Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:4595-59-9
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryItems Standard Result Assay 98%min ---------------------------------------------------------------------------------------------
Cas:4595-59-9
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryGood quality 5-Bromopyrimidine CAS 4595-59-9 with cheap price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additiv
Cas:4595-59-9
Min.Order:1 Gram
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Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Product description: Product name 5-Bromopyrimidine CAS number 4595-59-9 Assay ≥99% Appearance Off-white to yellowish crystal Capacity 100mt/year Application Organic Interme
Cas:4595-59-9
Min.Order:10 Gram
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inquiry5-Bromopyrimidine CAS No: 4595-59-9 Molecular Structure: Specifications: Item Details Appearance similar white to light yellow crystal
Cas:4595-59-9
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Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:4595-59-9
Min.Order:5 Kiloliter
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inquiryTIANFUCHEM--4595-59-9--5-Bromopyrimidine factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business rela
Cas:4595-59-9
Min.Order:1 Metric Ton
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:4595-59-9
Min.Order:10 Kilogram
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Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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Min.Order:1 Kilogram
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Type:Trading Company
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry plac
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry5-Bromopyrimidine CAS:4595-59-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:4595-59-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:4595-59-9
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryPRODUCT DETAILS
Cas:4595-59-9
Min.Order:1000 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
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Type:Trading Company
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:4 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:4595-59-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With boron trioxide In methanol at 180 - 185℃; for 15h; | 48% |
A
5-bromopyrimidine
B
indole
C
3-(5-bromopyrimidin-4-yl)-1H-indole
D
3-(pyrimidin-4-yl)-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide; potassium hexacyanoferrate(III) In water at 20℃; for 2h; | A 8 %Chromat. B 12 %Chromat. C 40% D 17 %Chromat. |
A
5-bromopyrimidine
B
N-Ethylindole
C
3-(5-Bromopyrimidin-4-yl)-1-ethyl-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide; potassium hexacyanoferrate(III) In water at 20℃; for 2h; | A 9 %Chromat. B 25 %Chromat. C 40% |
Conditions | Yield |
---|---|
With piperidine In water at 20℃; for 2h; | A 22 %Chromat. B 35 %Chromat. C 23% |
5-bromo-2-pyrimidinecarboxylic acid
5-bromopyrimidine
Conditions | Yield |
---|---|
at 250℃; |
pyrimidine hydrochloride
5-bromopyrimidine
Conditions | Yield |
---|---|
With bromine at 160℃; | |
With bromine; sodium carbonate In water; nitrobenzene; benzene |
2,4-dichloro-5-bromopyrimidine
5-bromopyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In diethyl ether; butan-1-ol |
5-bromo-2-iodopyrimidine
5-bromo-2-(5-bromothiophen-2-yl)pyridine
A
5-bromopyrimidine
B
5-bromo-2-(thiophen-2-yl)pyridine
Conditions | Yield |
---|---|
Stage #1: 5-bromo-2-iodopyrimidine; 5-bromo-2-(5-bromothiophen-2-yl)pyridine With isopropylmagnesium chloride In tetrahydrofuran Stage #2: Hydrolysis; |
5-bromopyrimidine
ethanol
carbon monoxide
ethyl pyrimidine-5-carboxylate
Conditions | Yield |
---|---|
