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Cas:606-45-1
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inquiryProduct description: Product name Methyl 2-methoxybenzoate CAS number 606-45-1 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Pharmaceutical intermedi
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inquiryProduct name 2-Methoxybenzoic acid ethyl ester CAS 7335-26-4 Synonyms ETHYL O-ANISATE Molecular formula C10H12O3 Molecular weight 1
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inquiryProduct Name: Methyl 2-methoxybenzoate CAS: 606-45-1 MF: C9H10O3 MW: 166.17 EINECS: 210-118-6 Mol File: 606-45-1.mol Methyl 2-methoxybenzoate Structure Methyl 2-methoxybenzoate Chemical Properties Boiling point 248 °C (lit
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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Methyl 2-methoxybenzoate cas 606-45-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 50 - 60℃; for 27h; Time; Large scale; | 99% |
With potassium carbonate In acetone at 0 - 10℃; for 4h; Reflux; Inert atmosphere; | 91.1% |
With potassium carbonate In acetone at 20℃; for 3.16667h; Heating / reflux; | 80% |
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; for 18h; Cooling with ice; Inert atmosphere; | 99% |
With Oxone In toluene at 60℃; for 48h; Green chemistry; | 97% |
With 2-(dimethoxymethylidene)propanedinitrile at 60℃; for 48h; | 95% |
methanol
2-bromoanisole
carbon monoxide
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With dichloro[2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II); triethylamine at 100℃; under 2585.74 Torr; for 16h; | 99% |
2-Methoxybenzoic acid
carbonic acid dimethyl ester
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With 5 wt percent zeolite NaY-Bf at 200℃; for 5h; Autoclave; Green chemistry; | 98% |
With potassium carbonate In dimethyl sulfoxide at 90℃; for 16h; Inert atmosphere; Green chemistry; | 96% |
carbonic acid dimethyl ester
salicylic acid
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With diiron nonacarbonyl at 180℃; for 1h; Sealed tube; | 97% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide for 0.0208333h; microwave irradiation; | 92% |
With potassium carbonate at 150℃; for 10h; |
Conditions | Yield |
---|---|
With perchloric acid; sodium percarbonate; vanadia for 1.3h; Cooling; | 96% |
With dihydrogen peroxide at 20℃; for 20h; | 95% |
With aluminium(III) chloride hexahydrate; urea hydrogen peroxide adduct at 60℃; Green chemistry; | 90% |
methanol
4-iodoanisol
carbon monoxide
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine at 100℃; under 3750.38 Torr; for 1.5h; Inert atmosphere; | 96% |
With triethylamine; palladium on activated charcoal at 130℃; under 3750.38 Torr; for 2h; Sonogashira coupling; | 77% |
With triethylamine; G1-C2 PAMAM dendrimer*PPh2*PdCl2 at 105℃; under 5171.62 Torr; for 19h; | 100 % Chromat. |
Conditions | Yield |
---|---|
With bismuth(III) chloride; palladium diacetate; potassium carbonate at 20℃; for 2h; chemoselective reaction; | 95% |
With sodium methylate; potassium iodide at 15℃; Electrochemical reaction; | 85% |
With oxygen; potassium carbonate at 70℃; under 750.075 Torr; for 48h; | 53% |
Conditions | Yield |
---|---|
With potassium hydroxide In water at 15 - 20℃; Concentration; Temperature; | 94% |
With sodium hydroxide In water at 20 - 25℃; Temperature; | 94% |
With sodium hydroxide In water at 11 - 20℃; Temperature; Cooling; | 94% |
methyl 2-hydroxy-5-nitrobenzoate
2-Methoxybenzoic acid
A
2-methoxybenzoic acid methyl ester
B
5-nitrosalicylic acid
Conditions | Yield |
---|---|
Stage #1: 2-Methoxybenzoic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl 2-hydroxy-5-nitrobenzoate at 110℃; for 24h; | A 93% B n/a |
2-Methoxybenzoic acid
methyl salicylate
A
2-methoxybenzoic acid methyl ester
B
salicylic acid
Conditions | Yield |
---|---|
Stage #1: 2-Methoxybenzoic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl salicylate at 110℃; for 24h; Solvent; Reagent/catalyst; Temperature; | A 92% B n/a |
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating; | 91% |
With silver(l) oxide; benzene | |
With potassium hydroxide; Aliquat 336 1.) 60 deg C, 0.1 Torr, 6 h, 2.) room temp., 24 h; Yield given. Multistep reaction; | |
With potassium carbonate In N,N-dimethyl-formamide at 90℃; | |
With potassium carbonate In acetone at 20℃; Reflux; Darkness; |
methanol
N-(2-methoxybenzoyl)-N-phenylhydroxylamine
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With sodium perchlorate In acetonitrile electrolysis; | 87% |
Methyltrimethoxysilan
o-iodo-methyl-benzoic acid
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With oxygen; copper diacetate; caesium carbonate In N,N-dimethyl-formamide at 145℃; under 760.051 Torr; for 18h; | 86% |
