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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Piperonylamine

Cas:2620-50-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Piperonylamine

Cas:2620-50-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 2620-50-0 with best quality

Cas:2620-50-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: Piperonylamine Synonyms: 3,4-Methylenedioxybenzylamine CAS: 2620-50-0 MF: C8H10NO2 Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum Application:Organic intermediate

Piperonylamine

Cas:2620-50-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,3-Benzodioxole-5-methanamine 2620-50-0

Cas:2620-50-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Piperonylamine CAS:2620-50-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat

Piperonylamine CAS:2620-50-0

Cas:2620-50-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3-Benzodioxole-5-methanamine

Cas:2620-50-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:2620-50-0

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Piperonylamine

Cas:2620-50-0

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Piperonylamine

Cas:2620-50-0

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Piperonylamine

Cas:2620-50-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Piperonylamine

Cas:2620-50-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Piperonylamine

Cas:2620-50-0

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Suzhou Sibian Chemical Technology Co., Ltd

The process is mature and can be mass produced to 100 kg, with good quality and purity up to 99%.The product has a large stock and can be supplied stably. Package:bottle Application:Drug R&D Transportation:Sealed drying(25℃) Port:ShangHai

Piperonylamine

Cas:2620-50-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

Benzo[d][1,3]dioxol-5-ylMethanaMine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

PiperonylaMine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Chemsigma International Co.,Ltd.

bulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Appearance:White powder Storage:YES Package:paper drum

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1,3-Benzodioxole-5-methanamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

Piperonylamine CAS No.2620-50-0

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

DB BIOTECH CO., LTD

best seller Application:API

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

2620-50-0

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

HANGZHOU TIANYE CHEMICALS CO., LTD.

HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou .We are a high-tech enterprise specialized in technical research and development, production, development and trade of chemical products. We supply Multiple so

BENZO[D][1,3]DIOXOL-5-YLMETHANAMINE

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

Piperonylamine

Cas:2620-50-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

piperonylonitrile
4421-09-4

piperonylonitrile

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 2h; Reflux;100%
With ammonia; hydrogen In water; isopropyl alcohol at 110℃; under 15001.5 Torr; for 24h; Temperature; Autoclave;95%
With ammonia; hydrogen In toluene at 120℃; under 22502.3 Torr; for 16h; Autoclave;91%
piperonal
120-57-0

piperonal

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine In 2,2,2-trifluoroethanol at 100℃; for 24h; chemoselective reaction;95%
With ammonia; hydrogen In tert-butyl alcohol at 120℃; for 15h;89%
With ammonium formate In toluene at 80℃; for 3h; Inert atmosphere; chemoselective reaction;72%
piperonylonitrile
4421-09-4

piperonylonitrile

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine
6701-35-5

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine

Conditions
ConditionsYield
With sodium tetrahydroborate; nickel dichloride In ethanol at 20℃; for 0.0833333h;A 85%
B 5%
5-(azidomethyl)benzo[d][1,3]dioxole
214783-17-2

5-(azidomethyl)benzo[d][1,3]dioxole

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
Stage #1: 5-(azidomethyl)benzo[d][1,3]dioxole With triphenylphosphine at 110℃; for 20h; Staudinger Azide Reduction; Green chemistry;
Stage #2: With hydrogenchloride In 1,4-dioxane; diethyl ether Green chemistry;
85%
2-Trimethylsilanyl-ethanesulfonic acid (benzo[1,3]dioxol-5-ylmethyl)-amide
106043-11-2

2-Trimethylsilanyl-ethanesulfonic acid (benzo[1,3]dioxol-5-ylmethyl)-amide

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With cesium fluoride In N,N-dimethyl-formamide at 95℃; for 22h;80%
With cesium fluoride In N,N-dimethyl-formamide at 110℃; for 48h; Inert atmosphere;
methanol
67-56-1

methanol

5-(azidomethyl)benzo[d][1,3]dioxole
214783-17-2

5-(azidomethyl)benzo[d][1,3]dioxole

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

N-methylpiperonylamine
15205-27-3

N-methylpiperonylamine

C

1-(N,N-dimethylaminomethyl)-3,4-(methylenedioxy)benzene
58995-64-5

1-(N,N-dimethylaminomethyl)-3,4-(methylenedioxy)benzene

Conditions
ConditionsYield
With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 3h; Sealed tube; Inert atmosphere; Glovebox;A 9 %Chromat.
B 66%
C 7 %Chromat.
C16H13NO5
432009-40-0