With triethylamine; bis-triphenylphosphine-palladium(II) chloride at 100℃; under 5171.5 Torr; | 100% |
Conditions | Yield |
---|---|
With caesium carbonate; palladium diacetate In N,N-dimethyl-formamide at 80℃; for 6h; Suzuki-Miyaura cross-coupling reaction; | 100% |
With potassium carbonate In ethanol; water at 30℃; for 1h; Suzuki-Miyaura Coupling; | 100% |
With N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine; potassium carbonate; palladium dichloride In 1,4-dioxane; N,N-dimethyl-formamide at 90℃; for 6h; Suzuki coupling; Inert atmosphere; | 99% |
5-bromopyrimidine
1-t-Butoxycarbonylpiperazine
tert-butyl 4-(pyrimidin-5-yl)piperazine-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: 5-bromopyrimidine; 1-t-Butoxycarbonylpiperazine With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In xylene at 50℃; Stage #2: With macroporous polymer-supported isocyanate In xylene at 50℃; for 24h; | 100% |
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 90℃; for 12h; | 58.7% |
Stage #1: 5-bromopyrimidine; 1-t-Butoxycarbonylpiperazine With sodium t-butanolate In toluene for 0.25h; Heating / reflux; Stage #2: palladium diacetate; tri-tert-butyl phosphine for 32h; Heating / reflux; | |
With tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene for 16h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium phosphate dodecahydrate; palladium 10% on activated carbon In isopropyl alcohol at 80℃; for 12h; hetero-Suzuki-Miyaura cross-coupling; Inert atmosphere; | 100% |
With sodium phosphate; palladium on activated charcoal In isopropyl alcohol at 80℃; for 3h; Suzuki-Miyaura coupling reaction; | 95% |
With C43H37ClFeNiP2*C4H8O; potassium carbonate In tetrahydrofuran; acetonitrile at 50℃; for 12h; Suzuki-Miyaura Coupling; Inert atmosphere; | 89% |
With tetra-butylammonium acetate; Pd EnCat-30TM In ethanol at 120℃; for 0.166667h; Suzuki cross-coupling; microwave irradiation; | 72% |
Conditions | Yield |
---|---|
With potassium phosphate monohydrate; C66H84O10P2Pd In water; toluene at 45℃; for 4.5h; Reagent/catalyst; Suzuki-Miyaura Coupling; Inert atmosphere; | 100% |
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In ethanol at 40℃; for 4h; Suzuki-Miyaura Coupling; Green chemistry; | 99% |
With potassium carbonate In water; toluene at 90℃; for 0.5h; Suzuki-Miyaura Coupling; | 97% |
5-bromopyrimidine
(4,4-difluoro-piperidin-1-yl)-[5-(1-isopropyl-piperidin-4-yloxy)-1H-indol-2-yl]-methanone
Conditions | Yield |
---|---|
Stage #1: 5-bromopyrimidine; (4,4-difluoro-piperidin-1-yl)-[5-(1-isopropyl-piperidin-4-yloxy)-1H-indol-2-yl]-methanone With potassium phosphate; (S,S)-1,2-diaminocyclohexane; copper(l) iodide In 1,4-dioxane for 72h; Heating / reflux; Stage #2: With potassium carbonate In 1,4-dioxane for 24h; Heating / reflux; | 100% |
5-bromopyrimidine
2-formylbenzene boronic acid
2-(pyrimidin-5-yl)benzaldehyde
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water Suzuki coupling; Heating; | 100% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In methanol; 1,2-dimethoxyethane; water at 80℃; | 70% |
With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride In water; acetonitrile at 150℃; for 0.0833333h; Microwave irradiation; | |
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In water; acetonitrile at 150℃; for 0.0833333h; Sealed tube; Microwave irradiation; | 220 mg |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 5-(di(adamantan-1-yl)phosphino)-1′,3′,5′-triphenyl-1′H-1,4′-bipyrazole; potassium phenolate In 1,4-dioxane at 100℃; for 6h; Sealed tube; Inert atmosphere; | 100% |
5-bromopyrimidine
2-methoxypyridin-3-yl-boronic acid
3-(pyrimidin-5-yl)thiophene
Conditions | Yield |
---|---|
With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride In tert-Amyl alcohol for 12h; Solvent; Suzuki-Miyaura Coupling; Heating; | 100% |
