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Min.Order:1 Kilogram
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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Benzyl methyl ether cas 538-86-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
2,6-di-tert-butyl-4-methylpyridine
methyltriphenylbismuthonium tetrafluoroborate
benzyl alcohol
A
benzyl methyl ether
B
2,6-di-tert-butyl-4-methylpyridinium tetrafluoroborate
C
triphenylbismuthane
Conditions | Yield |
---|---|
In chloroform-d1 Kinetics; alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR; | A 95% B 100% C 100% |
Conditions | Yield |
---|---|
With 1,1,3,3-Tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; | 99% |
With trimethylsilan; trimethylsilyl trifluoromethanesulfonate In dichloromethane 0 deg C, 30 min. then 28 deg C, 13 h.; | 96% |
With triethylsilane; Nafion-H (perfluororesinsulfonic acid) In dichloromethane for 2h; Heating; | 96% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide 1.) 0 deg C, 1 h, 2.) 25 deg C, 24 h; | 99% |
Conditions | Yield |
---|---|
Stage #1: benzyl alcohol With potassium carbonate In acetone for 0.25h; Stage #2: dimethyl sulfate In acetone for 15h; Reflux; | 97% |
With sodium hydroxide; zirconium (benzyldiethylammoniomethylphosphonate chloride) phosphate In ethanol; water; Petroleum ether at 42℃; for 8h; | 80.1% |
With sodium hydroxide at 40℃; |
methanol
carbon monoxide
benzyl chloride
A
benzyl methyl ether
B
sodium phenylacetate
Conditions | Yield |
---|---|
With sodium hydroxide; dicobalt octacarbonyl at 60 - 65℃; under 760.051 - 2280.15 Torr; | A n/a B 97% |
Conditions | Yield |
---|---|
With Decaborane at 20℃; for 22h; reductive etherification; | 96% |
With phenyltellurotrimethylsilane; zinc(II) iodide In benzene for 3h; Ambient temperature; | 89 % Chromat. |
Conditions | Yield |
---|---|
With copper(II) bis(tetrafluoroborate) In acetonitrile for 1.5h; Irradiation; | 94% |
benzyltributyltin
benzyl methyl ether
Conditions | Yield |
---|---|
With methanol; copper(II) bis(tetrafluoroborate) In acetonitrile Irradiation (UV/VIS); 1.5 h, λ > 200 nm; | 94% |
Conditions | Yield |
---|---|
With copper(ll) bromide at 175℃; for 10h; Inert atmosphere; Sealed tube; | A 93% B 7% |
With phosphoric acid at 350℃; under 36775.4 Torr; | |
With Cp*Ir(Cl)2(nBu2Im); silver trifluoromethanesulfonate at 110℃; for 12h; | A 88 %Spectr. B 6 %Spectr. |
Conditions | Yield |
---|---|
With iron(II) sulfate at 75℃; for 12h; | 92% |
Stage #1: methanol With potassium hydride In tetrahydrofuran at 25℃; for 8h; Metallation; Stage #2: benzyl bromide In tetrahydrofuran Alkylation; | 85% |
With silver(II) oxide at 0℃; | 82% |
Conditions | Yield |
---|---|
With bismuth(III) bromide In tetrachloromethane at 25℃; for 8h; Etherification; | 92% |
Stage #1: methanol With 15-crown-5; potassium In tetrahydrofuran at 25℃; Stage #2: benzyl alcohol In tetrahydrofuran | 25% |
Stage #1: benzyl alcohol With titanium tetrachloride In chloroform at 20℃; for 0.0166667h; Molecular sieve; Stage #2: methanol In chloroform for 72h; Reflux; | 20% |
Conditions | Yield |
---|---|
With iodine at 20℃; for 0.5h; | 92% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 16h; | 91% |
With sodium hydride; 1-n-butyl-2,3-dimethylimidazolium hexafluorophosphate at 25℃; for 2h; Williamson synthesis; | 91% |
With iron(III) perchlorate at 20℃; for 1h; neat (no solvent); | 90% |
benzyl methoxymethyl ether
benzyl methyl ether