C16H13NO5

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With ethylenediamine In 1,4-dioxane; propan-1-ol; water for 24h; Reflux;20.2%
sulfurous acid mono-(piperonylamino-methyl ester)

sulfurous acid mono-(piperonylamino-methyl ester)

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With hydrogenchloride; steam
piperonal-(Z)-oxime
20747-42-6

piperonal-(Z)-oxime

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With sodium amalgam; acetic acid at 50 - 70℃;
With sodium amalgam; ethanol; acetic acid
With lithium amalgam; diethyl ether
piperonal-(Z)-oxime
20747-42-6

piperonal-(Z)-oxime

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine
6701-35-5

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine

Conditions
ConditionsYield
With acetic acid; zinc
piperonal-(Z)-oxime
20747-42-6

piperonal-(Z)-oxime

aqueous-alcoholic acetic acid

aqueous-alcoholic acetic acid

sodium amalgam

sodium amalgam

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
at 50 - 70℃; lower-melting piperonal oxime;
acetic acid
64-19-7

acetic acid

(E)-3,4-methylenedioxybenzaldehyde oxime
2089-36-3, 20747-41-5, 20747-42-6

(E)-3,4-methylenedioxybenzaldehyde oxime

zinc dust

zinc dust

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine
6701-35-5

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine

piperonal
120-57-0

piperonal

ethanol
64-17-5

ethanol

ammonium amalgam

ammonium amalgam

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine
6701-35-5

bis(benzo[d][1,3]dioxol-5-ylmethyl)amine

C

meso-α,α'-diamino-3,4;3',4'-bis-methylenedioxy-bibenzyl

meso-α,α'-diamino-3,4;3',4'-bis-methylenedioxy-bibenzyl

piperonal
120-57-0

piperonal

rac-Ala-OH
302-72-7

rac-Ala-OH

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

acetaldehyde
75-07-0

acetaldehyde

C

methylammonium carbonate
15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

D

threo-α'-amino-3,4;3',4'-bis-methylenedioxy-bibenzyl-α-ol

threo-α'-amino-3,4;3',4'-bis-methylenedioxy-bibenzyl-α-ol

Conditions
ConditionsYield
at 160℃; anschliessendes Erwaermen mit wss.-aethanol. Salzsaeure;
1,2-(methylenedioxy)-4-bromobenzene
2635-13-4

1,2-(methylenedioxy)-4-bromobenzene

A

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

B

4-formyl-3-methoxyphenoxymethyl polystyrene

4-formyl-3-methoxyphenoxymethyl polystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dimethylformamide / 130 °C
2: LiAlH4; AlCl3 / diethyl ether / 5 h / 20 °C
View Scheme
5-chloro-1,3-benzodioxole
7228-38-8

5-chloro-1,3-benzodioxole

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium carbonate / 1,4-dioxane; water / 36 h / Reflux
2: ethylenediamine / 1,4-dioxane; propan-1-ol; water / 24 h / Reflux
View Scheme
piperonal oxime
2089-36-3

piperonal oxime

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃;
With hydrogen; palladium(II) hydroxide In ethanol at 30 - 60℃; for 6h;
piperonol
495-76-1

piperonol

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: manganese(IV) oxide / dichloromethane
2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 2 h / 60 °C
3: palladium(II) hydroxide; hydrogen / ethanol / 6 h / 30 - 60 °C
View Scheme
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 5.5 h / -30 - 20 °C / Inert atmosphere
2.1: sodium azide / N,N-dimethyl-formamide / 20 h / 23 °C
3.1: triphenylphosphine / 20 h / 110 °C / Green chemistry
3.2: Green chemistry
View Scheme
1,3-benzodioxol-5-ylmethyl methanesulfonate
78358-16-4

