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inquiryHebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
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inquirySodium fluoroborate [Name] Sodium fluoroborate [13755-29-8] [Molecular formula] NaBF4 [Molecular weight] 109.79 [UN] 1759 Index Name Index Index Name Index Appearance White crystalli
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryCAS No.: 13755-29-8 EINECS: 237-340-6 Density: 2.47 g/mL at 25 °C(lit.) Molecular Weight: 109.79 Molecular Formula: BF4Na Appearance:White powder Storage: Room Temperature Package: 25kg/drum or 20kg/bag Application: Pharmaceu
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inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquirySodium tetrafluoroborateCAS:13755-29-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryProduct Detail Minimum Order Qty. 10 Gram
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryPRODUCT DETAILS
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hubei Lidu New Materials Technology Co. , Ltd. is located in No. 12,3C Industrial Park, Zhongxiang Economic Development Zone, Hubei Province. The company is committed to fine chemical raw materials, pharmaceutical intermediates and other production,
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirySodium Fluoborate (Sodium Tetrafluoborate)Appearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx o
Cas:13755-29-8
Min.Order:1 Gram
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inquiryProduct name: Sodium Fluoroborate CAS No.:13755-29-8 Molecule Formula:BF4Na Molecule Weight:109.94 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquirydimanganese decacarbonyl
A
sodium tetrafluoroborate
B
(OC)3Fe(μ-η4:η1-cyclohexadiene)Mn(CO)5
Conditions | Yield |
---|---|
With sodium amalgam In tetrahydrofuran (Ar), reduced Mn-complex (45 min at 0°C, 30 min at 20°C) added at -70°C, stirred for 1 h; solvent removed in vacuo at -30°C, extracted four times with pentane at -25°C (Mn2(CO)10 as by-product), extracted two times with CH2Cl2, solvent removed, dried in high vacuum, (all steps at <-20°C), elem. anal.; | A n/a B 98% |
Conditions | Yield |
---|---|
With BF3 In tetrahydrofuran introduction of BF3 into suspn. of NaBH4 in THF with stirring (-8-(-12)°C, 6 h), stirring (12h, room temp.), addn. of further NaBF4, stirring (2 h); condensing in to N2 cooled Dewar-vessel (25°C, 50 Torr), warming (room temp.); (11)B-NMR; | A n/a B 97.5% |
Conditions | Yield |
---|---|
In further solvent(s) soln. NaBH4 in triglyme was added slowly for 1 h at room temp. to BF3-triglymate; B2H6 was absorbed with THF, NaBF4 was filtered off, solvent was removedby distillation to obtaine more NaBF4; | A 97% B >99 |
C6H4FN2(1+)*C6BF8(1-)
A
sodium tetrafluoroborate
B
para-difluorobenzene
Conditions | Yield |
---|---|
at 160 - 170℃; Glovebox; | A 5% B 95% C 83% D 10% |
sodium tetrahydroborate
BF3-monoglymate
A
sodium tetrafluoroborate
B
diborane
Conditions | Yield |
---|---|
In further solvent(s) soln. NaBH4 in triglyme was added slowly for 3 h at room temp. to BF3-monoglymate; B2H6 was absorbed with THF, NaBF4 was filtered off, solvent was removedby distillation to obtaine more NaBF4; | A 94% B >99 |
Conditions | Yield |
---|---|
In further solvent(s) soln. NaBH4 in tetraglyme was added slowly for 3 h at room temp. to BF3-tetraglymate; B2H6 was absorbed with THF, NaBF4 was filtered off, solvent was removedby distillation to obtaine more NaBF4; | A 94% B >99 |
Conditions | Yield |
---|---|