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; zinc(II) tetrahydroborate In diethyl ether; dichloromethane at 25℃; for 40h; | 90% |
Conditions | Yield |
---|---|
With iodine at 20℃; for 0.583333h; | 90% |
With Montmorillonite KSF for 12h; Ambient temperature; | 83% |
Conditions | Yield |
---|---|
With iron(III) chloride at 146.84℃; for 6h; Reagent/catalyst; | 89.3% |
Conditions | Yield |
---|---|
With silver(II) oxide Ambient temperature; | 89% |
With benzyltrimethylammonium chloride for 0.0833333h; Heating; Irradiation; | 87% |
With potassium hydroxide |
Conditions | Yield |
---|---|
With sodium hydroxide; cobalt tetracarbonyl anion In methanol at 55℃; for 4h; | A 10% B 85% |
6,7-diazatricyclo<3.2.2.02,4>nona-6,8-diene N-oxide
A
benzyl methyl ether
B
benzyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol Mechanism; Ambient temperature; | A n/a B 85% |
Conditions | Yield |
---|---|
With aluminium(III) triflate; tris(2,4-pentanedionato)ruthenium(III); hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In toluene at 160℃; under 45603.1 Torr; for 24h; Autoclave; | 84% |
Trimethyl orthoacetate
benzyl alcohol
A
benzyl methyl ether
B
Benzyl acetate
Conditions | Yield |
---|---|
Montmorillonite KSF at 20℃; for 12h; | A 83% B 4% |
Conditions | Yield |
---|---|
Stage #1: (dimethoxy)methylsilane; benzaldehyde With dicarbonyl(pentamethylcyclopentadienyl)(4-methoxyphenyl)iron In dichloromethane for 4h; Inert atmosphere; Irradiation; Schlenk technique; Stage #2: With sodium hydroxide In methanol; water Schlenk technique; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 59 - 70℃; for 48h; | 80% |
Conditions | Yield |
---|---|
With 2,4,6-triphenylpyrilium perchlorate In acetonitrile for 0.166667h; Irradiation; | 80% |
Conditions | Yield |
---|---|
With tetrachloromethane; bis(acetylacetonate)oxovanadium; triethylamine at 175℃; for 14h; Inert atmosphere; Autoclave; | A 80% B 10% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 1h; Heating; reduction failed; | A 79% B 61% |
With lithium aluminium tetrahydride In diethyl ether for 1h; Reflux; | A 79% B 61% |
methanol
(S)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-3-(4-hydroxy-phenyl)-propionic acid
A
benzyl methyl ether
B
L-tyrosine
Conditions | Yield |
---|---|
With potassium hydroxide; [bis(acetoxy)iodo]benzene at 0 - 5℃; for 1.5h; | A 78% B n/a |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Stage #2: chloromethyl methyl ether In tetrahydrofuran at -78 - 0℃; for 2h; | 76% |
With diethyl ether; sodium |
Conditions | Yield |
---|---|
Stage #1: phenol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.25h; Inert atmosphere; Schlenk technique; Stage #2: chloromethyl methyl ether In tetrahydrofuran at 0 - 25℃; for 2h; Inert atmosphere; Schlenk technique; | 76% |
methanol
C13H18ClNO3
A
benzyl methyl ether
B
3-nitroso-3-methylbutanoic acid methyl ester
C
benzyl chloride
D
C14H21NO4
Conditions | Yield |
---|---|
With triethylamine 1.) -20 deg C, 6 h, 2.) 20 deg C, 1 h; | A n/a B 24% C n/a D 75% |
Conditions | Yield |
---|---|
With iron In 1,2-dichloro-ethane at 80℃; for 7h; Schlenk technique; Inert atmosphere; regioselective reaction; | 99% |
With molybdenum(V) chloride In 1,2-dichloro-ethane at 80℃; for 3h; | 82% |
Conditions | Yield |
---|---|
1,1'-bis-(diphenylphosphino)ferrocene; [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; potassium iodide In diethyl ether; toluene at 80℃; for 10h; | 99% |
Conditions | Yield |
---|---|
With palladium dichloride In methanol at 40℃; for 12h; Inert atmosphere; Green chemistry; chemoselective reaction; | 99% |