1,3-benzodioxol-5-ylmethyl methanesulfonate

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium azide / N,N-dimethyl-formamide / 20 h / 23 °C
2.1: triphenylphosphine / 20 h / 110 °C / Green chemistry
2.2: Green chemistry
View Scheme
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

acetic anhydride
108-24-7

acetic anhydride

N-(2H-benzo[3,4-d]-1,3-dioxolen-5-ylmethyl)acetamide
59682-83-6

N-(2H-benzo[3,4-d]-1,3-dioxolen-5-ylmethyl)acetamide

Conditions
ConditionsYield
100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

fenoxaprop-p-ethyl
66441-23-4, 71283-80-2

fenoxaprop-p-ethyl

A

Benzo[1,3]dioxol-5-ylmethyl-(6-chloro-benzooxazol-2-yl)-amine

Benzo[1,3]dioxol-5-ylmethyl-(6-chloro-benzooxazol-2-yl)-amine

B

(R)-2-(4-hydroxyphenoxy)propionic acid ethyl ester
71301-98-9

(R)-2-(4-hydroxyphenoxy)propionic acid ethyl ester

Conditions
ConditionsYield
at 20℃;A 100%
B n/a
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

2-(tert-butoxyoxalyl-amino)-5-formyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid tert-butyl ester
330193-46-9

2-(tert-butoxyoxalyl-amino)-5-formyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid tert-butyl ester

5-(((benzo[1,3]dioxol-5-ylmethyl)-amino)methyl)-2-(tert-butoxyoxalyl-amino)-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid tert-butyl ester
330193-47-0

5-(((benzo[1,3]dioxol-5-ylmethyl)-amino)methyl)-2-(tert-butoxyoxalyl-amino)-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 1h;100%
Stage #1: 1,3-benzodioxol-5-ylmethyl amine; 2-(tert-butoxyoxalyl-amino)-5-formyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid tert-butyl ester With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 1h;
Stage #2: With water; sodium hydrogencarbonate In 1,2-dichloro-ethane
100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

3-(N-cyclohexylamino)-4-[N-(4-methylphenyl)amino]-1H-isochromen-1-one
1208940-88-8

3-(N-cyclohexylamino)-4-[N-(4-methylphenyl)amino]-1H-isochromen-1-one

2-{2-[N-(3,4-methylenedioxy)benzyl]carbamoyl}phenyl-2-[N-(4-methyl)phenyl]aminoacetic acid N-cyclohexyl amide
1308652-45-0

2-{2-[N-(3,4-methylenedioxy)benzyl]carbamoyl}phenyl-2-[N-(4-methyl)phenyl]aminoacetic acid N-cyclohexyl amide

Conditions
ConditionsYield
at 20℃; for 24h; Inert atmosphere;100%
pyridine-2-carbaldehyde
1121-60-4

pyridine-2-carbaldehyde

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

1-(benzo[1,3]dioxol-5-yl)-N-(pyridin-2-yl-methylene)methanamine
1363649-33-5

1-(benzo[1,3]dioxol-5-yl)-N-(pyridin-2-yl-methylene)methanamine

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
In water at 20℃; Inert atmosphere;90%
Isopropenyl acetate
108-22-5

Isopropenyl acetate

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

N-(2H-benzo[3,4-d]-1,3-dioxolen-5-ylmethyl)acetamide
59682-83-6

N-(2H-benzo[3,4-d]-1,3-dioxolen-5-ylmethyl)acetamide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 1.5h; Green chemistry;100%
4-Methoxyphenylacetic acid
104-01-8

4-Methoxyphenylacetic acid

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-oxo-benzaldehyde
1185185-57-2