In water addn. of NaOH to C5H5NHBF4; extn. of pyridine with CHCl3, concn., elem. anal.; | A n/a B 94% |
sodium tetrahydroborate
BF3-tert-butyl methyl etherate
A
sodium tetrafluoroborate
B
diborane
Conditions | Yield |
---|---|
In further solvent(s) soln. NaBH4 in triglyme was added slowly for 3 h at room temp. to BF3-tert-butyl methyl etherate; B2H6 was absorbed with THF, NaBF4 was filtered off, solvent was removedby distillation to obtaine more NaBF4; | A 93% B >99 |
sodium methylate
A
sodium tetrafluoroborate
B
[Ru(η(5)-C5H5)(C(CH=CPh2)=NnPr)(CO)(PiPr3)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: MeOH; stirring (1 h); evapn. (vac.), pptn. on toluene addn., filtering, evapn., washing (pentane); elem. anal.; | A n/a B 90% |
sodium methylate
A
sodium tetrafluoroborate
B
[Ru(η(5)-C5H5)(C(CH=CPh2)=NHPh)(CO)(PiPr3)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: MeOH; stirring (1 h); evapn. (vac.), pptn. on toluene addn., filtering, evapn., washing (pentane); elem. anal.; | A n/a B 90% |
trimethoxonium tetrafluoroborate
A
sodium tetrafluoroborate
B
Dimethyl ether
Conditions | Yield |
---|---|
In acetonitrile under N2, Mo complex dissolved in CH3CN, Me3OBF4 added, stirred at roomtemp. for 0.5 h; evapd., C6H6 added to residue, filtered, solvent removed, dried in vac., recrystd. from hexane with small quantity of CH2Cl2 at -50°C, elem. anal.; | A n/a B n/a C 85% |
sodium methylate
A
sodium tetrafluoroborate
B
[Ru(η(5)-C5H5)(C(NEt2)=C=CPh2)(CO)(PiPr3)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: MeOH; stirring (1 h); evapn. (vac.), toluene addn., filtering, evapn., washing (pentane); elem. anal.; | A n/a B 85% |
sodium methylate
A
sodium tetrafluoroborate
B
[Ru(η(5)-C5H5)(C(NC5H10)=C=CPh2)(CO)(PiPr3)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: MeOH; stirring (1 h); evapn. (vac.), toluene addn., filtering, evapn., washing (pentane); elem. anal.; | A n/a B 80% |
Conditions | Yield |
---|---|
In acetonitrile under N2, Mo complex dissolved in MeCN, added Et3OBF4, stirred for 0.5 h at room temp.; solvent evapd. in vac., added C6H6, filtered, solvent removed, dried invac., recrystd. from hexane with small quantity of CH2Cl2 at -50°C, elem. anal.; | A n/a B n/a C 80% |
sodium tetrahydroborate
((η-C5Me5)Ir(η6-3-methylbenzo{b}thiophene))(BF4)2
A
sodium tetrafluoroborate
B
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
C
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
D
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
E
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
Conditions | Yield |
---|---|
In dichloromethane; water To a stirred soln. of Cp(CH3)5Ir(3-MeBT)(BF4)2 in H2O and CH2Cl2 was added NaBH4 (under N2).; After 3 min the layers were sepd., and the water layer was extd. with CH2Cl2. The combined CH2Cl2 extracts were dried over Na2SO4 and filtered. Product was pptd. by addn. of Et2O. elem. anal.; ratio of isomers: 58:27:8:7; | A n/a B n/a C n/a D n/a E 79% |
trimethoxonium tetrafluoroborate
A
sodium tetrafluoroborate
B
Dimethyl ether
Conditions | Yield |
---|---|
In acetonitrile under N2, W complex dissolved in CH3CN, Me3OBF4 added, stirred at room temp. for 0.5 h; evapd., C6H6 added to residue, filtered, solvent removed, dried in vac., recrystd. from hexane with small quantity of CH2Cl2 at -50°C, elem. anal.; | A n/a B n/a C 79% |
C6H4FN2(1+)*C6BF8(1-)
A
sodium tetrafluoroborate
B
para-difluorobenzene
C
C6BF8(1-)*Na(1+)
Conditions | Yield |
---|---|
at 160 - 170℃; Glovebox; | A 11% B 79% C 71% |
sodium tetrahydroborate