Methoxytrimethylsilane
2-bromobenzoic acid methyl ester
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With oxygen; copper diacetate; caesium carbonate In N,N-dimethyl-formamide at 145℃; under 760.051 Torr; for 18h; | 86% |
Conditions | Yield |
---|---|
In dichloromethane for 2h; Heating; | 85% |
With pyridine for 2h; Yield given; | |
With triethylamine In dichloromethane at 0℃; | |
With triethylamine In dichloromethane at 0℃; Inert atmosphere; | 1.56 g |
methanol
2-bromoanisole
carbon monoxide
A
2-methoxybenzoic acid methyl ester
B
2-Methoxybenzoic acid
Conditions | Yield |
---|---|
With tert-Amyl alcohol; sodium hydride; cobalt(II) acetate In tetrahydrofuran at 40℃; under 760 Torr; for 20h; Irradiation; | A 84.5% B 8% |
2-bromoanisole
carbon monoxide
A
2-methoxybenzoic acid methyl ester
B
2-Methoxybenzoic acid
Conditions | Yield |
---|---|
With methanol; tert-Amyl alcohol; sodium hydride; cobalt(II) acetate In tetrahydrofuran at 40℃; under 760 Torr; for 20h; Irradiation; | A 84.5% B 8% |
methanol
carbon monoxide
2-Chloroanisole
lithium methanolate
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; 5 mol% Pd/C; sodium fluoride In 1,4-dioxane at 150℃; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
Stage #1: methyl salicylate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.333333h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 20℃; for 15h; | 81% |
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 4h; | 74% |
With potassium hydroxide In methanol for 3h; Reflux; | 53% |
With methanol; sodium methylate | |
With potassium carbonate; potassium iodide In acetone Reflux; |
diazomethyl-trimethyl-silane
methyl salicylate
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In methanol; hexane; acetonitrile for 15h; Ambient temperature; | 78% |
dihydroxy-methyl-borane
2-Methoxybenzoic acid
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With pyridine; copper (II) carbonate hydroxide at 90℃; for 24h; Chan-Lam Coupling; | 78% |
Conditions | Yield |
---|---|
With 1,3-bis(dicyclohexylphosphino)propane bis(tetrafluoroborate) salt; palladium diacetate; potassium carbonate In dimethyl sulfoxide at 120℃; for 20h; Molecular sieve; | 74% |
tert.-butylhydroperoxide
2-methoxybenzylamine
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: tert.-butylhydroperoxide; 2-methoxybenzylamine In water; dimethyl sulfoxide Stage #2: In water; dimethyl sulfoxide at 100℃; for 20h; Sealed tube; | 74% |
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran at 70℃; for 0.5h; | 72% |
O-methyl S-p-methylphenyl thiocarbonate
2-Methoxyphenylboronic acid
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane In 1,4-dioxane at 60℃; for 16h; Sealed tube; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,1,3,3-Tetramethyldisiloxane; tricyclohexylphosphine In toluene at 110℃; for 12h; Glovebox; Inert atmosphere; Sealed tube; | 68% |
tert.-butylhydroperoxide
ortho-anisaldehyde
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
With copper (II)-fluoride In water; dimethyl sulfoxide at 120℃; for 12h; Schlenk technique; Inert atmosphere; Green chemistry; | 67% |
Conditions | Yield |
---|---|
With N-iodo-succinimide; 1,10-Phenanthroline; oxygen; potassium carbonate; copper dichloride In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 24h; Molecular sieve; | 60% |
With oxygen; potassium carbonate at 150℃; under 4500.45 Torr; for 24h; Autoclave; | 84 %Chromat. |
methanol
methoxybenzene
N,N-dimethyl-formamide
A
2-methoxybenzoic acid methyl ester
B
ortho-anisaldehyde
Conditions | Yield |
---|---|
Stage #1: methoxybenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexane at -78 - 20℃; for 2h; Stage #3: methanol Further stages; | A 53% B 6% |
pyrrolidine
2-methoxybenzoic acid methyl ester
(2-methoxyphenyl)(pyrrolidin-1-yl)methanone
Conditions | Yield |
---|---|
In acetonitrile at 35℃; under 6000480 Torr; for 96h; | 100% |
2-methoxybenzoic acid methyl ester
methyl 2-methoxy-5-iodobenzoate
Conditions | Yield |
---|---|
With iodine; silver sulfate In methanol at 20℃; for 0.5h; Inert atmosphere; | 99% |
With gold(III) chloride; N-iodo-succinimide In dichloromethane at 20℃; for 24h; Inert atmosphere; | 96% |
With N-iodo-succinimide; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) In dichloromethane; toluene at 20℃; for 14h; regioselective reaction; | 91% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; silver hexafluoroantimonate; 1-methylthiotriptycene In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere; Schlenk technique; | 99% |
With gold(III) chloride; N-Bromosuccinimide In dichloromethane at 80℃; for 23h; Inert atmosphere; | 96% |