5-bromopyrimidine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane at 100℃; for 16h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In dichloromethane at 50℃; for 15h; Sonogashira Cross-Coupling; Inert atmosphere; | 99% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine; lithium chloride In water for 2h; Sonogashira coupling; Reflux; Inert atmosphere; | 83% |
With copper(l) iodide; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In N,N-dimethyl-formamide at 100℃; for 20h; | 75% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In dichloromethane for 2h; Heating; | |
With tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride at 80℃; Castro-Stevens reaction; |
Conditions | Yield |
---|---|
With cesium acetate; copper In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | 99% |
With dibenzylphosphoramidous acid 1,1'-binaphthyl-2,2'-diyl ester; caesium carbonate; copper(I) bromide In N,N-dimethyl-formamide at 90℃; for 36h; | 96% |
With dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; palladium diacetate; potassium carbonate In tert-butyl alcohol at 110℃; for 24h; Catalytic behavior; Reagent/catalyst; Buchwald-Hartwig Coupling; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With water; palladium diacetate; sodium carbonate at 80℃; for 4h; Suzuki Coupling; Green chemistry; | 99% |
With palladium diacetate; sodium carbonate; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate In water at 80℃; for 6h; Suzuki-Miyaura Coupling; | 99% |
With palladium diacetate; sodium carbonate In ethanol; water at 80℃; for 4h; Suzuki-Miyaura Coupling; | 98% |
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) In acetonitrile at 60℃; for 6h; Sonogashira coupling reaction; | 99% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; nickel(II) bromide dimethoxyethane; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate In dimethyl sulfoxide at 80℃; for 0.166667h; Flow reactor; Sealed tube; Schlenk technique; Inert atmosphere; Irradiation; | 99% |
Stage #1: pyrrolidine; 5-bromopyrimidine With nickel(II) chloride hexahydrate; cadmium(II) sulphide In N,N-dimethyl acetamide for 0.00277778h; Schlenk technique; Sonication; Stage #2: In N,N-dimethyl acetamide at 20℃; for 24h; Schlenk technique; Irradiation; | 98% |
With dibenzylphosphoramidous acid 1,1'-binaphthyl-2,2'-diyl ester; caesium carbonate; copper(I) bromide In N,N-dimethyl-formamide at 90℃; for 36h; | 83% |
With sodium t-butanolate; XPhos; tris(dibenzylideneacetone)dipalladium (0) In toluene at 100℃; for 15h; | 48% |
5-bromopyrimidine
4-methylphenylboronic acid
5-(4-methyl phenyl)pyrimidine
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In ethylene glycol at 80℃; for 0.116667h; Suzuki coupling; | 99% |
With potassium phosphate tribasic heptahydrate; palladium diacetate In isopropyl alcohol at 80℃; for 0.5h; Suzuki coupling; | 97% |
With potassium phosphate tribasic heptahydrate; palladium dichloride In ethanol; water at 80℃; for 1h; Suzuki-Miyaura reaction; | 93% |
5-bromopyrimidine
(1S,4S)-2,5-Diaza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
99% | |
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 80 - 85℃; for 5h; | 91% |
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene at 80 - 85℃; for 5h; | 91% |
5-bromopyrimidine
4-formylphenylboronic acid,
4-(pyrimidin-5-yl)benzaldehyde
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 90℃; for 18h; Suzuki Coupling; | 99% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate monohydrate In 1,2-dimethoxyethane; water at 90℃; Suzuki Coupling; Inert atmosphere; |
5-bromopyrimidine
4-n-methylphenylacetylene
5-((4-methylphenyl)ethynyl)pyrimidine
Conditions | Yield |
---|---|
With copper(l) iodide; potassium tetrachloropalladate(II); N,N,N,N,-tetramethylethylenediamine; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl acetamide at 50℃; for 48h; Sonogashira Cross-Coupling; Inert atmosphere; | 82% |