{C5(CH3)5IrC8H6S}(2+)*2(BF4)(1-)={C5(CH3)5IrC8H6S}(BF4)2
A
sodium tetrafluoroborate
B
{C5(CH3)5IrC8H7S}(1+)*(BF4)(1-)={C5(CH3)5IrC8H7S}BF4
C
{C5(CH3)5IrC8H7S}(1+)*(BF4)(1-)={C5(CH3)5IrC8H7S}BF4
D
{C5(CH3)5IrC8H7S}(1+)*(BF4)(1-)={C5(CH3)5IrC8H7S}BF4
E
{C5(CH3)5IrC8H7S}(1+)*(BF4)(1-)={C5(CH3)5IrC8H7S}BF4
Conditions | Yield |
---|---|
In dichloromethane; water H2O and CH2Cl2 were purged with N2 for 5 min. To this stirred soln. was added (C5(CH3)5Ir(BT))(BF4)2 and then NaBH4. After 5 min the layers were separated, and the water layer was extracted with CH2Cl2.; After 5 min the layers were separated, and the water layer was extd. with CH2Cl2. The combined CH2Cl2 extracts were dried over Na2SO4 and filtered. Product was pptd. by addn. of ether. elem. anal.; ratio of isomers: 61:25:8:6; | A n/a B n/a C n/a D n/a E 78% |
sodium tetrahydroborate
{C5(CH3)5Ir(CH3)C8H5S}(2+)*2(BF4)(1-)={C5(CH3)5Ir(CH3)C8H5S}(BF4)2
A
sodium tetrafluoroborate
B
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
C
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
D
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
E
{C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4
Conditions | Yield |
---|---|
In dichloromethane; water H2O and CH2Cl2 were purged with N2 for 5 min. To this stirred soln. was added (C5(CH3)5Ir(2-MeBT))(BF4)2 and then NaBH4.; After 5 min the layers were sepd., and the water layer was extd. with CH2Cl2. The combined CH2Cl2 extracts were dried over Na2SO4 and filtered. Product was pptd. by addn. of Et2O. elem. anal.; ratio of isomers: 60:23:9:8; | A n/a B n/a C n/a D n/a E 78% |
Conditions | Yield |
---|---|
at 160 - 170℃; Glovebox; | A 17% B 77% C 3% D 65% E 12% |
C6H4FN2(1+)*C3BF6(1-)
A
sodium tetrafluoroborate
B
para-difluorobenzene
C
C3BF6(1-)*Na(1+)
Conditions | Yield |
---|---|
at 160 - 170℃; Glovebox; | A 76% B 51% C 9% D 76% |
Conditions | Yield |
---|---|
In dichloromethane N2-atmosphere; 1 h; filtration (Al2O3), evapn. (vac.); | A n/a B 75% C n/a |
Conditions | Yield |
---|---|
In dichloromethane N2-atmosphere; 1 h; filtration (Al2O3), evapn. (vac.); | A n/a B 74% C n/a |
A
sodium tetrafluoroborate
{(OC)3Fe(μ-η4:η1-cyclohexadienyl)}2Os(CO)4
Conditions | Yield |
---|---|
In tetrahydrofuran (Ar), added at -70°C, after 1 h warmed to -30°C; solvent removed at -30°C, dissolved in CH2Cl2 at room temp., centrifugation, reduced to dryness, dried for 2 h in vacuo, elem. anal.; | A n/a B 71% |
sodium tetrafluoroborate
Ethyl 4-amino-N-(3,4-dichlorobenzyl)indole-2-carboxylate
N-(3,4-dichlorobenzyl)-2-ethoxycarbonylindole-4-diazonium tetrafluoroborate
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite In phosphorus pentaoxide; water | 100% |
sodium tetrafluoroborate
bis[(2-pyridyl)methyl]amine
Conditions | Yield |
---|---|
With ascorbic acid In water addn. of aq. ligand soln. to aq. FeCl2 soln. (contg. ascorbic acid to reduce Fe(III)) under N2, ratio Fe : Dipica = 1:2.1, addn. of excess NaBF4; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In dichloromethane; water A CH2Cl2 layer of Ni(HNC2H4NHC3H6NHC2H4N(C16H33)C3H6)(ClO4)2 is equilibrated with an aq. layer of NaBF4.; The ClO4(1-) ions are quantitatively replaced by the BF4(1-) ions forming the complex Ni(HNC2H4NHC3H6NHC2H4N(C16H33)C3H6)(BF4)2.; | 100% |
sodium tetrafluoroborate
[Ni(S((CH2)2SCH2C(CH3)NO)2H)(H2O)](1+)*ClO4(1-)=[Ni(S((CH2)2SCH2C(CH3)NO)2H)]ClO4*H2O
Conditions | Yield |
---|---|
In methanol | A 0% B 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