With iodine pentoxide; potassium bromide In water at 20℃; for 20h; regioselective reaction; | 92% |
acetic acid tert-butyl ester
2-methoxybenzoic acid methyl ester
tert-butyl 2-methoxybenzoate
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran Ambient temperature; | 98% |
2-methoxybenzoic acid methyl ester
dimethyl methane phosphonate
dimethyl [2-(2-methoxyphenyl)-2-oxoethyl]phosphonate
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran Barbier reaction; Cooling with ice; Inert atmosphere; | 97% |
With n-butyllithium In tetrahydrofuran at -78 - 0℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With platinum(IV) oxide; hydrogen at 60℃; under 750.075 - 1500.15 Torr; for 16h; Autoclave; Green chemistry; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
With aluminium trichloride; sodium iodide at 70 - 80℃; for 2h; | 95% |
With aluminum (III) chloride In dichloromethane at -5 - 25℃; | 94% |
With aluminium(III) iodide In carbon disulfide for 0.9h; Heating; | 76% |
With cerium(III) chloride; sodium iodide In acetonitrile for 20h; dealkylation; Heating; | 67% |
With niobium pentachloride In 1,2-dichloro-ethane for 6h; Heating; |
2-methoxybenzoic acid methyl ester
bis(pinacol)diborane
2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoic acid methyl ester
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 2-(dimethyl(phenyl)silyl)-1-(6-methoxypyridin-2-yl)-2,3-dihydro-1H-naphtho[1,8-de]-[1,3,2]diazaborinine In hexane at 80℃; for 20h; Time; Schlenk technique; Inert atmosphere; | 95% |
With silica-SMAP-Ir(OCH3)(C8H12) In hexane ligand reacted with B-compound in hexane in presence of Ir-complex as catalyst at 25°C for 2 h; | 85% |
With Silica-SMAP-Ir(OMe)(cod) In hexane at 25℃; for 2h; Autoclave; regioselective reaction; | 85% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; (2-(diisopropylsilyl)phenyl)di-p-tolylphosphane In tetrahydrofuran at 80℃; for 16h; Inert atmosphere; Glovebox; Sealed tube; | 82% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; (2-(diisopropylsilyl)phenyl)di-p-tolylphosphane In tetrahydrofuran at 80℃; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: 2-methoxybenzoic acid methyl ester With sodium hydroxide In methanol; water for 2h; Reflux; Stage #2: With hydrogenchloride In methanol; water pH=1; | 94% |
With sodium hydroxide In methanol at 40℃; for 2.5h; | 94.3% |
With potassium hydroxide In methanol at 35℃; for 1h; | 93% |
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol for 4h; Reflux; | 94% |
With hydrazine hydrate In ethanol at 80℃; for 1h; Inert atmosphere; | 92% |
With hydrazine hydrate for 5h; Heating; | 90% |
[hydroxy(tosyloxy)iodo]benzene
2-methoxybenzoic acid methyl ester
Conditions | Yield |
---|---|
In 2,2,2-trifluoroethanol at 20℃; for 17h; | 94% |
Diphenylmethane
2-methoxybenzoic acid methyl ester
A
benzophenone
B
methyl 5-benzhydryl-2-methoxybenzoate
C
1,1,2,2-tetraphenylethane
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride In 1,2-dichloro-ethane at 100℃; for 36h; Inert atmosphere; regioselective reaction; | A 0.14 mmol B 94% C 0.07 mmol |
1-methyl-4-(phenylmethyl)benzene
2-methoxybenzoic acid methyl ester
methyl 2-methoxy-5-(phenyl(p-tolyl)methyl)benzoate
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride In 1,2-dichloro-ethane at 100℃; for 36h; Inert atmosphere; regioselective reaction; | 94% |
methanesulfonic acid
hexamethylenetetramine
2-methoxybenzoic acid methyl ester
methyl 5-formyl-2-methoxybenzoate
Conditions | Yield |
---|---|
at 0 - 90℃; for 16h; Temperature; Large scale; | 94% |
Conditions | Yield |
---|---|
With AlBrCl3(1-)*C5H5N*H(1+) at 140℃; for 3h; | 93% |
With lithium chloride In N,N-dimethyl-formamide for 22h; Heating; | 90% |
With iodine; aluminium In cyclohexane at 80℃; for 18h; Solvent; Reagent/catalyst; | 86% |
2-methoxybenzoic acid methyl ester
(p-fluorophenyl)trimethylsilane
4'-fluoro-4-methoxy-biphenyl-3-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With (Ph3P)Au(I)(OTs); [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid In methanol; chloroform at 20℃; | 92% |
Conditions | Yield |
---|---|
With iodine; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; for 6h; Sealed tube; | 92% |
With iodine; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; for 6h; | 92% |
With iodine; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 6h; | 92% |
2-methoxybenzoic acid methyl ester
1-methoxy-2-methoxymethylbenzene
Conditions | Yield |
---|---|
With aluminium(III) triflate; tris(2,4-pentanedionato)ruthenium(III); hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In deuteromethanol; toluene at 130℃; under 30402 Torr; for 12h; Autoclave; | 91% |
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