With 1,4-diaza-bicyclo[2.2.2]octane In water at 100℃; for 48h; Catalytic behavior; Sonogashira Cross-Coupling; | 77% |
With copper(l) iodide; Pd(t-Bu3P)2; diethylamine In N,N-dimethyl-formamide at 70℃; for 0.166667h; Sonogashira coupling; Microwave irradiation; | |
With potassium carbonate In water; N,N-dimethyl-formamide at 100℃; for 4h; Sonogashira Cross-Coupling; | 97 %Chromat. |
Conditions | Yield |
---|---|
With dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); triethylamine In water at 20℃; for 6h; Suzuki-Miyaura coupling; Inert atmosphere; | 99% |
With 1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; Ni(4-CF3stb)3 In 1,4-dioxane at 80℃; for 8h; Inert atmosphere; | 99% |
With 1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; Ni(COD)(DQ) In 1,4-dioxane at 80℃; for 8h; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere; | 98% |
5-bromopyrimidine
4-methoxyphenylacetylen
5-((4-methoxyphenyl)ethynyl)pyrimidine
Conditions | Yield |
---|---|
With copper(l) iodide; potassium tetrachloropalladate(II); N,N,N,N,-tetramethylethylenediamine; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; Ni(COD)(DQ) In 1,4-dioxane at 80℃; for 8h; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere; | 99% |
With potassium phosphate; NiCl2(PCy3)2 In 2-methyltetrahydrofuran at 100℃; for 12h; Solvent; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; Sealed tube; | 97% |
With potassium phosphate; C28H31ClN2Ni; triphenylphosphine In toluene; tert-butyl alcohol at 90℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Sealed tube; | 94% |
5-bromopyrimidine
(4-chlorophenyl)zinc(II) chloride
5-(4-chlorobenzyl)pyrimidine
Conditions | Yield |
---|---|
With lithium chloride; bis(triphenylphosphine)nickel(II) chloride In tetrahydrofuran at 0℃; for 5h; Product distribution / selectivity; | 99% |
5-bromopyrimidine
2-benzofuranylboronic acid mida ester
Conditions | Yield |
---|---|
With dichloro[1,1′-bis[bis(1,1-dimethylethyl)phosphino]ferrocene-P,P′]palladium; TPGS-750-M; triethylamine In water at 20℃; Inert atmosphere; | 99% |
With dichloro[1,1′-bis[bis(1,1-dimethylethyl)phosphino]ferrocene-P,P′]palladium; triethylamine In water at 20℃; for 6h; Suzuki Coupling; | 90% |
5-bromopyrimidine
4-methyl-2,6-dioxo-8-phenylhexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide
5-phenylpyrimidine
Conditions | Yield |
---|---|
With potassium phosphate; [Pd(η(5)-C5H5)Fe(η(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)] In ethanol; water at 90℃; for 12h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; Green chemistry; | 99% |
5-bromopyrimidine
pyrimidine-5-carbonitrile
Conditions | Yield |
---|---|
With Palladium Nanoparticles with two shape-persistent covalent cages CC1' In N,N-dimethyl-formamide at 140℃; for 15h; Reagent/catalyst; Inert atmosphere; | 99% |
5-bromopyrimidine
S-(4-methoxyphenyl)-S-methylsulfoximine
Conditions | Yield |
---|---|
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; nickel(II)-4,4'-di(tert-butyl-2,2'-bipyridine) bromide; N,N,N',N'-tetramethylguanidine In N,N-dimethyl acetamide at 25℃; for 17h; Sealed tube; Inert atmosphere; Irradiation; | 99% |
5-bromopyrimidine
Conditions | Yield |
---|---|
With potassium phosphate monohydrate; C50H60F3NO6PPdS In water at 55℃; for 5h; Suzuki-Miyaura Coupling; | 99% |
5-bromopyrimidine
Conditions | Yield |
---|---|
With [Pd(IPr*IMe)An(3-Cl-pyridinyl)Cl2]; potassium carbonate; Trimethylacetic acid In N,N-dimethyl acetamide at 130℃; for 12h; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With sodium carbonate; palladium 10% on activated carbon for 24h; Heating / reflux; | 98.7% |
With Tedicyp; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In xylene at 130℃; for 20h; Suzuki cross-coupling reaction; | 80% |
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