With potassium chloride In dichloromethane; water; acetonitrile byproducts: KBF4; aq. soln. of KCl added to aq. soln. of complex, KBF4 filtered, soln. concd. in vac. to dryness, residue dissolved in MeCN and refluxed for 72 h,cooled to room temp., concd. to dryness then dissolved in CH2Cl2, shake d with aq. soln. of NaBF4; org. phase dried with Na2SO4, concd. in vac., dried at 0.05 Torr; pure by (1)H NMR; | 100% |
Conditions | Yield |
---|---|
In not given Atherton, M. J.; Fawcett, J.; Holloway, J. H.; Hope, E. G.; Karacar, A.;Russell, D. R.; Saunders, G. C. J. Chem. Soc., Dalton Trans. 1996, 321 5; elem. anal.; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In dichloromethane room tepm., pptn., addn. of excess of NaBF4; crystn. (C6H6/CH2Cl2); | 100% |
sodium tetrafluoroborate
(E)-1-((dibutyl(3-hydroxy-3-methylbut-1-en-1-yl)stannyl)hexyl)-3-ethyl-1H-imidazol-3-ium bromide
(E)-1-(6-(dibutyl(3-hydroxy-3-methylbut-1-en-1-yl)stannyl)hexyl)-3-ethyl-1H-imidazol-3-ium tetrafluoroborate
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 100% |
sodium tetrafluoroborate
2-(diacetoxyiodo)mesitylene
2-Methoxyphenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 2-(diacetoxyiodo)mesitylene; 2-Methoxyphenylboronic acid With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; Stage #2: sodium tetrafluoroborate In dichloromethane; water for 0.5h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In water at 20℃; for 5h; | 100% |
Conditions | Yield |
---|---|
In water at 60℃; | 100% |
sodium tetrafluoroborate
1,3-dimethyl-4-(3′,4′,5′-trimethoxyphenyl)-5-(4″-methoxyphenyl)imidazolium iodide
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 100% |
sodium tetrafluoroborate
4-(3-chloro-4,5-dimethoxyphenyl)-5-(4-methoxyphenyl)-1,3-diethylimidazolium iodide
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 100% |
sodium tetrafluoroborate
4-(3-bromo-4,5-dimethoxyphenyl)-5-(4-methoxyphenyl)-1,3-diethylimidazolium iodide
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 100% |
sodium tetrafluoroborate
methyl iodide
Conditions | Yield |
---|---|
Stage #1: BF4(1-)*C71H92N4O5*C24H32O8*H(1+); methyl iodide at 20℃; for 72h; Inert atmosphere; Schlenk technique; Stage #2: sodium tetrafluoroborate In dichloromethane; water; acetone at 20℃; for 18h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
Stage #1: BF4(1-)*C72H95N4O5(1+)*C24H32O8 With hydrogenchloride In diethyl ether; dichloromethane at 20℃; for 1h; Stage #2: sodium tetrafluoroborate In dichloromethane; water; acetone at 20℃; for 18h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane-d2 at 25℃; under 1500.15 Torr; for 120h; Inert atmosphere; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In water at 20℃; for 6h; Inert atmosphere; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In dichloromethane; water | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In acetone at 20℃; for 24h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In water at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; Sonication; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In methanol; water for 0.5h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In methanol; water for 0.5h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In water; acetone at 20℃; for 5h; | 100% |
sodium tetrafluoroborate
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In water; acetone at 20℃; | 100% |
In water; acetone at 20℃; for 0.75h; | 94% |
In water; acetone at 20℃; for 1h; | 89% |
In methanol; water at 20℃; for 1h; Inert atmosphere; |
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