4-oxo-benzaldehyde

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

C29H30N2O6

C29H30N2O6

Conditions
ConditionsYield
Stage #1: 1,3-benzodioxol-5-ylmethyl amine; 4-oxo-benzaldehyde In methanol at 60℃; for 0.0833333h; Ugi Condensation; Microwave irradiation;
Stage #2: 4-Methoxyphenylacetic acid; tert-butylisonitrile In methanol at 60℃; for 3h; Ugi Condensation; Microwave irradiation;
100%
formic acid
64-18-6

formic acid

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-oxo-benzaldehyde
1185185-57-2

4-oxo-benzaldehyde

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

C21H22N2O5

C21H22N2O5

Conditions
ConditionsYield
Stage #1: 1,3-benzodioxol-5-ylmethyl amine; 4-oxo-benzaldehyde In methanol at 60℃; for 0.0833333h; Ugi Condensation; Microwave irradiation;
Stage #2: formic acid; tert-butylisonitrile In methanol at 60℃; for 3h; Ugi Condensation; Microwave irradiation;
100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

C15H12ClNO2

C15H12ClNO2

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
at 120℃;
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

benzaldehyde
100-52-7

benzaldehyde

N-benzylidene piperonylamine
112776-37-1

N-benzylidene piperonylamine

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
In benzene at 65℃; for 0.25h; Microwave irradiation;
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

C16H15NO2

C16H15NO2

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

meta-hydroxybenzaldehyde
100-83-4

meta-hydroxybenzaldehyde

C15H13NO3

C15H13NO3

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-fluorobenzaldehyde
459-57-4

4-fluorobenzaldehyde

C15H12FNO2

C15H12FNO2

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

3,4-dichlorobenzaldehyde
6287-38-3

3,4-dichlorobenzaldehyde

C15H11Cl2NO2

C15H11Cl2NO2

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

C15H12N2O4

C15H12N2O4

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
3-pyridinecarboxaldehyde
500-22-1

3-pyridinecarboxaldehyde

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

C14H12N2O2

C14H12N2O2

Conditions
ConditionsYield
In neat (no solvent) for 0.05h;100%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

piperonylonitrile
4421-09-4

piperonylonitrile

Conditions
ConditionsYield
With copper(I) chloride; 4 A molecular sieve; oxygen In pyridine at 60℃; for 24h;99%
With dmap; copper(l) iodide; 9-azabicyclo[3.3.1]nonane N-oxyl; oxygen; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; under 760.051 Torr; for 15h; Reagent/catalyst;97%
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 110℃; under 1500.15 Torr; for 15h; Autoclave; Green chemistry;93%
piperonal
120-57-0

piperonal

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

α-[(1,3-benzodioxol-5-ylmethyl)amino]-1,3-benzodioxol-5-acetonitrile

α-[(1,3-benzodioxol-5-ylmethyl)amino]-1,3-benzodioxol-5-acetonitrile

Conditions
ConditionsYield
With azaphosphatrane salt on Merrifield resin In acetonitrile at 20℃; for 12h; Strecker coupling;99%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

benzaldehyde
100-52-7

benzaldehyde

2-phenyl-2-(N-piperonylamino)acetonitrile

2-phenyl-2-(N-piperonylamino)acetonitrile

Conditions
ConditionsYield
With azaphosphatrane salt on Merrifield resin In acetonitrile at 20℃; for 8h; Strecker coupling;99%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

methyl 3-piperonylaminopropionate
91641-91-7

methyl 3-piperonylaminopropionate

Conditions
ConditionsYield
With azaphosphatrane salt on Merrifield resin In acetonitrile at 20℃; for 24h; Michael addition;99%
With Pseudomonas fluorescence lipase immobilized on hyroxypropyl methyl cellulose support In toluene at 50℃; for 3.5h; Reagent/catalyst; Michael Addition; Enzymatic reaction; chemoselective reaction;
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

1-(1-naphthylmethyl)-4-methoxycarbonylpiperidine
1233939-82-6

1-(1-naphthylmethyl)-4-methoxycarbonylpiperidine

1-(1-naphthylmethyl)-4-[3,4-(methylenedioxy)benzylamino]carbonylpiperidine
1233939-91-7

1-(1-naphthylmethyl)-4-[3,4-(methylenedioxy)benzylamino]carbonylpiperidine

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 23℃; Inert atmosphere;99%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