With methanol; toluene-4-sulfonic acid at 25℃; for 7.5h; Reagent/catalyst; Inert atmosphere; Sealed tube; UV-irradiation; | 95% |
With samarium diiodide; water In tetrahydrofuran; decane at 20℃; | |
With diisobutylaluminium hydride; sodium t-butanolate; bis(1,5-cyclooctadiene)nickel(0); 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In tetrahydrofuran at 80℃; for 16h; Product distribution / selectivity; Inert atmosphere; | 82 %Chromat. |
Conditions | Yield |
---|---|
With fac-tris(2-(4,6-difluorophenyl)pyridinato,N,C(2'))iridium(III); N-[3,5-bis(trifluoromethyl)phenyl]-2,4,6-triisopropylbenzenesulfonamide; potassium carbonate In acetone at 40℃; for 24h; Sealed tube; Inert atmosphere; Irradiation; | 99% |
With tris[2-phenylpyridinato-C2,N]iridium(III); dipotassium hydrogenphosphate; Octanal; Methyl thioglycolate In N,N-dimethyl acetamide at -78 - 23℃; for 12h; Reagent/catalyst; Solvent; Irradiation; Inert atmosphere; | 77% |
With thiobenzoic acid; potassium phosphate In N,N-dimethyl acetamide at 20℃; for 6h; Irradiation; | 55% |
Conditions | Yield |
---|---|
With hydrogen In n-heptane at 160℃; under 750.075 Torr; for 6h; Catalytic behavior; Temperature; | A 93% B 98% |
benzyl methyl ether
(4-chlorphenyl)magnesium bromide
1-chloro-4-(methoxy(phenyl)methyl)benzene
Conditions | Yield |
---|---|
Stage #1: benzyl methyl ether With 2,3-dicyano-5,6-dichloro-p-benzoquinone In chlorobenzene at 80℃; for 1.5h; Inert atmosphere; Stage #2: (4-chlorphenyl)magnesium bromide In chlorobenzene at 0℃; for 3h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen In acetonitrile at 80℃; for 12h; | 95% |
With tert.-butylhydroperoxide; C45H52CuN4O3 In decane; acetonitrile at 70℃; for 18h; | 93% |
With sodium periodate; ruthenium trichloride In tetrachloromethane; water; acetonitrile for 8h; Ambient temperature; | 89% |
benzyl methyl ether
5-nitroindole
3,3′-benzylidenebis(5-nitro-1H-indole)
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; iron(II) chloride at 80℃; for 1h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
Stage #1: benzyl methyl ether With 2,3-dicyano-5,6-dichloro-p-benzoquinone In chlorobenzene at 80℃; for 1.5h; Inert atmosphere; Stage #2: 4-flourophenylmagnesium bromide In chlorobenzene at 0℃; for 3h; Inert atmosphere; | 94% |
benzyl methyl ether
α-azidobenzyl methyl ether
Conditions | Yield |
---|---|
With iodine(I) azide In acetonitrile for 0.416667h; Heating; | 93% |
With [bis(acetoxy)iodo]benzene; trimethylsilylazide In acetonitrile at 0 - 25℃; | 88% |
With polystyrene supported diazidoiodate(I) In acetonitrile at 83℃; for 4h; | 68% |
benzyl methyl ether
anthranilic acid amide
2-phenyl-4(3H)-quinazolinone
Conditions | Yield |
---|---|
With oxygen In dimethyl sulfoxide at 120℃; under 760.051 Torr; for 12h; Temperature; Solvent; Schlenk technique; Sealed tube; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With iron(III) perchlorate hydrate In neat (no solvent) at 100℃; for 2h; Ritter Amidation; | 92% |
Conditions | Yield |
---|---|
With iron(III) perchlorate hydrate In neat (no solvent) at 100℃; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Ritter Amidation; | 91% |
With iron(III) chloride for 12h; Ritter reaction; Heating; | 22% |
Conditions | Yield |
---|---|
iron(III) chloride at 90℃; for 12h; Friedel-Crafts reaction; | 90% |
Conditions | Yield |
---|---|
With iron(III) perchlorate hydrate In neat (no solvent) at 100℃; for 2h; Ritter Amidation; | 90% |
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