig Coupling; Inert atmosphere; Reflux; | 96% |
With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In toluene at 110℃; for 25h; Inert atmosphere; | 96% |
phenoxazine
2,4,6-tris(3-bromophenyl)-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: phenoxazine; 2,4,6-tris(3-bromophenyl)-1,3,5-triazine With potassium carbonate In toluene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With tri-tert-butyl phosphine; palladium diacetate In toluene for 24h; Inert atmosphere; Reflux; | 95.3% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene Reflux; Inert atmosphere; | 95% |
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 6h; Inert atmosphere; Reflux; | 95% |
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 120℃; for 48h; Inert atmosphere; | 76.8% |
phenoxazine
4,6-bis(4-bromophenyl)pyrimidine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In N,N-dimethyl-formamide at 130℃; for 48h; Inert atmosphere; | 95% |
phenoxazine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 48h; | 95% |
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene Reflux; Inert atmosphere; | 93% |
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 100℃; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In toluene at 110 - 120℃; Inert atmosphere; | 95% |
With palladium diacetate; caesium carbonate; triphenylphosphine In toluene at 110℃; for 24h; Inert atmosphere; | 82.6% |
phenoxazine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 24h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
Stage #1: 4-(4-bromophenyl)-2,6-diphenylpyridine; phenoxazine With potassium carbonate In toluene for 0.25h; Inert atmosphere; Stage #2: With triisopropylamine; palladium diacetate In toluene for 48h; Reflux; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; potassium carbonate at 130℃; for 4h; Schlenk technique; Inert atmosphere; Sealed tube; | 94% |
With N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; [Pd(π-cinnamyl)Cl]2 at 130℃; for 4h; Schlenk technique; Inert atmosphere; Sealed tube; | 94% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 220℃; for 6h; Inert atmosphere; | 94% |
With copper(I) oxide In N,N-dimethyl acetamide at 160℃; for 24h; Inert atmosphere; | 90% |
With copper(I) oxide In N,N-dimethyl acetamide at 160℃; for 8h; | 90% |
phenoxazine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 110℃; for 24h; Inert atmosphere; | 94% |
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 110℃; for 24h; Buchwald-Hartwig Coupling; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 20 - 110℃; for 24h; Inert atmosphere; | 93.2% |
phenoxazine
5-bromo-10,15,20-tris(3,5-di-tert-butylphenyl)porphyrinato nickel(II)
Conditions | Yield |
---|---|
With C40H57Cl2N3Pd; sodium t-butanolate In tetrahydrofuran at 60℃; for 13h; Buchwald-Hartwig Coupling; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With oxygen; potassium carbonate In 1,2-dichloro-benzene at 130℃; for 3h; | 93% |
With oxygen; sodium nitrite In toluene at 0 - 20℃; Sealed tube; | 61% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In water; toluene at 120℃; for 24h; Glovebox; Inert atmosphere; | 93% |
phenoxazine
Conditions | Yield |
---|---|
With ytterbium(III) triflate In 1,2-dichloro-ethane | 93% |
With ytterbium(III) triflate In 1,2-dichloro-ethane | 93% |
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