C15H20N2O4

C15H20N2O4

Conditions
ConditionsYield
In acetonitrile at 50℃; for 18h;99%
formaldehyd
50-00-0

formaldehyd

1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

N-(benzo[d][1,3]dioxol-5-ylmethyl)-3-(trimethylsilyl)-N-(3-(trimethylsilyl)prop-2-yn-1-yl)prop-2-yn-1-amine

N-(benzo[d][1,3]dioxol-5-ylmethyl)-3-(trimethylsilyl)-N-(3-(trimethylsilyl)prop-2-yn-1-yl)prop-2-yn-1-amine

Conditions
ConditionsYield
With Echavarren's catalyst In dichloromethane; water at 50℃; under 1500.15 Torr; for 1h; Inert atmosphere;99%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

carbon monoxide
201230-82-2

carbon monoxide

1,3-bis(benzo[d][1,3]dioxol-5-ylmethyl)urea
113260-75-6

1,3-bis(benzo[d][1,3]dioxol-5-ylmethyl)urea

Conditions
ConditionsYield
With 2C7H9N4*Au(1+)*Cu(1+)*2I(1-) In toluene at 60℃; Autoclave;98%
With copper diacetate; air; palladium diacetate In toluene under 760 Torr; for 2h; Heating;82%
With C62H52AgAu4N2O4P4(3+)*3F6Sb(1-) In tetrahydrofuran at 60℃; under 3750.38 Torr; for 24h; Inert atmosphere;78%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

5-isocyanato-1,3-benzodioxole
69922-28-7

5-isocyanato-1,3-benzodioxole

1-(3,4-methylenedioxyphenyl)-3-(3,4-methylenediobenzyl) urea

1-(3,4-methylenedioxyphenyl)-3-(3,4-methylenediobenzyl) urea

Conditions
ConditionsYield
In benzene for 1h; Heating / reflux;98%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

diisopropylamine
108-18-9

diisopropylamine

N-(benzo[1,3]dioxol-5-ylmethyl)propan-2-amine
68291-92-9

N-(benzo[1,3]dioxol-5-ylmethyl)propan-2-amine

Conditions
ConditionsYield
With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium) In 5,5-dimethyl-1,3-cyclohexadiene at 155℃; for 10h; Inert atmosphere;98%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

4-diphenylsulfonyl chloride
1623-93-4

4-diphenylsulfonyl chloride

N-(1,3-benzodioxol-5-ylmethyl)-4-diphenylsulfonamide

N-(1,3-benzodioxol-5-ylmethyl)-4-diphenylsulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 4h; Reflux;98%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

6-chloro-2-iodo-9-isopropyl-9H-purine
207220-30-2

6-chloro-2-iodo-9-isopropyl-9H-purine

(2-iodo-9-isopropyl-9H-purin-6-yl)(3,4-methylenedioxybenzyl)amine
267885-20-1

(2-iodo-9-isopropyl-9H-purin-6-yl)(3,4-methylenedioxybenzyl)amine

Conditions
ConditionsYield
With triethylamine In ethanol at 50℃; Substitution;97%
1,3-benzodioxol-5-ylmethyl amine
2620-50-0

1,3-benzodioxol-5-ylmethyl amine

trifluoroacetic acid
76-05-1

trifluoroacetic acid

N-benzylthiourea
621-83-0

N-benzylthiourea

N-benzo[1,3]dioxol-5-ylmethyl-N'-benzylguanidinium trifluoroacetate

N-benzo[1,3]dioxol-5-ylmethyl-N'-benzylguanidinium trifluoroacetate

Conditions
ConditionsYield
Stage #1: N-benzylthiourea With bromomethyl resin In dichloromethane; N,N-dimethyl-formamide at 50℃; for 4h; solid phase reaction;
Stage #2: 1,3-benzodioxol-5-ylmethyl amine In dichloromethane; N,N-dimethyl-formamide at 50℃; for 20h;
Stage #3: trifluoroacetic acid
97%

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